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Grenoble, Ray W.

Publications and source records attributed to Grenoble, Ray W..

Recertification and Equivalency Test Results for IM7/8552-1 Following Extended Freezer Storage

In 2015, the Composites for Exploration Upper Stage (CEUS) Project established an equivalency test program to reduce the scope of laminate coupon tests within the project. The material selected was IM7/8552-1, a variant of the IM7/8552 prepreg used to populate a National Center for Advanced Materials Performance (NCAMP) database. The CEUS successor program, Composites Technology for Exploration (CTE), kicked off in 2017 with the remaining CEUS prepreg planned for use. The IM7/8552-1 prepreg was recertified through an in-house defined set of pass/fail criteria then evaluated for equivalency to the NCAMP database. Over the course of recertification and equivalency panel fabrication, the time of freezer storage ranged from 19 - 22 months. Panels for recertification and equivalency tests were fiber placed at NASA Marshall Space Flight Center (MSFC) and NASA Langley Research Center (LARC).

carbon fiber/epoxy

Material Property Characterization of AS4/VRM-34 Textile Laminates

Several material properties (modulus, strengths, and fracture toughness) of a textile composite have been evaluated to provide input data to analytical models of Pultruded Rod Stiffened Efficient Unitized Structure (PRSEUS). The material system is based on warp-knitted preforms of AS4 carbon fibers and VRM-34 epoxy resin, which have been processed via resin infusion and oven curing. Tensile, compressive, shear, and fracture toughness properties have been measured at ambient and elevated temperatures. All specimens were tested in as-fabricated (dry) condition. Specimens were tested with and without through-thickness stitching.

Grenoble, Ray W.

Notched Strength Allowables and Inplane Shear Strength of AS4/VRM-34 Textile Laminates

Notched and unnotched strength allowables were developed for a textile composite to provide input data to analytical structural models based on the Pultruded Rod Stiffened Efficient Unitized Structure (PRSEUS) concept. Filled-hole tensile strength, filled-hole compressive strength, and inplane shear strength along stitch lines have been measured. The material system evaluated in this study is based on warp-knitted preforms of AS4 carbon fibers and VRM-34 epoxy resin, which have been processed via resin infusion and oven curing. All specimens were tested in as-fabricated (dry) condition. Filled-hole strengths were evaluated with and without through-thickness stitching. The effects of scaling on filled-hole tensile strength were evaluated by testing specimens in two widths, but with identical width / hole-diameter ratios. Inplane shear specimens were stitched in two configurations, and two specimen thicknesses were tested for each stitch configuration.

Grenoble, Ray W.

Structural Integrity Testing Method for PRSEUS Rod-Wrap Stringer Design

NASA Langley Research Center and The Boeing Company are developing an innovative composite structural concept, called PRSEUS, for the flat center section of a future environmentally friendly hybrid wing body (HWB) aircraft. The PRSEUS (Pultruded Rod Stitched Efficient Unitized Structure) concept uses dry textile preforms for the skins, frames, and stiffener webs. The highly loaded stiffeners are made from precured unidirectional carbon/epoxy rods and dry fiber preforms. The rods are wrapped with the dry fiber preforms and a resin infusion process is used to form the rod-wrap stiffeners. The structural integrity of the rod-wrap interface is critical for maintaining the panel s high strength and bending rigidity. No standard testing method exists for testing the strength of the rod-wrap bondline. Recently, Boeing proposed a rod push-out testing method and conducted some preliminary tests using this method. This paper details an analytical study of the rod-wrap bondline. The rod-wrap interface is modeled as a cohesive zone for studying the initiation and growth of interfacial debonding during push-out testing. Based on the correlations of analysis results and Boeing s test data, the adequacy of the rod-wrap testing method is evaluated, and potential approaches for improvement of the test method are proposed.

Wang, John T.

Hydrogen Permeability of Polymer Matrix Composites at Cryogenic Temperatures

This paper presents experimental methods and results of an ongoing study of the correlation between damage state and hydrogen gas permeability of laminated composite materials under mechanical strains and thermal loads. A specimen made from IM-7/977-2 composite material has been mechanically cycled at room temperature to induce microcrack damage. Crack density and tensile modulus were observed as functions of number of cycles. Damage development was found to occur most quickly in the off-axis plies near the outside of the laminate. Permeability measurements were made after 170,000 cycles and 430,000 cycles. Leak rate was found to depend on applied mechanical strain, crack density, and test temperature.

Grenoble, Ray W.

Thermal/Mechanical Durability of Polymer-Matrix Composites in Cryogenic Environments

In order to increase the reliability of the next generation of space transportation systems, the mechanical behavior of polymeric-matrix composite (PMC) materials at cryogenic temperatures must be investigated. This paper presents experimental data on the residual mechanical properties of a carbon fiber polymeric composite, IM7/PETI-5 as a function of temperature and aging. Tension modulus and strength were measured at room temperature, -196 C, and -269 C on five different specimens ply lay-ups. Specimens were preconditioned with one set of coupons being isothermally aged for 576 hours at -184 C, in an unloaded state. Another set of corresponding coupons were mounted in constant strain fixtures such that a constant uniaxial strain was applied to the specimens for 576 hours at -184 C. A third set was mechanically cycled in tension at -184 C. The measured properties indicated that temperature, aging, and loading mode can all have significant influence on performance. Moreover, this influence is a strong function of laminate stacking sequence. Thermal-stress calculations based on lamination theory predicted that the transverse tensile ply stresses could be quite high for cryogenic test temperatures. Microscopic examination of the surface morphology showed evidence of degradation along the exposed edges of the material because of aging at cryogenic temperatures. ________________

Gates, Thomas S.

Hybrid IR-Gas Heater for Automated Tow Placement

A hybrid infrared-hot gas heat source has been developed and tested for the NASA Langley Tow Placement Facility. The IR heat source provides supplemental heat to the nip region. The additional heat is intended to reduce the need for conduction heating by the compaction roller, which causes (he roller to stick to the panel surface. Initial bench scale testing was performed to identify the most effective means of focusing IR energy into the nip region. A compact lamp and reflector that placed the lamp as close to the nip point as possible was found to deliver the highest heat flux in the nip region. A prototype heater was installed on the NASA Langley tow placement robot. Panels placed with a 400 C (sticking) compaction roller gave DCB initiation toughness numbers comparable to those reported for autoclave processed panels but were found to have unexpectedly high void contents. Placement with compaction roller temperatures that prevented roller sticking resulted in mode I fracture toughness approximately 70% that reported for autoclave processed panels. The variability in strength among specimens placed with reduced roller temperature was found to be greatly reduced, which implies that use of supplemental nip point heat may improve the robustness of the tow placement process. Use of the IR heat source permitted placement with a compaction roller temperature that would have resulted in negligible interfacial strength with the hot gas torch alone. The roller temperature reductions eliminated the need for the robot operator to attend placement operations.

Grenoble, Ray W.