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C. J. Snead

Publications and source records attributed to C. J. Snead.

Investigating Space Weathering of Ryugu Grains Using Electron Microscopy and X-Ray Computed Tomography

The effects of micrometeorite bombardment and solar wind ion irradiation – collectively known as space weathering – alter the microstructural, chemical, and spectral properties of airless surfaces. Characteristics of space weathering include vesiculated textures, amorphous grain rims (upper ~100 nm), and the production of Fe-bearing nanoparticles (npFe). The resulting modifications in the optical properties of the surface regolith include changes in spectral slope and overall reflectance of the surfaces as well as the attenuation of their characteristic absorption bands across VIS-NIR wavelengths. As the surface is continuously exposed to interplanetary space over time, the accrual of these features complicates the interpretation of remote sensing spectral data and the characterization of returned samples. Laboratory experiments that simulate solar wind irradiation and micrometeoroid impacts using carbonaceous analogs have revealed novel and complex microstructural and chemical changes, including the decrease in organic species concentrations and the reduction of Fe 3+ . In 2020, the Japan Aerospace Exploration Agency (JAXA)’s Hayabusa2 mission returned over 5 g of regolith particles from near- Earth C-type asteroid (162173) Ryugu – a unique opportunity to study space weathering on carbonaceous materials. Initial studies have established that the surface morphology and chemical signatures of space weathering in returned samples share characteristics with laser irradiation experiments simulating micrometeoroid bombardment, indicating that impacts are a significant space weathering mechanism operating on Ryugu. Here, we seek to improve our understanding of space weathering of carbonaceous asteroidal regolith grains by characterizing its effects directly on returned samples to determine the nature of space weathering on Ryugu. To do so, we performed coordinated analyses using electron beam techniques and X-ray computed tomography (XCT) to examine the effects of space weathering on grains returned from the surface of Ryugu by the Hayabusa2 mission.

L. E. Melendez↗

Investigating the Physical Modification of the Bennu Sample During Entry, Descent, and Landing

On September 24, 2023, the OSIRIS-REx Sample Return Capsule (SRC) entered Earth’s atmosphere and landed in the Utah Test and Training Range (UTTR). Preliminary examination of the returned Bennu sample has confirmed that OSIRIS-REx sample mass exceeds the mission requirement of 60 g of material. The sample consists of particles that range from a few centimeters to microscopic fines. During the SRC’s entry, descent, and landing (EDL) sequence, it may have experienced (i) peak decelerations of 10s of g (ii) tumbling, and (iii) touchdown at approximately 10 m/s, which could have induced physical modification of the sample. In addition, the act of sampling may have altered or biased the physical properties of the collected materials. Here, we investigate the likelihood and extent of physical modification of the sample between collection and return using observations and modeling. This work addresses the mission’s hypothesis 12, which concerns, in part, the modification of the sample during collection and Earth entry.

asteroid↗

Curation planning and facilities for asteroid Bennu samples returned by the OSIRIS-REx mission

NASA's OSIRIS-REx spacecraft collected samples from carbonaceous near-Earth asteroid (101955) Bennu on October 20, 2020, and will deliver them to the Earth on September 24, 2023. The samples will be processed at the NASA Johnson Space Center (JSC), where most of the sample collection will be subsequently curated in a new cleanroom suite. The spacecraft collected loose regolith two ways: in a bulk sample chamber capable of holding up to 2 kg, and on industrial Velcro “contact pads” intended to collect small particles at the surface. Included in the JSC collection will be the bulk sample, the contact pads, contamination-monitoring witness plates, and supporting hardware. Planning for the curation of the samples and hardware started at the earliest phase of proposal development and continued in parallel with project development and execution. Because a major mission goal is characterization of organic compounds in the Bennu samples, extra effort was spent in the design stage to ensure a clean curation environment. Here, we describe the preparations to receive the sample, including the design, construction, outfitting, and monitoring of the cleanrooms at JSC; the planned recovery of the sample-containing capsule when it lands on Earth; and the approach to characterizing and cataloging the samples. These curation efforts will result in the distribution of pristine Bennu samples from JSC to the OSIRIS-REx science team, international partners, and the global scientific community for years to come.

curation↗

Characterizing Space Weathering Features in Grains From Asteroid Ryugu

Airless bodies such as asteroids are characterized by a lack of a protective atmosphere to guard against the effects of micrometeorite bombardment and solar wind irradiation. These processes, cumulatively known as space weathering, alter the microstructural and chemical properties of grains on asteroidal surfaces, signatures of which are recognized as vesiculated textures, amorphous grain rims, and fe-bearing nanoparticles. The accumulation of these features also causes changes in the optical properties of the surface regolith, complicating the interpretation of remote sensing data and the characterization of returned samples.

