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Reiss, Donald A.

Publications and source records attributed to Reiss, Donald A..

Gas-Liquid Separation Strategies in Microgravity Environment

Bubble entrainment in liquids represents a serious problem in the microgravity environment. Whenever bubbles are entrained in a liquid,they tend to remain stationary in the liquid bulk in the absence of any external forcing. This is due to the reduction or complete absence of the buoyancy force in the microgravity environment, Thus the buoyancy force can not the be exploited to place the bubbles at the top of the liquid volume as in Ig(sub o) conditions. This situation represents a serious drawback in many space based engineering and scientific applications. We have demonstrated in a series of low gravity experiments conducted during parabolic flight on board aircraft that bubbles can be controlled in such a manner as to increase,the probability of their expulsion from a liquid bulk. In these tests the liquid'bulk was made either to be contained within, or to flow through specially designed containers using capillary force alone. Such containers appear to facilitate bubble removal, from the liquid bulk. Different successful liquid flow configurations will be discussed and the efficacy of the resulting bubble expulsion mechanisms will be demonstrated.

Antar, Basil N.

Mir Glovebox Facility

The Glovebox Facility on Mir was developed by the Marshall Space Flight Center for use on the space shuttle middeck and modified slightly for use on the Mir Space Station. Its design is based on a similar facility provided by the European Space Agency for use on Spacelab and flown on the USML-I and 2 missions. Its purpose is to provide a work space for experiments which is isolated from the manned environment while allowing a high degree of access to the experiment apparatus. It also provides experiment power, lighting, and data acquisition. This facility has successfully supported 7 experiments representing the fluid physics and combustion disciplines during NASA increments 2 - 5. During over 400 hours of operation, only 3 minor facility anomalies were encountered, none of which prevented science operations or resulted in hazardous conditions. No in-flight maintenance has been required through increment 5. Crew comments have been generally favorable, stressing the usefulness, reliability and ease of use of the facility. The success of the glovebox to date demonstrates the value of this type of multi-use facility in a space station environment.

Kroes, Roger L.

Nucleation of Crystals From Solution in Microgravity (USML-1 Glovebox (GBX) Investigation)

A new method for initiating nucleation from solutions in microgravity which avoids nucleation on container walls and other surfaces is described. This method consists of injecting a small quantity of highly concentrated, heated solution into the interior of a lightly supersaturated, cooler host gowth solution. It was tested successfully on USML-I, producing a large number of LAP crystals whose longest dimension averaged 1 mm.

Kroes, Roger L.

Crystal growth in a microgravity environment

Gravitational phenomena, including convection, sedimentation, and interactions of materials with their containers all affect the crystal growth process. If they are not taken into consideration they can have adverse effects on the quantity and quality of crystals produced. As a practical matter, convection, and sedimentation can be completely eliminated only under conditions of low gravity attained during orbital flight. There is, then, an advantage to effecting crystallization in space. In the absence of convection in a microgravity environment cooling proceeds by thermal diffusion from the walls to the center of the solution chamber. This renders control of nucleation difficult. Accordingly, there is a need for a new improved nucleation process in space. Crystals are nucleated by creating a small localized region of high relative supersaturation in a host solution at a lower degree of supersaturation.

Kroes, Roger L.

Initiating Growth Of Crystals Away From Container Walls

Nucleation controlled to obtain better crystals. In technique proposed specifically for growing large protein crystals in microgravity (where no thermal convection), small region of high supersaturation created by injection of hot concentrated solution or by use of cold probe. Crystals nucleate preferably in this small region. Also conceivable technique applied on Earth to crystallizations in melts and solutions sufficiently viscous to suppress convection to extent necessary to prevent cooling-induced nucleation in undesired sites.

Kroes, Roger L.

Concepts for microgravity experiments utilizing gloveboxes

The need for glovebox facilities on spacecraft in which microgravity materials processing experiments are performed is discussed. At present such facilities are being designed, and some of their capabilities are briefly described. A list of experiment concepts which would require or benefit from such facilities is presented.

Kroes, Roger L.

Development of new techniques for the characterization of crystals and their growth solutions: Center director's discretionary fund

The solubility measurement system and the laser scattering microscope system were designed, built, and utilized for the study of crystal growth solutions and crystal characterization measurements. Solubility measurements and crystal defect maps were made with this equipment for a number of new materials. In some cases, where there have been published solubility data (i.e., TGS), more accurate measurements were made and discrepancies in the published data were resolved. The design of these instruments is presented along with a description of their use and some typical data generated using them.

Kroes, Roger L.