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Chouhan, V.

Publications and source records attributed to Chouhan, V..

Excellent performance of 650 MHz single-cell niobium cavity after electropolishing

Electropolishing process and cathodes have undergone modification and optimization for both low- and high-beta 650 MHz five-cell niobium cavities for PIP-II. Cavities treated with these modified electropolishing conditions exhibited smooth surfaces and good performance in baseline tests. Nonetheless, due to administrative constraints on project cavities, maximum gradient performance testing was not conducted. This paper presents a study conducted on a single-cell 650 MHz cavity utilizing the optimized electropolishing conditions, highlighting the maximum performance attained for this specific cavity. The cavity tested at 2 K in a vertical cryostat reached a superior accelerating field gradient of 53.3 MV/m at Q0 of 1.6x1010, which is the highest gradient attained for this type of large-sized cavities.

43 PARTICLE ACCELERATORS↗

Study of Mechanical Grinding Effects on Niobium Surface

Mechanical grinding is commonly employed to eliminate surface defects such as scratches and pits from niobium cavity surfaces or sheets before cavity fabrication. Subsequently, chemically buffered polishing or electropolishing is often utilized to completely remove residues of the polishing media and any defects induced by mechanical grinding, ensuring a pristine surface. In this study, we conducted a systematic investigation to assess the influence of mechanical grinding using silicon carbide (SiC) and aluminium oxide (Al2O3) polishing media on niobium surfaces. Additionally, the study examines the effects of post-mechanical grinding chemical treatments on surface quality.

Chouhan, V.↗

Transfer of EP and Doping Technology for PIP-II HB650 Cavities from Fermilab to Industry

Fermilab has optimized the surface processing conditions for PIP-II high beta 650 MHz cavities. This encompasses conditions for bulk electropolishing, heat treatment, nitrogen doping, post-doping final electropolishing, and post-processing surface rinsing. The technology has been effectively transitioned to industry. This paper highlights the efforts made to fine-tune the process and to smoothly share them with the partner labs and an associated vendor.

Chouhan, V.↗

Study of Mechanical Grinding Effects on Niobium Surface

Mechanical grinding is commonly employed to eliminate surface defects such as scratches and pits from niobium cavity surfaces or sheets before cavity fabrication. Subsequently, chemically buffered polishing or electropolishing is often utilized to completely remove residues of the polishing media and any defects induced by mechanical grinding, ensuring a pristine surface. In this study, we conducted a systematic investigation to assess the influence of mechanical grinding using silicon carbide and aluminum oxide polishing media on niobium surfaces. Additionally, the study examines the effects of post-mechanical grinding chemical treatments on surface quality.

Chouhan, V.↗

Visual, Optical and Replica Inspections: Surface Preparation of 650 MHz NB Cavity for PIP-II Linac

Surface preparation of niobium superconducting RF cavities is a critical step for achieving good RF performance under the superconducting state. Surface defect, roughness, and contamination affect the accelerating gradient and quality factor of the cavities. We report surface inspection methods used to control the surface processing of 650 MHz cavities designated for the pre-production and prototype cryomodules for PIP-II linac. The cavity surface was routinely inspected visually, with an optical camera, and by microscopic scanning of surface replicas. This article covers details on the surface inspection methods and surface polishing process used to repair the surface.

43 PARTICLE ACCELERATORS↗

Electropolishing Study on Nitrogen-doped Niobium Surface

The nitrogen doping (N-doping) process is applied to niobium (Nb) superconducting cavities to enhance their quality factors. The N-doping is followed by an electropolishing process that provides the final surface of the cavities. A controlled EP process is necessary to get the benefit of N-doping and achieve a high accelerating gradient. We have performed electropolishing of N-doped Nb surface under various conditions to understand their impact on the surface. A modified EP process was developed to obtain a smooth pit-free surface.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Electropolishing parameters study for surface smoothening of low-$\beta$650 MHz five-cell niobium superconducting radio frequency cavity