L. E. Melendez↗

Small Particle Glovebox Experiments - Preliminary Results

A substantial portion of the asteroid samples returned by the HAYABUSA2 and OSIRIS-REx missions will consist of small (submm) components (due to the collection of those particles on the asteroid surface and due to the fragmenting of larger, friable material post-collection). In order to minimize the alteration/oxidation of asteroid regolith, the bulk collections will be stored and curated in nitrogen purged gloveboxes. The processing of small particles in an N2 glovebox will present challenges that are different from those experienced during lunar and meteorite sample processing. Particles in this size range are susceptible to unpredictable electrostatic charging that can result in sample loss during processing operations. Methods for the handling of sub-mm particles have been well developed for environments with ambient atmospheric conditions and relative humidity (RH) ranges between 40-70%. In such conditions, a number of factors can be successfully employed to minimize the effects of triboelectric charging, including the use of Po-210 sources that neutralize excess charge and the utilization of conductive manipulation tools and sample substrates. However, relative humidity levels above 40% also contribute significantly to dissipation of triboelectric effects. We had not previously investigated our charge mitigation methods in a completely dry, nitrogen-purged environment, or whether they would be sufficient in enabling the successful processing of sub-mm samples. Current glovebox configurations in use in our lunar and meteorite curation laboratories are optimized for the processing of macroscopic samples and tools; these glovebox designs are likely unsuitable for the processing of collections for which the bulk collection is comprised of sub-mm components. Small particle sample preparation requires the use of an optical magnification instrument – typically a stereo binocular microscope with at least 20x magnification. Current glovebox designs are not optimized for the utilization or integration of stereo microscopes; while many current cabinets include microscope viewports that enable the use of small, externally mounted stereo microscopes, the focusing methods (usually involving the use of a lab jack) lack the fidelity and precision required for small particle manipulation and imaging. Working distances of higher (>50x magnification) objective lenses may preclude the external use of a stereo microscope through a viewport; in order to successfully manipulate and image very small (< 20m) particles, stereo and digital microscope systems that are integrated within the glovebox should be investigated. Finally, ergonomic considerations for small particle work within a glovebox must be considered to minimize risk of injury to sample processors. In order to investigate some of the unknown parameters relating to small particle processing within an N2 glovebox, we conducted preliminary, qualitative experiments utilizing a small lunar cabinet that was originally used for film development.

C. J. Snead↗

Hydrated Interplanetary Dust Particles: Implications for Oxygen Reservoirs in the Outer Solar System

A re-evaluation of solar energetic particle (SEP) track densities in interplanetary dust particles (IDPs) show that many are derived from outer solar system parent bodies such as Kuiper belt objects (KBOs) or beyond. Kuiper belt objects are widely believed to represent the frozen remnants from the birth of the solar system. The population of track-rich IDPs include members from both the anhydrous chondritic-porous and hydrated chondritic-smooth classes and earlier work suggested that the hydrated IDPs may represent anhydrous IDP material that was aqueously altered. We are performing systematic studies of the mineralogy, chemistry and isotopic compositions of track-rich IDPs to gain a fuller understanding of the origin and evolution of KBOs. Here, we focus on the identification of hydrated Kuiper belt dust particles that allows for the direct evaluation of their O isotopic compositions and the implications for the oxygen isotopic composition of outer solar system ices.

L. P. Keller↗

Materials-Compliant Containers in Preparation for OSIRIS-REx Sample Return

The Origins, Spectral Interpretation, Resource Identification, and Security–Regolith Explorer (OSIRIS-REx) is a spacecraft that collected samples from near-Earth asteroid Bennu in 2020. NASA is expecting OSIRIS-REx to return about 250 grams of Bennu dust particles and rocky material (regolith) in the Sample Return Capsule landing on September 24, 2023.This carbonaceous material is predicted to be rich in water and organic compounds that will provide key information on the solar system's genesis. The NASA Johnson Space Center (JSC) curation team is preparing to process the returned regolith and flight hardware to support critical scientific investigations worldwide.

Curation↗