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Bartolotta, P. A.

Publications and source records attributed to Bartolotta, P. A..

Microstructure, Mechanical Properties, Hot-Die Forming, and Joining of 47XD Gamma TiAl Rolled Sheets

The microstructure and mechanical properties, along with the hot-die forming and joining of Ti-47Al-2Nb-2Mn-0.8 vol% TiB, sheets (known as 47XD), produced by a low-cost rolling process, were evaluated. A near-gamma microstructure was obtained in the as-rolled condition. The microstructures of heat-treated sheets ranged from a recrystallized equiaxed near-gamma microstructure at 1,200 to 1,310 C, to a duplex microstructure at 1,350 C, to a fully lamellar microstructure at 1,376 C. Tensile behavior was determined for unidirectionally rolled and cross-rolled sheets for room temperature (RT) to 816 C. Yield stress decreased gradually with increasing deformation temperature up to 704 C; above 704 C, it declined rapidly. Ultimate tensile strength exhibited a gradual decrease up to 537 C before peaking at 704 C, followed by a rapid decline at 816 C. The modulus showed a gradual decrease with temperature, reaching approximately 72% of the RT value at 816 C. Strain to failure increased slowly from RT to 537 C; between 537 C and 704 C it exhibited a phenomenal increase, suggesting that the ductile-brittle transition temperature was below 704 C. Fracture mode changed from transgranular fracture at low temperature, to a mixture of transgranular and intergranular fracture at intermediate temperature, to ductile fracture at 816 C, coupled with dynamic recrystallization at large strains. Creep rupture response was evaluated between 649 and 816 C over the stress range of 69 to 276 MPa. Deformation parameters for steady-state creep rate and time-to-rupture were similar: activation energies of approximately 350 kJ/mol and stress exponents of approximately 4.5. Hot-die forming of sheets into corrugations was done at elevated temperatures in vacuum. The process parameters to join sheets by diffusion bonding and brazing with TiCuNi 70 filler alloy were optimized for test coupons and successfully used to fabricate large truss-core and honeycomb structures. Nondestructive evaluation methods, e.g., ultrasonic C-scans and thermography along with metallography, were used to characterize bond quality. Microstructural evaluation during heat treatment, identification of phases at the braze/matrix interface, determination of shear strengths of brazed joints, and deformation mechanisms during tensile and creep processes will be discussed.

Das, G.↗

Failure Mechanisms During Isothermal Fatigue of SiC/Ti-24Al-11Nb Composites

Failure mechanisms during isothermal fatigue of unidirectional SiC/Ti-24Al-11Nb (at.%) composites have been determined by microstructural analysis of samples from tests interrupted prior to the end of life and from tests conducted to failure. Specimens from three regions of life were examined based on the maximum strain from a fatigue life diagram: Region 1 (high strain), Region 2 (mid-strain) and Region 3 (low strain). Crack lengths were also measured from interrupted samples and compared based on temperature (23-815 C), region of life and numbers of cycles. Region 1 was controlled by fiber-dominated failure. A transition zone was observed between Regions 1 and 2 due to competition between failure mechanisms. Failure in Region 2 was generally described as surface-initiated cracking with varying amounts of fiber bridging. However, the specific descriptions of crack propagation through the fibers and matrix varied with strain and temperature over this broad region. Region 3 exhibited endurance behaviour at 23 C with no cracking after lO(exp 6) cycles. However at 425 C, surface-initiated cracking was observed after 10(exp 6) cycles with fractured fibers in the crack wake. If endurance behaviour exists for conditions of isothermal fatigue in air at temperatures of greater than or equal to 425 C, it may only be found at very low strains and at greater than 10(exp 6) cycles.