Electropolishing (EP) is applied to niobium (Nb) superconducting radio frequency (SRF) cavities, which are used in particle accelerators for their surface treatment. The EP process for 1.3 GHz cavities has been extensively studied earlier. In this work, a parametric study on EP of low-β (0.61) 650 MHz Nb SRF cavities (LB650), which will be used in pre-production cryomodule for proton improvement plan-II (PIP-II) linear accelerator, was conducted to determine adequate EP conditions for attaining a smooth surface of the cavities. EP performed with the standard parameters and an initial cathode (cathode-I) having a cathode surface area of ~5% of the cavity surface area yielded a rough equator surface of the cavity. The grain step height on the equator weld position was measured to be ~ 32 μm. The rough surface was attributed to preferential grain etching confirmed by a polarization curve showing a linear relationship between the EP current and voltage and the absence of the current plateau region. The cathode was modified to make its surface area twice that of cathode-I. The modified cathode (cathode-M) provided a current plateau region in the corresponding I-V curves measured at different cavity temperatures. The onset voltage for the plateau was found to be higher at higher cavity temperatures. Here this study revealed that even with cathode-M, the standard 18 V was low for EP of such large-sized cavities when the cavity temperature was 18 °C. EP performed at a higher voltage of 22–24.5 V with cathode-M yielded a smooth surface with a grain step height of only 0.6 μm. The applied EP conditions also improved removal uniformity along the cavity length. In contrast to the cavity treated with cathode-I, the cavities treated with cathode-M achieved a significantly higher accelerating gradient (E acc ) in vertical tests conducted in a cryostat at 2 K. The modified EP was found efficient to produce the cavities that achieved E acc of 22.4 MV/m, required by PIP II project in the baseline RF tests, to qualify for further surface processing used to enhance their quality factors.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Effect of Electropolishing on Nitrogen Doped and Undoped Niobium Surfaces

Cold electropolishing (EP) of a nitrogen-doped (N-doped) niobium (Nb) superconducting RF (SRF) cavity was found to improve its quality factor. In order to understand the effect of EP temperature on N-doped and undoped surfaces, a systematic EP study was conducted with 2/0 N-doped and heat-treated Nb samples in a beaker. The Nb samples were electropolished at different surface temperatures ranging from 0 to 42 C. The results showed that the doped surface was susceptible to the sample temperature during EP. EP resulted in the surface pitting on the doped samples where the number density of pits increased at a higher temperature. The surface results were compared with the surface of cutouts from a 9-cell cavity which was 2/0 N-doped and electropolished. This paper shows de-tailed surface features of the N-doped and undoped Nb surfaces electropolished at different temperatures.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Study on Electropolishing Conditions for 650 MHz Niobium SRF Cavity

The PIP II linear accelerator includes different types of niobium SRF cavities including 650 MHz elliptical low (0.61) and high (0.92) beta cavities. The elliptical cavity surface is processed with the electropolishing method. The elliptical cavities especially the low-$\beta$ 650 MHz cavities showed a rough equator surface after the EP was per-formed with the standard EP conditions. This work was focused to study the effect of different EP parameters, including cathode surface area, temperature and voltage, and optimize them to improve the cavity surface.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Computational Fluid Dynamic Simulation for Electrolyte Flow in Horizontal EP of Nb SRF Elliptical Cavities

An electrolyte flow velocity on an electropolishingsurface affects a material removal rate where higherremoval is observed with a higher velocity of theelectrolyte. In horizontal EP (HEP) of an ellipticalcavity, an electrolyte flow near the equator positionmight remain slow and responsible for a lowerremoval compared to that on the iris and beam pipepositions. In order to understand the flow dynamicon an elliptical cavity surface in the horizontal EPprocess, a computational fluid dynamic simulationwas conducted. This study was conducted on 1.3GHz cavity with different cathodes and acid flowrates. Final aim of the study is to improve the flowuniformity to attain uniform removal especially inmulticell cavities.

Chouhan, V.↗