Schilling, Christopher

NASA NTRS1988

Making Smaller Microshells From Refractory Metals

Tendency toward gas porosity exploited. Falling through drop tube, fine drops of molten metal lose heat to surroundings, forming hard shells around precipitated gas. Second heating/cooling cycle in drop tube of lower pressure lets gas expand. Process produces smaller shells in greater variety of materials than possible with such current processes as based on hollow-jet instability, dry-chemical blowing or fluid-droplet drying. Shell aspect ratio (ratio of radius to wall thickness) controllable. New process makes shells having diameters smaller than 100 micrometer. There are several candidate shell materials including refractory metals.

Lee, Mark C.↗

NASA NTRS1987

Method and apparatus for generating microshells of refractory materials

A system is described for forming accurately spherical and centered fluid-filled shells, especially of high melting temperature material. Material which is to form the shells is placed in a solid form in a container, and the material is rapidly heated to a molten temperature to avoid recrystallization and the possible generation of unwanted microbubbles in the melt. Immediately after the molten shells are formed, they drop through a drop tower whose upper end is heated along a distance of at least one foot to provide time for dissipation of surface waves on the shells while they cool to a highly viscous, or just above melting temperature so that the bubble within the shell will not rise and become off centered. The rest of the tower is cryogenically cooled to cool the shell to a solid state.

Lee, Mark C.↗