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Naumann, Robert J.

Publications and source records attributed to Naumann, Robert J..

At least 19 records

Polydiacetylene Films Prepared in Microgravity

A diffusive/kinetic rate equation was developed for the growth of polydiacetylene films from solution and compared with a microgravity experiment. The model takes into account both the kinetics of thin film growth and the diffusive transport limitations inherent to microgravity. In order to apply this model, measurements of the density and the ultraviolet extinction coefficient of the films, as well as of the diffusion coefficient of the monomer/solvent system, were made. The thin films grown in microgravity were predicted by the model to grow to a thickness of 0.148 micron, versus 0.150 micron for the ground control films. The flight films grew to 0.102 micron.

Carswell, William E.

Spacelab Science Results Study: External Observations - Volume 1

Some of the 36 Spacelab missions were more or less dedicated to specific scientific disciplines, while other carried a eclectic mixture of experiments ranging from astrophysics to life sciences. However, the experiments can be logically classified into two general categories; those that make use of the Shuttle as an observing platform for external phenomena (including those which use the Shuttle in an interactive mode) and those which use the Shuttle as a microgravity laboratory. This first volume of this Spacelab Science Results study will be devoted to experiments of the first category. The disciplines included are Astrophysics, Solar Physics, Space Plasma Physics, Atmospheric Sciences, and Earth Sciences. Because of the large number of microgravity investigations, Volume 2 will be devoted to Microgravity Sciences, which includes Fluid Physics, Combustion Science, Materials Science, and Biotechnology, and Volume 3 will be devoted to Space Life Sciences, which studies the response and adaptability of living organisms to the microgravity environment.

Naumann, Robert J.

Spacelab Science Results Study: Executive Summary

Beginning with OSTA-1 in November 1981, and ending with Neurolab in March 1998, thirty-six shuttle missions are considered Spacelab missions because they carried various Spacelab components such as the Spacelab module, the pallet, the Instrument Pointing System (IPS), or the MPESS. The experiments carried out during these flights included astrophysics, solar physics, plasma physics, atmospheric science, Earth observations, and a wide range of microgravity experiments in life sciences, biotechnology, materials science, and fluid physics which includes combustion and critical point phenomena. In all, some 764 experiments were conducted by investigators from the United States, Europe, and Japan. These experiments resulted in several thousand papers published In refereed journals, and thousands more in conference proceedings, chapters in books, and other publications. The purpose of this Spacelab Science Results Study is to document the contributions made in each of the major research areas by giving a brief synopsis of the more significant experiments and an extensive list of the publications that were produced. We have also endeavored to show how these results impacted the existing body of knowledge, where they have spawned new fields, and, if appropriate, where the knowledge they produced has been applied.

Naumann, Robert J.

Spacelab Science Results Study: Microgravity Science - Volume 3

Beginning with OSTA-1 in November 1981, and ending with Neurolab in March 1998, thirty-six shuttle missions are considered Spacelab missions because they carried various Spacelab components such as the Spacelab module, the pallet, the Instrument Pointing System (IPS), or the MPESS. The experiments carried out during these flights included astrophysics, solar physics, plasma physics, atmospheric science, Earth observations, and a wide range of microgravity experiments in life sciences, biotechnology, materials science, and fluid physics which includes combustion and critical point phenomena. In all, some 764 experiments were conducted by investigators from the United States, Europe, and Japan. These experiments resulted in several thousand papers published in refereed journals, and thousands more in conference proceedings, chapters in books, and other publications. The purpose of this Spacelab Science Results Study is to document the contributions made in each of the major research areas by giving a brief synopsis of the more significant experiments and an extensive list of the publications that were produced. We have also endeavored to show how these results impacted the existing body of knowledge, where they have spawned new fields, and, if appropriate, where the knowledge they produced has been applied.

Naumann, Robert J.

