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Frank, D.

Publications and source records attributed to Frank, D..

At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS2020

Isotopes of H, N, and O in H Chondrite Xenoliths

Brecciated H chrondites host a variety of xenoliths, including unshocked, phyllosilate-rich carbonaceous chondrites (CCs) [1-2]. The brecciated H chondrite Zag (H3-6) is one of two chondrites to host macroscopic (1 - 5mm), xenolithic crystals of halite (NaCl) with aqueous fluid inclusions and organics [3-4]. A ~1cm CC xenolith in Zag (Zag clast) also encloses halite in its matrix, linking the halite and the xenolith to the same parent object. The Zag clast has mineralogy similar to CI chondrites, but it has a unique bulk oxygen isotopic composition among all meteorites (Δ17O = 1.49 Âą 0.04 ‰, ð›ŋ18O = 22.38 Âą 0.17 ‰) and is therefore derived from a uniquely sampled parent object [5-6]. Organics have high bulk ð›ŋD and ð›ŋ15N values with isotopic "hotspots" similar to organics in CR chondrites and Bells (C2-ung.) [6-7]. Bulk ð›ŋ15N is also similar to CRs and Bells [7]. We provide further isotopic characterization of the Zag clast to constrain the formation temperature and origin of its primary and secondary components.

Frank, D.↗
NASA NTRS2014

Stardust Interstellar Preliminary Examination IX: High-Speed Interstellar Dust Analog Capture in Stardust Flight-Spare Aerogel

The NASA Stardust mission used silica aerogel slabs to slowly decelerate and capture impinging cosmic dust particles for return to Earth. During this process, impact tracks are generated along the trajectory of the particle into the aerogel. It is believed that the morphology and dimensions of these tracks, together with the state of captured grains at track termini, may be linked to the size, velocity, and density of the impacting cosmic dust grain. Here, we present the results of laboratory hypervelocity impact experiments, during which cosmic dust analog particles (diameters of between 0.2 and 0.4 lm), composed of olivine, orthopyroxene, or an organic polymer, were accelerated onto Stardust flight spare low-density (approximately 0.01 g/cu cm) silica aerogel. The impact velocities (3-21 km/s) were chosen to simulate the range of velocities expected during Stardust's interstellar dust (ISD) collection phases. Track lengths and widths, together with the success of particle capture, are analyzed as functions of impact velocity and particle composition, density, and size. Captured terminal particles from low-density organic projectiles become undetectable at lower velocities than those from similarly sized, denser mineral particles, which are still detectable (although substantially altered by the impact process) at 15 km/s. The survival of these terminal particles, together with the track dimensions obtained during low impact speed capture of small grains in the laboratory, indicates that two of the three best Stardust candidate extraterrestrial grains were actually captured at speeds much lower than predicted. Track length and diameters are, in general, more sensitive to impact velocities than previously expected, which makes tracks of particles with diameters of 0.4 lm and below hard to identify at low capture speeds (<10 km/s). Therefore, although captured intact, the majority of the interstellar dust grains returned to Earth by Stardust remain to be found.

Stardust↗
NASA NTRS2014

Surviving High-temperature Components in CI Chondrites

The CI1 chondrites, while having the most solar-like compo-sition of any astromaterial available for laboratory analysis, have also been considerably altered by asteroidal processes including aqueous alteration. It is of fundamental importance to determine their pre-alteration mineralogy, so that the state of matter in the early Solar System can be better determined. In the course of a re-examination of the compositional range of olivine and low-Ca pyroxene in CI chondrites Orgueil, Ivuna and Alais [1] we found the first reported complete CAI, as already reported [2], with at-tached rock consisting mainly of olivine and low-Ca pyroxene. The range of residual olivine major element compositions we have determined in the CIs (Fig. 1) may now be directly com-pared with those of other astromaterials, including Wild 2 grains. The abundance of olivine and low-Ca pyroxene in CIs is higher than is generally appreciated, and in fact much higher than for some CMs [1]. We also noted numerous rounded objects varying in shape from spheres to oblate spheroids, and ranging up to 100Ξm in size (Fig. 2), which have been previously noted [3] but have not been well documented or appreciated. We characterized the mineralogy by transmission electron microscopy and found that they consist mainly of rather fine-grained, flaky single phase to intergrown serpentine and saponite. These two materials in fact dominate the bulk of the host CI1 chondrites. With the exception of sparse spinels, the rounded phyllosilicate objects are remarka-bly free of other minerals, suggesting that the precursor from which the phyllosilicates were derived was a homogeneous mate-rial. We suggest that these round phyllosilicates aggregates in CI1 chondrites were cryptocrystalline to glassy microchondrules. If so then CI chondrites cannot be considered chondrule-free. Small though they are, the abundance of these putative microchondrules is the same as that of chondrules in the Tagish Lake meteorite.