Brindley, P. K.↗

ASTM and VAMAS activities in titanium matrix composites test methods development

Titanium matrix composites (TMC's) are being considered for a number of aerospace applications ranging from high performance engine components to airframe structures in areas that require high stiffness to weight ratios at temperatures up to 400 C. TMC's exhibit unique mechanical behavior due to fiber-matrix interface failures, matrix cracks bridged by fibers, thermo-viscoplastic behavior of the matrix at elevated temperatures, and the development of significant thermal residual stresses in the composite due to fabrication. Standard testing methodology must be developed to reflect the uniqueness of this type of material systems. The purpose of this paper is to review the current activities in ASTM and Versailles Project on Advanced Materials and Standards (VAMAS) that are directed toward the development of standard test methodology for titanium matrix composites.

Johnson, W. S.↗

Unified Viscoplastic Behavior of Metal Matrix Composites

The need for unified constitutive models was recognized more than a decade ago in the results of phenomenological tests on monolithic metals that exhibited strong creep-plasticity interaction. Recently, metallic alloys have been combined to form high-temperature ductile/ductile composite materials, raising the natural question of whether these metallic composites exhibit the same phenomenological features as their monolithic constituents. This question is addressed in the context of a limited, yet definite (to illustrate creep/plasticity interaction) set of experimental data on the model metal matrix composite (MMC) system W/Kanthal. Furthermore, it is demonstrated that a unified viscoplastic representation, extended for unidirectional composites and correlated to W/Kanthal, can accurately predict the observed longitudinal composite creep/plasticity interaction response and strain rate dependency. Finally, the predicted influence of fiber orientation on the creep response of W/Kanthal is illustrated.

Arnold, S. M.↗

Fatigue life prediction of an intermetallic matrix composite at elevated temperatures

A strain-based fatigue life prediction method is proposed for an intermetallic matrix composite (IMC) under tensile cyclic loadings at elevated temperatures. Styled after the 'Universal Slopes' method, the model utilizes the composite's tensile properties to estimate fatigue life. Factors such as fiber volume ratio (Vf), number of plys and temperature dependence are implicitly incorporated into the model through these properties. The model constants are determined by using unidirectional fatigue data at temperatures of 425 and 815 C. Fatigue lives from two independent sources are used to verify the model at temperatures of 650 and 760 C. Cross-ply lives at 760 C are also predicted. It is demonstrated that the correlation between experimental and predicted lives is within a factor of two.

Bartolotta, P. A.↗

High temperature fatigue behavior of a SiC/Ti-24Al-11Nb composite

A series of tension-tension strain- and load-controlled tests were conducted on unidirectional SiC/Ti-24Al-11Nb (at percent) composites at 425 and 815 C. Several regimes of damage were identified using Talrega's concept of fatigue life diagrams. Issues of test technique, test control mode, and definition of failure were also addressed.

Bartolotta, P. A.↗

Investigation of a SiC/Ti-24Al-11Nb composite

A summary of ongoing research on the characterization of a continuous fiber reinforced SiC/Ti-24Al-11Nb (at percent) composite is presented. The powder metallurgy fabrication technique is described as are the nondestructive evaluation results of the as-fabricated composite plates. Tensile properties of the SiC fiber, the matrix material, and the 0-deg SiC/Ti-24Al-11Nb composite (fibers oriented unidirectionally, parallel to the loading axis) from room temperature to 1100 C are presented and discussed with regard to the resultant fractography. The as-fabricated fiber-matrix interface has been examined by scanning transmission electron microscopy and the compounds present in the reaction zone have been identified. Fiber-matrix interaction and stability of the matrix near the fiber is characterized at 815, 985, and 1200 C from 1 to 500 hr. Measurements of the fiber-matrix reaction, the loss of C-rich coating from the surface of the SiC fiber, and the growth of the Beta depleted zone in the matrix adjacent to the fiber are presented. These data and the difference in coefficient of thermal expansion between the fiber and the matrix are discussed in terms of their likely effects on mechanical properties.

Brindley, P. K.↗

Use of inelastic strain as a basis for analyzing thermomechanical test data

It was shown that the proposed data analysis method, based on inelastic strain-time response, can be used effectively to represent cyclic response at elevated temperatures for Hastelloy-X. A high level of confidence in this method was built by making comparisons of the experimental and fitted data in two forms. Because of this level of confidence, the analysis was taken one step further and inelastic strain rates were calculated from the derivatives of the fit equations.