Spacelab Science Results Study: Microgravity Science - Volume 2

Beginning with OSTA-1 in November 1981, and ending with Neurolab n March 1998, thirty-six shuttle missions are considered Spacelab missions because they carried various Spacelab components such as the Spacelab module, the pallet, the Instrument Pointing System (IPS), or the MPESS (Mission Peculiar Experiment Support Structure). The experiments carried out during these flights included astrophysics, solar physics, plasma physics, atmospheric science, Earth observations, and a wide range of microgravity experiments in life sciences, biotechnology, materials science, and fluid physics which includes combustion and critical point phenomena. In all, some 764 experiments were conducted by investigators from the United States, Europe, and Japan. These experiments resulted in several thousand papers published in refereed journals, and thousands more in conference proceedings, chapters in books, and other publications. The purpose of this Spacelab Science Results Study is to document the contributions made in each of the major research areas by giving a brief synopsis of the more significant experiments and an extensive list of the publications that were produced. We have also endeavored to show how these results impacted the existing body of knowledge, where they have spawned new fields, and, if appropriate, where the knowledge they produced has been applied.

Naumann, Robert J.

Analytical Model For Fluid Dynamics In A Microgravity Environment

Report presents analytical approximation methodology for providing coupled fluid-flow, heat, and mass-transfer equations in microgravity environment. Experimental engineering estimates accurate to within factor of 2 made quickly and easily, eliminating need for time-consuming and costly numerical modeling. Any proposed experiment reviewed to see how it would perform in microgravity environment. Model applied in commercial setting for preliminary design of low-Grashoff/Rayleigh-number experiments.

Naumann, Robert J.

USML-1 Glovebox experiments

This report covers the development of and results from three experiments that were flown in the Materials Science Glovebox on USML-1: Marangoni convection in Closed Containers (MCCC), Double Float Zone (DFZ), and Fiber Pulling in Microgravity (FPM). The Glovebox provided a convenient, low cost method for doing simple 'try and see' experiments that could test new concepts or elucidate microgravity phenomena. Since the Glovebox provided essentially one (or possibly two levels of confinement, many of the stringent verification and test requirements on the experiment apparatus could be relaxed and a streamlined test and verification plan for flight qualification could be implemented. Furthermore, the experiments were contained in their own carrying cases whose external configurations could be identified early in the integration sequence for stowage considerations while delivery of the actual experiment apparatus could be postponed until only a few months before flight. This minimized the time fluids must be contained and reduced the possibility of corrosive reactions that could ruin the experiment. In many respects, this exercise was as much about developing a simpler, cheaper way of doing crew-assisted science as it was about the actual scientific accomplishments of the individual experiments. The Marangoni Convection in Closed Containers experiment was designed to study the effects of a void space in a simulated Bridgman crystal growth configuration and to determine if surface tension driven convective flows that may result from thermal gradients along any free surfaces could affect the solidification process. The Fiber Pulling in Microgravity experiment sought to separate the role of gravity drainage from capillarity effects in the break-up of slender cylindrical liquid columns. The Stability of a Double Float Zone experiment explored the feasibility of a quasi-containerless process in which a solidifying material is suspended by two liquid bridges of its own melt.

Naumann, Robert J.

Estimates of effects of residual acceleration on USML-1 experiments

The purpose of this study effort was to develop analytical models to describe the effects of residual accelerations on the experiments to be carried on the first U.S. Microgravity Lab mission (USML-1) and to test the accuracy of these models by comparing the pre-flight predicted effects with the post-flight measured effects. After surveying the experiments to be performed on USML-1, it became evident that the anticipated residual accelerations during the USML-1 mission were well below the threshold for most of the primary experiments and all of the secondary (Glovebox) experiments and that the only set of experiments that could provide quantifiable effects, and thus provide a definitive test of the analytical models, were the three melt growth experiments using the Bridgman-Stockbarger type Crystal Growth Furnace (CGF). This class of experiments is by far the most sensitive to low level quasi-steady accelerations that are unavoidable on space craft operating in low earth orbit. Because of this, they have been the drivers for the acceleration requirements imposed on the Space Station. Therefore, it is appropriate that the models on which these requirements are based are tested experimentally. Also, since solidification proceeds directionally over a long period of time, the solidified ingot provides a more or less continuous record of the effects from acceleration disturbances.

Naumann, Robert J.