Zolensky, M.↗
NASA NTRS2014

Collecting Comet Samples by ER-2 Aircraft: Cosmic Dust Collection During the Draconid Meteor Shower in October 2012

Many tons of dust grains, including samples of asteroids and comets, fall from space into the Earth's atmosphere each day. NASA periodically collects some of these particles from the Earth's stratosphere using sticky collectors mounted on NASA's high-flying aircraft. Sometimes, especially when the Earth experiences a known meteor shower, a special opportunity is presented to associate cosmic dust particles with a known source. NASA JSC's Cosmic Dust Collection Program has made special attempts to collect dust from particular meteor showers and asteroid families when flights can be planned well in advance. However, it has rarely been possible to make collections on very short notice. In 2012, the Draconid meteor shower presented that opportunity. The Draconid meteor shower, originating from Comet 21P/Giacobini-Zinner, has produced both outbursts and storms several times during the last century, but the 2012 event was not predicted to be much of a show. Because of these predictions, the Cosmic Dust team had not targeted a stratospheric collection effort for the Draconids, despite the fact that they have one of the slowest atmospheric entry velocities (23 km/s) of any comet shower, and thus offer significant possibilities of successful dust capture. However, radar measurements obtained by the Canadian Meteor Orbit Radar during the 2012 Draconids shower indicated a meteor storm did occur October 8 with a peak at 16:38 (+/-5 min) UTC for a total duration of approximately 2 hours.

Bastien, Ron↗
NASA NTRS2013

The Hayabusa Curation Facility at Johnson Space Center

The Japan Aerospace Exploration Agency (JAXA) Hayabusa spacecraft made contact with the asteroid 25143 Itokawa and collected regolith dust from Muses Sea region of smooth terrain [1]. The spacecraft returned to Earth with more than 10,000 grains ranging in size from just over 300 Ξm to less than 10 Ξm [2, 3]. These grains represent the only collection of material returned from an asteroid by a spacecraft. As part of the joint agreement between JAXA and NASA for the mission, 10% of the Hayabusa grains are being transferred to NASA for parallel curation and allocation. In order to properly receive process and curate these samples, a new curation facility was established at Johnson Space Center (JSC). Since the Hayabusa samples within the JAXA curation facility have been stored free from exposure to terrestrial atmosphere and contamination [4], one of the goals of the new NASA curation facility was to continue this treatment. An existing lab space at JSC was transformed into a 120 sq.ft. ISO class 4 (equivalent to the original class 10 standard) clean room. Hayabusa samples are stored, observed, processed, and packaged for allocation inside a stainless steel glove box under dry N2. Construction of the clean laboratory was completed in 2012. Currently, 25 Itokawa particles are lodged in NASA's Hayabusa Lab. Special care has been taken during lab construction to remove or contain materials that may contribute contaminant particles in the same size range as the Hayabusa grains. Several witness plates of various materials are installed around the clean lab and within the glove box to permit characterization of local contaminants at regular intervals by SEM and mass spectrometry, and particle counts of the lab environment are frequently acquired. Of particular interest is anodized aluminum, which contains copious sub-mm grains of a multitude of different materials embedded in its upper surface. Unfortunately the use of anodized aluminum was necessary in the construction of the clean room frame to strengthen it and eliminate corrosion and wear over time. All anodized aluminum interior to the lab was thus covered or replaced by minimally contaminating materials.

