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Graf, Neil A.

Publications and source records attributed to Graf, Neil A..

Subscale Composite Liquid Oxygen Tank Testing

Lockheed Martin Space Systems Company recently completed a two-year fabrication and test program on subscale composite liquid oxygen (LO2) tanks. The goals of this program included the development of fabrication and inspection techniques, cryogenic acceptance testing of composite articles, and demonstrating oxygen compatibility under launch vibration loads. Two subscale diameter test bottles were fabricated using a proprietary Lockheed Martin material, known as LM21C03. The bottles were then inspected using an array of NDE techniques and then put through a cryogenic acceptance test program at Lockheed Martin. A NASA/Lockheed Martin test team then subjected a composite bottle to testing at an X-33 vibration profile for 15 minutes at use pressure. The tests were run at various LO2 fill levels, with and without intentionally added debris. All tests were successful in that the composite bottle showed no signs of ignition or combustion as a result of the vibration testing. This test program is an important bridge between coupon-level and subcomponent LO2 compatibility tests and full-scale composite LO2 tank use.

Graf, Neil A.↗

Oxygen Compatibility Testing of Composite Materials

The development of polymer composite liquid oxygen LO2 tanks is a critical step in creating the next generation of launch vehicles. Future launch vehicles need to minimize the gross liftoff weight (GLOW), which is possible due to the 25%-40% reduction in weight that composite materials could provide over current aluminum technology. Although a composite LO2 tank makes these weight savings feasible, composite materials have not historically been viewed as "LO2 compatible." To be considered LO2 compatible, materials must be selected that will resist any type of detrimental, combustible reaction when exposed to usage environments. This is traditionally evaluated using a standard set of tests. However, materials that do not pass the standard tests can be shown to be safe for a particular application. This paper documents the approach and results of a joint NASA/Lockheed Martin program to select and verify LO2 compatible composite materials for liquid oxygen fuel tanks. The test approach developed included tests such as mechanical impact, particle impact, puncture, electrostatic discharge, friction, and pyrotechnic shock. These tests showed that composite liquid oxygen tanks are indeed feasible for future launch vehicles.

Graf, Neil A.↗

Adhesive Bonding Characterization of Composite Joints for Cryogenic Usage

The development of polymer composite cryogenic tanks is a critical step in creating the next generation of launch vehicles. Future reusable launch vehicles need to minimize the gross liftoff weight (GLOW). This weight reduction is possible due to the large reduction in weight that composite materials can provide over current aluminum technology. In addition to composite technology, adhesively bonded joints potentially have several benefits over mechanically fastened joints, such as weight savings and cryogenic fluid containment. Adhesively bonded joints may be used in several areas of these cryogenic tanks, such as in lobe-to-lobe joints (in a multi-lobe concept), skirt-to-tank joint, strut-to-tank joint, and for attaching stringers and ring frames. The bonds, and the tanks themselves, must be able to withstand liquid cryogenic fuel temperatures that they contain. However, the use of adhesively bonded composite joints at liquid oxygen and hydrogen temperatures is largely unknown and must be characterized. Lockheed Martin Space Systems Company, Michoud Operations performed coupon-level tests to determine effects of material selection, cure process parameters, substrate surface preparation, and other factors on the strength of these composite joints at cryogenic temperatures. This led to the selection of a material and process that would be suitable for a cryogenic tank. KEY WORDS: Composites, Adhesive Bonding, Cryogenics

Graf, Neil A.↗