Engineering topics

Shah, K.

Publications and source records attributed to Shah, K..

3 records

DOE OSTI2024

X-ray sources for in situ wavelength calibration of x-ray imaging crystal spectrometers

X-ray sources for a range of wavelengths are being considered for in situ calibration of X-ray Imaging Crystal Spectrometers (XICSs) and for monitoring line shifts due to changes in the crystal temperature, which can vary during experimental operation over a day [A. Ince-Cushman et al., Rev. Sci. Instrum. 79, 10E302 (2008), L. Delgado-Aparicio et al., Plasma Phys. Control. Fusion 55, 125011 (2013)]. Such crystal temperature dependent shifts, if not accounted for, could be erroneously interpreted as Doppler shifts leading to errors in plasma flow-velocity measurements. The x-ray sources encompass characteristic x-ray lines falling within the wavelength range of 0.9–4.0 Å, relevant for the XICSs on present and future fusion devices. Several technological challenges associated with the development of x-ray sources for in situ calibration are identified and are being addressed in the design of multiple x-ray tubes, which will be installed inside the spectrometer housing of the XICS for the JT-60SA tokamak. These x-ray sources will be especially useful for in situ calibration between plasma discharges. Here, in this paper, laboratory experiments are described that were conducted with a Cu x-ray source, a heated quartz (102) crystal, and a pixelated Pilatus detector to measure the temperature dependent shifts of the Cu Kα 1 and Kα 2 lines at 1.5405 and 1.5443 Å, respectively, and to evaluate the 2d-lattice constant for the Bragg reflecting crystal planes as a function of temperature, which, in the case of in situ wavelength calibration, would have to be used for numerical analysis of the x-ray spectra from the plasma.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NASA NTRS1999

Modeled Impact of Cirrus Cloud Increases Along Aircraft Flight Paths

The potential impact of contrails and alterations in the lifetime of background cirrus due to subsonic airplane water and aerosol emissions has been investigated in a set of experiments using the GISS GCM connected to a q-flux ocean. Cirrus clouds at a height of 12-15km, with an optical thickness of 0.33, were input to the model "x" percentage of clear-sky occasions along subsonic aircraft flight paths, where x is varied from .05% to 6%. Two types of experiments were performed: one with the percentage cirrus cloud increase independent of flight density, as long as a certain minimum density was exceeded; the other with the percentage related to the density of fuel expenditure. The overall climate impact was similar with the two approaches, due to the feedbacks of the climate system. Fifty years were run for eight such experiments, with the following conclusions based on the stable results from years 30-50 for each. The experiments show that adding cirrus to the upper troposphere results in a stabilization of the atmosphere, which leads to some decrease in cloud cover at levels below the insertion altitude. Considering then the total effect on upper level cloud cover (above 5 km altitude), the equilibrium global mean temperature response shows that altering high level clouds by 1% changes the global mean temperature by 0.43C. The response is highly linear (linear correlation coefficient of 0.996) for high cloud cover changes between 0. 1% and 5%. The effect is amplified in the Northern Hemisphere, more so with greater cloud cover change. The temperature effect maximizes around 10 km (at greater than 40C warming with a 4.8% increase in upper level clouds), again more so with greater warming. The high cloud cover change shows the flight path influence most clearly with the smallest warming magnitudes; with greater warming, the model feedbacks introduce a strong tropical response. Similarly, the surface temperature response is dominated by the feedbacks, and shows little geographical relationship to the high cloud input. Considering whether these effects would be observable, changing upper level cloud cover by as little as 0.4% produces warming greater than 2 standard deviations in the Microwave Sounding Unit (MSU) channels 4, 2 and 2r, in flight path regions and in the subtropics. Despite the simplified nature of these experiments, the results emphasize the sensitivity of the modeled climate to high level cloud cover changes, and thus the potential ability of aircraft to influence climate by altering clouds in the upper troposphere.

Rind, David↗

NASA NTRS1987

Soft x ray window encapsulant for HgI2 detectors

HgI2 is an excellent semiconductor material for a low energy, room temperature x-ray spectrometer. The high values of the atomic numbers for its constituent elements gives high x-ray and gamma ray stopping power. The band gap of HgI2 is significantly higher than other commonly used semiconductors. Owing to the large value band gap, the leakage current for HgI2 devices is smaller, thus allowing low noise performance. Devices fabricated from HgI2 crystals have demonstrated energy resolution sufficient to distinguish the x-ray emission from the neighboring elements on the periodic table. Also the power requirements of HgI2 are very low. These characteristics make a HgI2 spectrometer an ideal component in a satellite based detection system. Unfortunately, HgI2 crystals tend to deteriorate with time, even if protected by standard semiconductor encapsulants. This degradation ruins the performance of the device in terms of its energy resolution and pulse amplitude. The degrading mechanism is believed to be material loss occurring from below the electrodes, due to high vapor pressure of HgI2 at room temperature. To address this major obstacle to rapid expansion of HgI2 technology, a research program aimed at improving device stability by encapsulation with inert polymeric materials was carried out. The program focused specifically on optimizing the encapsulant materials and their deposition techniques. The principal objectives for this program were device encapsulation, device testing, and accelerated testing to ensure very long term stability of these high resolution sensors. A variety of encapsulants were investigated with the selection criteria based on their chemical diffusion barrier properties, mechanical stability, reactivity, and morphology of encapsulant films. The investigation covered different classes of encapsulants including solvent based encapsulants, vapor deposited encapsulants, and plasma polymerized encapsulants. A variety of characterization techniques were employed to examine their effectiveness in stabilizing HgI2 devices; these included permeability evaluation, vacuum and heat testing, scanning electron microscopy (SEM) as well as studying the detector performance of coated detectors. The plasma polymerized films appear to have entirely solved the HgI2 degradation problem. Another achievement of this program was the development of an accelerated testing technique which correlates extremely well with long term tesing.

Entine, G.↗