Passive Vibration Isolator For Experiments

Passive isolator reduces natural vibrational frequency of platform to less than 1 Hz - well below frequencies of vibration induced by human activity. Biological, crystal-growth, and other experiments mounted on platform protected against disturbances by technicians working in vicinity. Designed for use in microgravitational environment of spacecraft. Modified version designed for use on Earth by including components counteracting steady normal Earth gravitation. Consumes no electrical power, simple, and inexpensive.

Naumann, Robert J.

Analytical estimates of radial segregation in Bridgman growth from low-level steady and periodic accelerations

Approximate analytical solutions are developed that are mathematically tractable but provide the elements of CFD models for estimating convective flows subjected to low-level accelerations. The estimates are applicable to dilute systems that have horizontal temperature gradients in the vertical Bridgman configuration. The Navier-Stokes momentum equation is solved in 1D and subsequently in 2D by the first-order perturbation method. The analysis used is the case of plane-front solidification of a dilute system in the vertical thermally stable configuration. The model is found to predict the degree of radial segregation within a factor of two for a range of material and processing parameters. The method provides detailed information on the effects of processing on solute distribution in the grown crystal which are of interest in the orbital experiments emphasizing the control of radial segregation.

Naumann, Robert J.

Preliminary results from three USML-1 Glovebox experiments

Three simple experiments, namely, Marangoni convection in closed containers (MCCC), fiber pulling in microgravity, and stability of a double float zone are described which were conducted during the U.S. Microgravity Laboratory mission (USML) in July 1992. Results show that, in the MCCC experiment, there was no evidence of partial wetting between the liquid and the walls either in the wetting or nonwetting configuration. In the nonwetting system, the void formed a hemispherical bubble that remained pinned to the walls with considerable contact line resistance. Significant differences were observed in the ability to pull liquid strings in low gravity in those materials which readily form liquid strands in normal gravity and do not necessarily form strands in reduced gravity. The double float zone configuration appeared to be quite stable in both cylindrical and sheet form.

Naumann, Robert J.

Passive Accelerometer

Motion of ball in liquid indicates acceleration. Passive accelerometer measures small accelerations along cylindrical axis. Principle of operation based on Stokes' law. Provides accurate measurements of small quasi-steady accelerations. Additional advantage, automatically integrates out unwanted higher-frequency components of acceleration.

Naumann, Robert J.

Hanging drop crystal growth apparatus

This invention relates generally to control systems for controlling crystal growth, and more particularly to such a system which uses a beam of light refracted by the fluid in which crystals are growing to detect concentration of solutes in the liquid. In a hanging drop apparatus, a laser beam is directed onto drop which refracts the laser light into primary and secondary bows, respectively, which in turn fall upon linear diode detector arrays. As concentration of solutes in drop increases due to solvent removal, these bows move farther apart on the arrays, with the relative separation being detected by arrays and used by a computer to adjust solvent vapor transport from the drop. A forward scattering detector is used to detect crystal nucleation in drop, and a humidity detector is used, in one embodiment, to detect relative humidity in the enclosure wherein drop is suspended. The novelty of this invention lies in utilizing angular variance of light refracted from drop to infer, by a computer algorithm, concentration of solutes therein. Additional novelty is believed to lie in using a forward scattering detector to detect nucleating crystallites in drop.

Naumann, Robert J.

Desirable limits of accelerative forces in a space-based materials processing facility

There are three categories of accelerations to be encountered on orbiting spacecraft: (1) quasi-steady accelerations, caused by atmospheric drag or by gravity gradients, 10(exp -6) to 10(exp -7) g sub o; (2) transient accelerations, caused by movements of the astronauts, mass translocations, landing and departure of other spacecraft, etc.; and (3) oscillary accelerations, caused by running machinery (fans, pumps, generators). Steady accelerations cause continuing displacements; transients cause time-limited displacements. The important aspect is the area under the acceleration curve, measured over a certain time interval. Note that this quantity is not equivalent to a velocity because of friction effects. Transient motions are probably less important than steady accelerations because they only produce constant displacements. If the accelerative forces were not equal and opposite, the displacement would increase with time. A steady acceleration will produce an increasing velocity of a particle, but eventually an equilibrium value will be reached where drag and acceleration forces are equal. From then on, the velocity will remain constant, and the displacement will increase linearly with time.

