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Sandlin, A. C.

Publications and source records attributed to Sandlin, A. C..

The influence of gravity level during directional solidification of immiscible alloys

During directional solidification of immiscible (hypermonotectic) alloys it is theoretically possible to establish a stable macroscopically-planar solidification front, and thus avoid sedimentation. Unfortunately, convective instabilities often occur which interfere with the directional solidification process. In this paper, stability conditions are discussed and results presented from directional solidification studies carried out aboard NASA's KC-135 zero-g aircraft. Samples were directionally solidified while the effective gravity level was varied from approximately 0.01 g for 25 s to 1.8 g for 45 s. Dramatic variations in microstructure were observed with gravity level during solidification.

Andrews, J. B.↗

Directional solidification in immiscible systems - The influence of gravity

The possibility of producing aligned fibrous composite microstructures with a high volume fraction of the immiscible phase, L2, through the directional solidification of hypermonotectic alloys is examined. Early work suggests that low gravity conditions are necessary to prevent sedimentation of the more dense L2 phase. However, if convective flows result, they disrupt the formation of the desired fibrous microstructure and produce a disperse structure. The need for long-duration low-g experiments is emphasized.

Andrews, J. B.↗

The effect of processing conditions on solidified structures in immiscible systems

The incentive for low-gravity processing of immiscible alloys is usually tied to an attempt to eliminate sedimentation of the more dense immiscible liquid phase during processing. However, many other factors can influence the solidified structure of these alloys. For example, crucible wetting by one of the immiscible liquid phases during normal (non-directional) low-gravity solidification in a container has been shown to often lead to a completely separated structure. For containerless, low-gravity processing, alloy composition has a tremendous affect on the structure formed. During directional solidification, alloy composition, thermal gradient, solidification rate, convective instability and the miscibility gap height of the system all have a major effect on the structures obtained. This paper discusses the conditions necessary for the production of desired microstructures in each of these processing techniques. Examples are shown of samples processed under both desirable and undesirable conditions.

Andrews, J. B.↗

Influence of gravity level and interfacial energies on dispersion-forming tendencies in hypermonotectic Cu-Pb-Al alloys

Results on the nondirectional solidification of several hypermonotectic Cu-Pb-Al alloys were obtained aboard NASA's KC-135 zero-gravity aircraft in order to determine the influence of interfacial energies and gravity levels on dispersion-forming tendencies. The Al content was systematially varied in the alloys. The dispersion-forming ability is correlated with gravity level during solidification, the interfacial energy between the immiscible phases, and the tendency for the minority immiscible phase to wet the walls of the crucible.

Andrews, J. B.↗

The influence of interfacial energies and gravitational levels on the directionally solidified structures in hypermonotectic alloys

Various Cu-Pb-Al alloys were directionally solidified under 1-g conditions and alternating high-g/low-g conditions (achieved using NSAS's KC-135 aircraft) as a means of studying the influence of interfacial energies and gravitational levels on the resulting microstructures. Directional solidification of low Al content alloys was found to result in samples with coarser more irregular microstructures than in alloys with high Al contents under all the gravity conditions considered. Structures are correlated with interfacial energies, growth rates, and gravitational levels.

Andrews, J. B.↗