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Golden, J. L.

Publications and source records attributed to Golden, J. L..

The Komplast Experiment: Space Environmental Effects after 12 Years in LEO (and Counting)

The Komplast materials experiment was designed by the Khrunichev Space Center, together with other Russian scientific institutes, and has been carried out by Mission Control Moscow since 1998. The purpose is to study the effect of the low earth orbit (LEO) environment on exposed samples of various spacecraft materials. The Komplast experiment began with the launch of the first International Space Station (ISS) module on November 20, 1998. Two of eight experiment panels were retrieved during Russian extravehicular activity in February 2011 after 12 years of LEO exposure, and were subsequently returned to Earth by Space Shuttle "Discovery" on the STS-133/ULF-5 mission. The retrieved panels contained an experiment to detect micrometeoroid and orbital debris (MMOD) impacts, radiation sensors, a temperature sensor, several pieces of electrical cable, both carbon composite and adhesive-bonded samples, and many samples made from elastomeric and fluoroplastic materials. Our investigation is complete and a summary of the results obtained from this uniquely long-duration exposure experiment will be presented.

Shaevich, S. K.↗

The Komplast Experiment: Space Environmental Effects after 12 Years in LEO (and Counting)

The Komplast materials experiment was designed by the Khrunichev Space Center, together with other Russian scientific institutes, and has been carried out by Mission Control Moscow since 1998. The purpose is to study the effect of the low earth orbit (LEO) environment on exposed samples of various spacecraft materials. The Komplast experiment began with the launch of the first International Space Station (ISS) module on November 20, 1998. Two of eight experiment panels were retrieved during Russian extravehicular activity in February 2011 after 12 years of LEO exposure, and were subsequently returned to Earth by Space Shuttle "Discovery" on the STS-133/ULF-5 mission. The retrieved panels contained an experiment to detect micrometeoroid and orbital debris (MMOD) impacts, radiation sensors, a temperature sensor, several pieces of electrical cable, both carbon composite and adhesive-bonded samples, and many samples made from elastomeric and fluoroplastic materials. Our investigation is complete and a summary of the results obtained from this uniquely long-duration exposure experiment will be presented.

Golden, J. L.↗

Analysis of International Space Station Vehicle Materials Exposed on Materials International Space Station Experiment from 2001 to 2011

Since August 2001, the Materials on International Space Station Experiment (MISSE) has provided data on a variety of materials and spacecraft components, including samples chosen to provide sustaining engineering and life extension data for the International Space Station vehicle itself. This Technical Publication is by no means a complete set of MISSE data but does provide changes in solar absorptance, infrared emittance, and visual appearance due to atomic oxygen, ultraviolet radiation, and thermal cycling in vacuum. Conversion coatings, anodizes, thermal control coatings with organic and inorganic binders, multilayer insulation components, optical materials, and part markings are discussed.

Finckenor, M. M.↗

The Komplast Experiment: Space Environmental Effects after 12 Years in LEO (and Counting)