Bartolotta, P. A.↗

Preliminary study of creep thresholds and thermomechanical response in Haynes 188 at temperatures in the range 649 to 871 C

The following conclusions were drawn from this study of creep thresholds and thermomechanical response: (1) creep threshold can be determined using the latest electrohydraulic test equipment, providing that test durations are short and relatively large accumulations of creep strain are used in defining the threshold; (2) significant creep strains were measured under monotonic loading as stress levels as low as 4 ksi at temperatures predicted for solar receiver service; and (3) the material exhibited creep ratchetting during simulated service cycles, a result not predicted by analysis using current constitutive models for Haynes 188.

Ellis, J. R.↗

The NASA Lewis Research Center High Temperature Fatigue and Structures Laboratory

The physical organization of the NASA Lewis Research Center High Temperature Fatigue and Structures Laboratory is described. Particular attention is given to uniaxial test systems, high cycle/low cycle testing systems, axial torsional test systems, computer system capabilities, and a laboratory addition. The proposed addition will double the floor area of the present laboratory and will be equipped with its own control room.

Mcgaw, M. A.↗

Thermomechanical characterization of Hastelloy-X under uniaxial cyclic loading

In most high-temperature engineering applications, components are subjected to complex combinations of thermal and mechanical loading during service. A number of viscoplastic constitutive models were proposed which potentially can provide mathematical descriptions of material response under such conditions. Implementation of these models into large finite element codes such as MARC has already resulted in much improved inelastic analysis capability for hot-section aircraft engine components. However, a number of questions remain regarding the validity of methods adopted in characterizing these constitutive models for particular high-temperature materials. One area of concern is that the majority of experimental data available for this purpose are determined under isothermal conditions. This is in contrast to service conditions which, as noted above, almost always involve some form of thermal cycling. The obvious question arises as to whether a constitutive model characterized using an isothermal data base can adequately predict material response under thermomechanical conditions. An experimental program was initiated within the HOST program to address this particular concern. The results of the most recent isothermal and thermomechanical experiments are described.

Ellis, J. R.↗

Thermomechanical cyclic hardening behavior of Hastelloy-X

Experimental evidence of thermomechanical history dependence on the cyclic hardening behavior of a representative combustor liner material Hastelloy-X is presented, along with a discussion about the relevant concept of thermomechanical path dependence. Based on the experimental results, a discussion is given on the inadequacy of formulating nonisothermal constitutive equations solely on the basis of isothermal testing. Finally, the essence of a mathematical representation of thermoviscoplasticity is presented that qualitatively accounts for the observed hereditary behavior. This is achieved by formulating the scaler evolutionary equation in an established viscoplastic theory to reflect thermomechanical path dependence. Although the necessary nonisothermal tests for further quantifying the thermoviscoplastic model have been identified, such data are not yet available.

Bartolotta, P. A.↗

Viscoplastic constitutive relationships with dependence on thermomechanical history

Experimental evidence of thermomechanical history dependence in the cyclic hardening behavior of some common high-temperature structural alloys is presented with special emphasis on dynamic metallurgical changes. The inadequacy of formulating nonisothermal constitutive equations solely on the basis of isothermal testing is discussed. A representation of thermoviscoplasticity is proposed that qualitatively accounts for the observed hereditary behavior. This is achieved by formulating the scalar evolutionary equation in an established viscoplasticity theory to reflect thermomechanical path dependence. To assess the importance of accounting for thermomechanical history dependence in practical structural analyses, two qualitative models are specified: (1) formulated as if based entirely on isothermal information; (2) to reflect thermomechanical path dependence using the proposed thermoviscoplastic representation. Predictions of the two models are compared and the impact the calculated differences in deformation behavior may have on subsequent lifetime predictions is discussed.

Robinson, D. N.↗