In-situ Hypersonic Degradation Mechanisms of ZrB2
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Materials science↗
Engineering topics
Rosenberg, William
Publications and source records attributed to Rosenberg, William.
Thermostructural evolution of boron carbide characterized using in-situ x-ray diffraction
Boron carbide, with a nominal stoichiometry of B 4 C, is a highly desired ceramic candidate for armor applications due to its high hardness derived from the complex crystal structure. However, stress-induced local amorphization can lead to failure and is a known challenge for this material which must be addressed for applications in ballistic environments. Understanding boron carbide's atomic structural behavior and bonding environment is critical in determining effective strategies to mitigate these issues. Here, in this work, the thermo-structural behavior of B 4 C has been studied in detail using a conical nozzle levitator system coupled with in-situ synchrotron X-ray diffraction. Lattice expansion and the resulting thermal expansion coefficients (CTEs) were determined from 25-2100 °C. Rietveld refinements showed anisotropic atomic displacement for each of the 4 unique sites as a function of temperature. An exceptionally large z-axis displacement for the boron chain center is linked to bond weakness and may be linked to faster expansion of the α 33 relative to α 11 CTEs. Thermally induced lattice changes can inform the use of boron carbide at elevated temperatures as well as help develop strategies for mitigating structural failure for armor applications.
36 MATERIALS SCIENCE↗
Hubble Space Telescope particulate optical test
The Particulate Optical Test was designed to record and measure particulate contaminants on the Hubble Space Telescope primary mirror. The objective of the test was to quantify the primary mirror particulate contamination prior to launch. The test consists of taking dark-field photographs of the primary mirror from in front of the telescope's aperture door. These photographs are subsequently digitized and analyzed to produce the areal coverage estimates. The estimated particulate areal obscuration is approximately 1.0 percent of the primary mirror surface in the usable region. This level of contamination is within the budget value of 2.5 percent and indicates that there was little increase in particulate contamination during the HST assembly process or the acoustic test period.
Metheny, Wayne↗