The Komplast materials experiment was designed by the Khrunichev State Research and Production Space Center, together with other Russian scientific institutes, and has been carried out by Mission Control Moscow since 18. Komplast panels fitted with material samples and sensors were located on the International Space Station (ISS) Functional Cargo Block (FGB) module exterior surface. Within the framework of this experiment, the purpose was to study the effect of the low earth orbit (LEO) environment on exposed samples of various materials. The panels were sent into orbit with the FGB when it launched on November 20, 1998. Panels #2 and #10 were retrieved during Russian extravehicular activity in February 2011 and sealed within cases to temporarily protect the samples from exposure to air until they could be studied on the ground. Panel #2 contained an experiment to detect micrometeoroid and orbital debris (MMOD) impacts, radiation and UV sensors, several pieces of electrical cable, and samples made from elastomeric and fluoroplastic materials. Panel #10 contained a temperature sensor, and both carbon composite and adhesive-bonded samples. A figure shows the location of panels #2 and #10 on the FGB module aft endcone. The panels were subsequently returned to Earth by Space Shuttle Discovery on the STS-133/ULF-5 mission after 12 years of LEO exposure and opened in an argon chamber at the Institute of Nuclear Physics at Moscow State University in July 2011. Based on the results of analyzing the readings from sensors located on Komplast panels and in studying material samples from the panels, the comprehensive effect of spaceflight factors on the FGB (at the locations of Panels #2 and #10) was evaluated. Total solar exposure was determined to be 960 +/- 200 kJ/square cm or 21,000 equivalent solar hours. Because of location of these two panels and the ISS flight attitude, atomic oxygen (AO) fluence was relatively low for such a long duration exposure, approximately 1.5x10 (exp 21) O atoms/sq. cm. Most of the AO fluence occurred during the early phase of ISS assembly. Temperatures ranged from a maximum of 107 C to a minimum of -80 C. The MMOD environment was determined, as is shown. Interestingly, the distribution of craters and low-velocity impact particles observed in the 5-50 micron size range was approx 2-3 orders of magnitude higher than that predicted by the ORDEM2000 model of natural and artificial origin microparticles in the ISS orbit. Contamination observations were also made, through the evaluation of optical properties on thermal control coatings and by the examination of visible deposits located near several samples on the panels, primarily from elastomeric samples. These elastomer samples were extensively investigated for their physical property changes and sealing capability. In addition, 16 samples of adhesive-bonded joints using three types of epoxy adhesive were evaluated studying fracture toughness, failure surface, and adhesive volume properties. Both rubber and adhesive-bonded specimens also underwent additional (post-flight) ground-based exposures to simulate a total 30 years in LEO prior to their evaluation. Overall, results indicate that space environmental effects will not adversely impact the service life of the FGB through 2028. Our investigation is complete and a summary of the results obtained from this uniquely long-duration exposure experiment will be presented.

Shaevich, S. K.↗

Analysis of Microcrafters in Materials Specimens after Long-Term Exposure on ISS Surface

The "Komplast" experiment has been carried out on the ISS by the Khrunichev Space Center jointly with other Russian scientific centers since 1998. The experiment incorporates the "Komplast" cartridges on the FGB exterior, which are fitted with materials specimens and sensors. The cartridges were sent into orbit together with FGB on 20 November 1998. In March 2011, two of the cartridges were taken back from the ISS by the "Discovery" American space shuttle after being exposed in the open space for 12 years. In the framework of this experiment the subject of analysis is the effect of the space environment on the exposed specimens of various materials. This report covers the analysis results of the surface morphology of various materials taken from the "Komplast" cartridges exposed to hits of micrometeors and micronic particles of space debris. Analysis is made of microcraters of 5 to 250 mcm in specimens of polished metals and silicone comprised in the sensor for micrometeoric particles. The report represents optic and scanning electron microscope images of craters formed in the specimens by high-velocity and low-velocity particles impacting the surface. By virtue of the electronic microscope, data on composition of the substance in the craters and of the substance of the low-velocity particles are obtained. The data make it possible to differentiate the particles as the natural-origin particles or anthropogenic-origin space debris particles. Distribution of craters and low-velocity particles in the size range of 5 to 50 mcm is obtained. The data are compared with the existing models of fluxes of natural-origin and artificial-origin microparticles on the ISS orbit. Inhomogeneous particles of complicated configuration are discovered on the surface of the analyzed specimens, whose origin are not uniquely determined and are to be the subject of further study.

Shaevich, S. K.↗

A Study of Micro Craters in Material Samples after Long Duration Exposure on ISS Komplast Panels

The Komplast materials experiment was designed by the Khrunichev State Research and Production Space Center, together with other Russian scientific institutes, and has been carried out by Mission Control Moscow since 1998. Komplast panels fitted with material samples and sensors were located on the International Space Station (ISS) Functional Cargo Block (FGB) module exterior surface. Within the framework of this experiment, the purpose was to study the effect of the low earth orbit (LEO) environment on exposed samples of various materials. The panels were sent into orbit with the FGB when it launched on November 20, 1998. .