Zolensky, M.↗
NASA NTRS2012

Status of the Stardust ISPE and the Origin of Four Interstellar Dust Candidates

Some bulk properties of interstellar dust are known through infrared and X-ray observations of the interstellar medium. However, the properties of individual interstellar dust particles are largely unconstrained, so it is not known whether individual interstellar dust particles can be definitively distinguished from interplanetary dust particles in the Stardust Interstellar Dust Collector (SIDC) based only on chemical, mineralogical or isotopic analyses. It was therefore understood from the beginning of the Stardust Interstellar Preliminary Examination (ISPE) that identification of interstellar dust candidates would rest on three criteria - broad consistency with known extraterrestrial materials, inconsistency with an origin as secondary ejecta from impacts on the spacecraft, and consistency, in a statistical sense, of observed dynamical properties - that is, trajectory and capture speed - with an origin in the interstellar dust stream. Here we quantitatively test four interstellar dust candidates, reported previously [1], against these criteria.

Westphal, A. J.↗
NASA NTRS2012

Coordinated Analyses of Diverse Components in Whole Stardust Cometary Tracks

Analyses of samples returned from Comet Wild-2 by the Stardust spacecraft have resulted in a number of surprising findings that show the origins of comets are more complex than previously suspected [1]. Stardust aerogel tracks show considerable compositional diversity and the degree of impact related thermal modification and destruction is also highly variable. We are performing systematic examinations of entire Stardust tracks to discern the representative mineralogy and origins of comet Wild 2 components and to search for well preserved fine grained materials. Previously, we used ultramicrotomy to prepare sequential thin sections of entire "carrot" and "bulbous" type tracks along their axis while preserving their original shapes [2]. This technique allows us to characterize the usually well-preserved terminal particle (TP), but also any associated, fine-grained fragments that were shed along the track pathway. This report focuses on coordinated analyses of surviving indigenous cometary materials (crystalline and amorphous) along the aerogel track walls, their interaction with aerogel during collection and comparisons with their TPs. We examined the distribution of fragments throughout the track from the entrance hole to the TP.

Nakamura-Messenger, K.↗
NASA NTRS2011

A Bi-Modal Distribution of ALHA77307 Matrix Olivine: Evidence for Fine-Grained Mixing from Multiple Reservoirs in the CO Formation Zone

The CO 3.0 chondrite ALHA77307 is thought to be the least metamorphosed of all the CO chondrites [1]. As such, the fine-grained (<30 m) olivine found in its matrix is a valuable resource for investigating the CO formation environment since its compositions should be primary. In the CO matrix, we indeed find a wide range of major element compositions (Fa(0.5-71)). However, more importantly, we find that the olivines make up two compositionally distinct populations (Fa(0.5-5) and Fa(21-71)). Grains from both populations are found within an extremely close proximity and we see no obvious evidence of two distinct lithologies within our samples. Therefore, we conclude that the olivine grains found in the ALHA77307 matrix must have crystallized within two unique formation conditions and were later mixed at a very fine scale during the accretion epoch. Here, we propose a possible explanation based on Cr and Mn concentrations in the olivine.

Frank, D.↗
NASA NTRS2011

Stardust Interstellar Foils I1061N,1 and I1031N, 1: First Results from Automated Crater Searches and Future Analytical Possibilities

In addition to samples from comet 81P/Wild 2, NASA's Stardust mission may have returned the first samples of contemporary interstellar dust. The interstellar tray collected particles for 229 days during two exposures prior to the spacecraft encounter with Wild 2 and tracked the interstellar dust stream for all but 34 days of that time. In addition to aerogel capture cells, the tray contains Al foils that make up approx.15% of the total exposed collection surface . Interstellar dust fluxes are poorly constrained, but suggest that on the order of 12-15 particles may have impacted the total exposed foil area of 15,300 sq mm; 2/3 of these are estimated to be less than approx.1 micrometer in size . Examination of the interstellar foils to locate the small rare craters expected from these impacts is proceeding under the auspices of the Stardust Interstellar Preliminary Examination (ISPE) plan. Below we outline the automated high-resolution imaging protocol we have established for this work and report results obtained from two interstellar foils.