Naumann, Robert J.

Prospects for a contamination-free ultravacuum facility in low-earth orbit

The old concept of using the wake of a spacecraft to obtain an ultrahigh vacuum is revisited. A wakeshield can be configured so that a surface of interest does not subtend any walls that could become contaminated, thus it should be possible to achieve a contamination-free, ultrahigh vacuum capability with infinite pumping speed even in the presence of high heat loads and moderate gas loads. This papar analyzes the conceptual design for a Space Ultravacuum Research Facility (SURF), both in a shuttle-attached mode and as a free flyer. It is shown that even in the shuttle-attached mode, it should be possible to obtain vacuum levels equivalent to 10 to the -9th to 10 to the -10th Torr with O and N2 as the primary constituents. As a free flyer the SURF will be limited primarily by the gas load from the process being performed. For chemical beam epitaxy it is shown that equivalent vacuum levels of 10 to the -14th Torr should be possible at 300 km.

Naumann, Robert J.

Liquid encapsulated float zone process and apparatus

The process and apparatus for growing crystals using float zone techniques are described. A rod of crystalline materials is disposed in a cylindrical container, leaving a space between the rod and container walls. This space is filled with an encapsulant, selected to have a slightly lower melting point than the crystalline material. The rod is secured to a container end cap at one end and to a shaft at its other end. A piston slides over the rod and provides pressure to prevent loss of volatile components upon melting of the rod. Prior to melting the rod the container is first heated to melt the encapsulant, with any off-gas from this step being vented to a cavity behind the piston. The piston moves slightly forward owing to volume change upon melting of the encapsulant, and the vent passageway is closed. The container is then moved longitudinally through a heated zone to progressively melt sections of the rod as in conventional float zone processes. The float zone technique may be used in the microgravity environment of space.

Naumann, Robert J.

Analysis of the performance of the space ultravacuum research facility in attached and free-flyer mode

The old concept of using the wake of a spacecraft to obtain an ultrahigh vacuum is revisited with a somewhat different emphasis. Since it is possible to configure a wake shield so that a surface of interest does not subtend any walls that could become contaminated, it appears that it should be possible to achieve a contamination-free, ultrahigh vacuum capability with infinite pumping speed even in the presence of high heat loads and moderate gas loads. With the new interest in developing thin films with precision controlled synthetic microstructures such as superlattices, mixed metal oxide high temperature superconductors, rare-earth magneto-optical devices, and nano-crystalline alloys, the ability to work with a variety of different materials without cross contamination should be of significance. This paper analyzes the performance of the conceptual design for a Space Ultravacuum Research Facility (SURF), both in a Shuttle-attached mode and as a free-flyer. It is shown that even in the Shuttle-attached mode, it should be possible to obtain vacuum levels equivalent to 10 to the -10 Torr with O and N2 as the primary constituents. This should be sufficient to demonstrate the feasibility of the concept, particularly the infinite pumping speed and virtual elimination of contamination aspects. As a free-flyer the SURF will be limited primarily by the gas load associated with the process being performed. For chemical beam epitaxy (CBE) it is shown that equivalent vacuum levels of 10 to the -14 Torr should be possible at 300 km.

Naumann, Robert J.

Space ultra-vacuum facility and method of operation

A wake shield space processing facility (10) for maintaining ultra-high levels of vacuum is described. The wake shield (12) is a truncated hemispherical section having a convex side (14) and a concave side (24). Material samples (68) to be processed are located on the convex side of the shield, which faces in the wake direction in operation in orbit. Necessary processing fixtures (20) and (22) are also located on the convex side. Support equipment including power supplies (40, 42), CMG package (46) and electronic control package (44) are located on the convex side (24) of the shield facing the ram direction. Prior to operation in orbit the wake shield is oriented in reverse with the convex side facing the ram direction to provide cleaning by exposure to ambient atomic oxygen. The shield is then baked-out by being pointed directed at the sun to obtain heating for a suitable period.

Naumann, Robert J.