With the recent advances in additive manufacturing (AM), long-range periodic lattice assemblies are being developed for vibration and shock mitigation components in aerospace and military applications with unique geometric and topological structures. There has been extensive work in understanding the static properties associated with varying topology of these lattice architectures, but there is almost no understanding of microstructural affects in such structures under high-strain rate dynamic loading conditions. Here we report the shock behavior of lattices with varying intrinsic grain structures achieved by post process annealing. High resolution 316L stainless steel lattices were 3D printed by a laser-powder bed fusion machine and characterized by computed tomography. Subsequent annealing resulted in stress-relieved and recrystallized lattices. Overall the lattices had strong cubic texture aligning with the x-, y- and z-directions of the build with a preference outside the build direction (z). The recrystallized sample had more equiaxed polygonal grains and a layer of BCC ferrite at the surface of the structure approximately 1 grain thick. Upon dynamic compression the as-deposited lattice showed steady compaction behavior while the heat-treated lattices exhibit negative velocity behavior indicative of failure. We attribute this to the stiffer BCC ferrite in the annealed lattices becoming damaged and fragmenting during compression.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Stabilization of Electrodeposited Calcium: The Impact of Morphology Interphases and Impurities.

Abstract not provided.

McClary, Scott Andrew↗

DOE OSTI2020

Lattice Structures for Dynamic Impact Environments.

Abstract not provided.

Jared, Bradley↗

DOE OSTI2019

The Terra Vega Active Light Source: A First Step in a New Approach to Perform Nighttime Absolute Radiometric Calibrations and Early Results Calibrating the VIIRS DNB

A fully automated, National Institute of Standards and Technology (NIST)-traceable artificial light source called Terra Vega has been developed to radiometrically calibrate the Visible Infrared Imaging Radiometer (VIIRS) Day Night Band (DNB) working in high gain stage (HGS) mode. The Terra Vega active point source is a calibrated integrating sphere that is only a fraction in size of a VIIRS DNB pixel. As such, it can be considered analogous to a ground-based photometric reference star. Vicarious calibrations that employ active point sources are different than those that make use of traditional extended sources and can be applyed to quantify the brightness of artificial light sources. The active source is successfully fielded, and early results indicate that it can be used to augment and validate the radiometric calibration of the VIIRS DNB HGS sensor on both the Suomi National Polar-orbiting Partnership (NPP) and NOAA-20 satellites. The VIIRS DNB HGS sensor can benefit from this technology as on-board calibration is challenging and hinges on transferring low gain stage (LGS) calibration using a solar diffuser to the medium gain stage (MGS) and HGS via regions of overlap. Current vicarious calibration methods that use a lunar-illuminated extended source estimate the HGS radiometric accuracy to within 8-15%. By comparison, early results and analysis showed that Terra Vega is stable to about 1%. Under clear dark night conditions, predicted top-of-atmosphere radiance from Terra Vega ranged between 1–11% of VIIRS measured values. Terra Vega’s excellent stability opens up new opportunities to validate and develop nighttime imaging applications based on point sources.

Ryan, Robert↗

NASA NTRS2016

Dislocation Content Measured Via 3D HR-EBSD Near a Grain Boundary in an AlCu Oligocrystal

Interactions between dislocations and grain boundaries are poorly understood and crucial to mesoscale plasticity modeling. Much of our understanding of dislocation-grain boundary interaction comes from atomistic simulations and TEM studies, both of which are extremely limited in scale. High angular resolution EBSD-based continuum dislocation microscopy provides a way of measuring dislocation activity at length scales and accuracies relevant to crystal plasticity, but it is limited as a two-dimensional technique, meaning the character of the grain boundary and the complete dislocation activity is difficult to recover. However, the commercialization of plasma FIB dual-beam microscopes have made 3D EBSD studies all the more feasible. The objective of this work is to apply high angular resolution cross correlation EBSD to a 3D EBSD data set collected by serial sectioning in a FIB to characterize dislocation interaction with a grain boundary. Three dimensional high angular resolution cross correlation EBSD analysis was applied to an AlCu oligocrystal to measure dislocation densities around a grain boundary. Distortion derivatives associated with the plasma FIB serial sectioning were higher than expected, possibly due to geometric uncertainty between layers. Future work will focus on mitigating the geometric uncertainty and examining more regions of interest along the grain boundary to glean information on dislocation-grain boundary interaction.

Ruggles, Timothy↗