Zolensky, M. E.↗
NASA NTRS2011

Identification of Impact Craters in Foils from the Stardust Interstellar Dust Collector

The Stardust Interstellar Dust Collection tray provides the first opportunity for the direct laboratory-based measurement of contemporary interstellar dust. The total exposed surface of the tray was approximately 0.1 square meters, including 153 square centimeters of Al foil in addition to the silica aerogel tiles that are the primary collection medium. Preliminary examination of aerogel tiles has already revealed 16 tracks from particle impacts with an orientation consistent with an interstellar origin, and to date four of the particles associated with these tracks have a composition consistent with an extraterrestrial origin. Tentative identification of impact craters on three foil samples was also reported previously. Here we present the definitive identification of 20 impact craters on five foils.

Stroud, R. M.↗
NASA NTRS2011

Olivine and Pyroxene Compositions in Fine-Grained Chondritic Materials

Our analyses of the Wild-2 samples returned by the Stardust Mission have illuminated critical gaps in our understanding of related astromaterials. There is a very large database of olivine and low-calcium pyroxene compositions for coarse-grained components of chondrites, but a sparse database for anhydrous silicate matrix phases. In an accompanying figure, we present comparisons of Wild-2 olivine with the available chondrite matrix olivine major element data. We thus have begun a long-term project measuring minor as well as major element compositions for chondrite matrix and chondritic IDPs, and Wild 2 grains. Finally, we wish to re-investigate the changes to fine-grained olivine and low-Ca pyroxene composition with progressive thermal metamorphism. We have examined the LL3-4 chondrites which because of the Hayabusa Mission have become very interesting.

Zolensky, Michael E.↗
NASA NTRS2011

A New View on Interstellar Dust - High Fidelity Studies of Interstellar Dust Analogue Tracks in Stardust Flight Spare Aerogel

In 2000 and 2002 the Stardust Mission exposed aerogel collector panels for a total of about 200 days to the stream of interstellar grains sweeping through the solar system. The material was brought back to Earth in 2006. The goal of this work is the laboratory calibration of the collection process by shooting high speed [5 - 30km/s] interstellar dust (ISD) analogues onto Stardust aerogel flight spares. This enables an investigation into both the morphology of impact tracks as well as any structural and chemical modification of projectile and collector material. First results indicate a different ISD flux than previously assumed for the Stardust collection period.

Zolensky, Michael E.↗
NASA NTRS2011

FTIR Analysis of Aerogel Keystones from the Stardust Interstellar Dust Collector: Assessment of Terrestrial Organic Contamination and X-Ray Microprobe Beam Damage

The Stardust Interstellar Dust Collector (SIDC) was intended to capture and return contemporary interstellar dust. The approx.0.1 sq m collector was composed of aerogel tiles (85% of the collecting area) and aluminum foils and was exposed to the interstellar dust stream for a total exposure factor of 20 sq m day. The Stardust Interstellar Preliminary Examination (ISPE) is a consortium-based project to characterize the collection using nondestructive techniques. Sandford et al. recently assessed numerous potential sources of organic contaminants in the Stardust cometary collector. These contaminants could greatly complicate the analysis and interperetation of any organics associated with interstellar dust, particularly because signals from these particles are expected to be exceedingly small. Here, we present a summary of FTIR analyses of over 20 aerogel keystones, many of which contained candidates for interstellar dust.

Zolensky, M. E.↗
NASA NTRS2011

Four Interstellar Dust Candidates from the Stardust Interstellar Dust Collector

In January 2006, the Stardust sample return capsule returned to Earth bearing the first solid samples from a primitive solar system body, Comet 81P/Wild2, and a collector dedicated to the capture and return of contemporary interstellar dust. Both collectors were approx. 0.1 sq m in area and were composed of aerogel tiles (85% of the collecting area) and aluminum foils. The Stardust Interstellar Dust Collector (SIDC) was exposed to the interstellar dust stream for a total exposure factor of 20 sq m/day. The Stardust Interstellar Preliminary Examination (ISPE) is a consortium-based project to characterize the collection using nondestructive techniques. The goals and restrictions of the ISPE are described . A summary of analytical techniques is described.

