Method for fabricating a mass spectrometer inlet leak
A method of fabricating an inlet leak for measuring chemically reactive gases is proposed. The method involves the steps of preparing a selected internal surface of a high melting point metal tubing for sealing to a glass tubing. A portion of the glass tubing is inserted into the prepared portion of the metal tubing, the glass tubing having an outer diameter substantially the same as the inner diameter of the metal tubing. The inserted glass tubing is sealed to the internal surface of the metal tubing; the glass tubing is drawn under a magnifying device to reduce the entire interior diameter thereof to substantially two microns; and an end portion of the drawing glass tubing is broken away.
Harris, R. F.↗