Shaevich, S. K.↗

Examination of Surface Residuals Obtained During Re-Lubrication of the International Space Station (ISS) Solar Alpha Rotary Joint (SARJ)

The starboard SARJ mechanism on the ISS suffered a premature lubrication failure, resulting in widespread loss of the nitride case layer on its 10.3 meter circumference, 15-5PH steel race ring [1, 2]. To restore functionality, vacuum-stable grease was applied on-orbit, first to the port SARJ mechanism to save it from the damage suffered by the starboard mechanism. After 3 years of greased operation, telemetry indicated that the port mechanism required relubrication, so part of that process included sampling each of the three race ring surfaces to evaluate any wear debris recovered and the state of the originally applied grease. Extensive microscopic examination was conducted, which directed subsequent microanalysis of particulate. Since the SARJ mechanism operates in the vacuum of space, a sampling method and tool had to be developed for use by astronauts while working in the extravehicular mobility unit (EMU). The sampling tool developed was a cotton terry-cloth mitt for the EMU glove, with samples taken by swiping each of the three port SARJ race-ring surfaces. The sample mitts for each surface were folded inward after sampling to preserve sample integrity, for return and ground analysis. The sample mitt for what is termed the outer canted surface of the SARJ race-ring is shown in Figure 1. Figure 1 also demonstrates how increasing levels of magnification were used to survey the contamination removed in sampling, specifically looking for signs of wear debris or other features which could be further evaluated using Scanning Electron Microscopy (SEM) methods. The most surprising overall result at this point in the analysis was the relatively small amounts of grease recovered during sampling. It is clear that the mechanism was not operating with surplus lubricant. Obviously, evidence of molybdenum disulfide (MoS2), a major component in the grease applied, was prevalent in the analysis conducted. But a small amount of mechanism wear debris was observed. Figure 2 shows an example of a region of concentrated wear debris. Although some MoS2 is observed, most of the contaminant in this location is nitrided 15-5PH steel, as verified by the associated chemical analysis. High oxygen content was also observed which, when associated with the apparent friable nature of the steel material, suggests that this contaminant could be quite old, perhaps even associated with the mechanism s original manufacture and acceptance testing. Additional microscopic

Martinez, J. E.↗

External Surface Changes Observed on the International Space Station (ISS) Through 2010

Some worse-than-expected materials degradation effects have been observed, but none have created any operational issues and some hardware (as with the anodized aluminum labels) appear to be recovering. Inadvertent materials substitutions have been observed, but none have created any operational issues. Hardware handling contamination effects have been observed, and although none have created operational issues, there is clearly room for improvement in this regard. Even with robust materials selections, space environmental effects will be observed. Be cautious when interpreting on-orbit photography, as lighting conditions and the space environment affect imaging.

Golden, J. L.↗

Effects of Space Environments: Techniques and Lessons from Selected Flight Experiments

Data describing long-term materials performance under exposure to space environments has accumulated gradually over the past four decades. The authors present here selected results from several previous flight experiments and operational spacecraft, and a few examples from a current flight experiment. As examples of environmental effects on materials, analysis of Gortex samples from the Passive Optical Sample Assembly II (POSA II) experiment on the MIR-Shuttle docking module will be described. Results from a previous evaluation of radiation on silverized Teflon from over ten individual satellites will be summarized. Several examples of contamination effects on materials properties will be presented. These include outgassing of solar arrays onto nearby surfaces of the POSA I experiment and contamination of certain surfaces of the Long Duration Exposure Facility (LDEF). Results from experiments with silicone contamination on satellites in geosynchronous orbit will be compared with measurements on the Solar Maximum satellite and the LDEF. A number of techniques are being attempted to extend the range of exposure conditions present on selected experiments. Use of focusing concentrators on the Effect of Space Environments on Materials (ESEM), POSA, and Materials International Space Station Experiment (MISSE) will be described. A technique for obtaining time-resolved data from a passive materials experiment will be described. The status of an on-going materials flight experiment, MISSE, will be reported. Finally, the authors will draw some conclusions about the current state of knowledge relating to materials chosen for spacecraft applications. Understanding of degradation mechanisms, state of predictive models, and the need to strengthen model inputs will be discussed.

Golden, J. L.↗