Westphal, A. J.↗
NASA NTRS2010

Analysis of "Midnight" Tracks in the Stardust Interstellar Dust Collector: Possible Discovery of a Contemporary Interstellar Dust Grain

In January 2006, the Stardust sample return capsule returned to Earth bearing the first solid samples from a primitive solar system body, Comet 81P/Wild2, and a collector dedicated to the capture and return of contemporary interstellar dust. Both collectors were approximately 0.1m(exp 2) in area and were composed of aerogel tiles (85% of the collecting area) and aluminum foils. The Stardust Interstellar Dust Collector (SIDC) was exposed to the interstellar dust stream for a total exposure factor of 20 m(exp 2) day. The Stardust Interstellar Preliminary Examination (ISPE) is a three-year effort to characterize the collection using nondestructive techniques.

Westphal, A. J.↗
NASA NTRS2009

Carbon XANES Data from Six Aerogel Picokeystones Cut from the Top and Bottom Sides of the Stardust Comet Sample Tray

Great care and a large effort was made to minimize the amount of organic matter contained within the flight aerogel used to collect Comet 81P/Wild 2 samples. Even so, by the very nature of the production process and silica aerogel s affinity for volatile organics keeping silica aerogel free from organics is a monumental task. Silica aerogel from three production batches was flown on the Stardust sample return mission. All 3 types had layered densities varying from 5mg/ml to 50 mg/ml where the densest aerogel was farthest away from the collection area. A 2 step gelation process was used to make the flight aerogel and organics used in this process were tetraethylorthosilicate, ethanol and acetonitrile. Both ammonium hydroxide and nitric acid were also used in the aerogel production process. The flight aerogel was baked at JPL at 300 C for 72 hours, most of the baking was done at atmosphere but twice a day the oven was pumped to 10 torr for hour [1]. After the aerogel was baked it was stored in a nitrogen purged cabinet until flight time. One aerogel cell was located in the SRC away from any sample collection area as a witness to possible contamination from out gassing of the space craft, re-entry gases and any other organic encounter. This aerogel was aerogel used in the interstellar collection sample tray and is the least dense of the 3 batches of aerogel flown. Organics found in the witness tile include organics containing Si-CH3 bonds, amines and PAHS. Besides organic contamination, hot spots of calcium were reported in the flight aerogel. Carbonates have been detected in comet 81P/Wild2 samples . During preflight analyses, no technique was used to analyze for carbonates in aerogel. To determine if the carbonates found in 81P/Wild2 samples were from the comet, it is necessary to analyze the flight aerogel for carbonate as well as for organics.

Wirick, S.↗
NASA NTRS2008

Preliminary Examination of the Interstellar Collector of Stardust

The findings of the Stardust spacecraft mission returned to earth in January 2006 are discussed. The spacecraft returned two unprecedented and independent extraterrestrial samples: the first sample of a comet and the first samples of contemporary interstellar dust. An important lesson from the cometary Preliminary Examination (PE) was that the Stardust cometary samples in aerogel presented a technical challenge. Captured particles often separate into multiple fragments, intimately mix with aerogel and are typically buried hundreds of microns to millimeters deep in the aerogel collectors. The interstellar dust samples are likely much more challenging since they are expected to be orders of magnitudes smaller in mass, and their fluence is two orders of magnitude smaller than that of the cometary particles. The goal of the Stardust Interstellar Preliminary Examination (ISPE) is to answer several broad questions, including: which features in the interstellar collector aerogel were generated by hypervelocity impact and how much morphological and trajectory information may be gained?; how well resolved are the trajectories of probable interstellar particles from those of interplanetary origin?; and, by comparison to impacts by known particle dimensions in laboratory experiments, what was the mass distribution of the impacting particles? To answer these questions, and others, non-destructive, sequential, non-invasive analyses of interstellar dust candidates extracted from the Stardust interstellar tray will be performed. The total duration of the ISPE will be three years and will differ from the Stardust cometary PE in that data acquisition for the initial characterization stage will be prolonged and will continue simultaneously and parallel with data publications and release of the first samples for further investigation.

Westphal, A. J.↗