Engineering topics

Smith, Alan R.

Publications and source records attributed to Smith, Alan R..

6 records

DOE OSTI2021

Trace explosives sampling for security applications (TESSA) study: Evaluation of procedures and methodology for contact sampling efficiency

We report the detection of trace amounts of explosive materials is critical to the security at mass transit centers (e.g., airports and railway stations). In a typical screening process, a trap is used to probe a surface of interest to collect and transfer particulate residue to a detector for analysis. The collection of residues from the surface being probed is widely viewed as the limiting step in this process. A multi-institutional study was performed to establish a methodology for the evaluation of sampling media collection efficiencies. Dry deposited residues of 1,3,5-trinitroperhydro-1,3,5-triazine (RDX), C-4 (an RDX-based explosive), and pentaerythritol tetranitrate (PETN) were harvested from acrylonitrile butadiene styrene (ABS) plastic, ballistic nylon (NYL), and uncoated aluminum surfaces using muslin, Texwipe cotton, and stainless-steel mesh traps. Transfer and collection efficiencies of the sample media were calculated based on liquid chromatography-mass spectrometry analysis. Dry transfer efficiencies (DTE%) to all tested surfaces were greater than 75%, with transfer to ABS plastic being the lowest. Collection efficiency (CE%) varied significantly across the traps and the surfaces, yet some conclusions can be drawn; nylon had the lowest CE% for all cases (~10%), and the stainless steel mesh had the lowest CE% for the evaluated traps (~20%). Though the testing parameters have been standardized among the participants to establish a framework for an independent comparison of contact sampling media and surfaces, substantial variations in the DTE% and the CE% were observed, suggesting that other variables can affect contact sampling.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1995

Doing photons with MERLIN 2 at Oroville

A very large n-type high-purity Ge-semiconductor detector has recently been installed in the Lawrence Berkeley Laboratory's underground low-background facility at Oroville. The detector (named MERLIN II) is mounted in a low-activity cryostat and has a rated 'efficiency' of about 115 percent -- nearly 4 times higher than our original MERLIN detector, which was used extensively to measure the minute amounts of radioactivity in samples from the LDEF satellite. We discuss gamma-spectrometric analyses with MERLIN II on some of the same LDEF samples, providing direct evidence for improvement in performance achieved with the larger detector.

Smith, Alan R.↗

NASA NTRS1993

A photon phreak digs the LDEF happening

A year ago at the First Long Duration Exposure Facility (LDEF) Post-Retrieval Symposium, detailed measurements on trunnion sections, as well as results from 'intentional' samples (Co, Ni, In, Ta, and V) and spacecraft parts were reported. For this year's Symposium, some of these findings are re-evaluated in combination with more recent results, to cast a longer perspective on the LDEF experience, and to sketch some promising avenues toward more effective participation in future missions. The LDEF analysis effort has been a superb training exercise, from which lessons learned need to be applied to future missions - right back to the early phases of mission planning.

Smith, Alan R.↗

NASA NTRS1992

A photon-phreak digs the LDEF happening

Radioactivities of the LDEF onboard experiments induced by gamma emitting rays in both intentional samples and spacecraft parts were examined. The long time greatly enhanced the ability to detect some of the longer lived nuclides, including: 2.6 yr Na-22 in Al and Fe; 5.3 yr Co-60 in Co, Ni, and In; 2.9 yr Rh-102 in In; and 38 yr Bi-207 in Pb. These radionuclides, along with such other as 33 yr Ar-42 in Ti, Fe, or Ni and 47 yr Ti-44 in the same elements, would be appropriate monitors of the high energy space radiation field on long round-trip voyages in the solar system. Additional candidate radionuclides are also discussed. Radiometric analysis of the LDEF samples was a substantial effort among a dedicated group of experts in low level counting, and highlights several important aspects of the procedures needed to achieve success in this kind of endeavor. Target elements should be chosen to differentiate between neutron and proton induced reactions, whenever this is feasible. Reactions should be chosen with a wide range of energy thresholds, to enable calculation of both intensity and energy spectra of the particle fluxes.

Smith, Alan R.↗

NASA NTRS1992

Radioactivities of Long Duration Exposure Facility (LDEF) materials: Baggage and bonanzas

Radioactivities in materials onboard the returned Long Duration Exposure Facility (LDEF) satellite were studied by a variety of techniques. Among the most powerful is low-background Ge-semiconductor detector gamma-ray spectrometry, illustrated here by results obtained at the Lawrence Berkeley Laboratory's (LBL) Low Background Facilities. The observed radioactivities are of two origins: those radionuclides produced by nuclear reactions with the radiation field in orbit, and radionuclides present initially as 'contaminants' in materials used for construction of the spacecraft and experimental assemblies. In the first category are experiment-related monitor foils and tomato seeds, and such spacecraft materials as aluminum, stainless steel, and titanium. In the second category are aluminum, beryllium, titanium, vanadium, and some special glasses.

Smith, Alan R.↗

NASA NTRS1991

Radioactivities of Long Duration Exposure Facility (LDEF) materials: Baggage and bonanzas

Radioactivities in materials onboard the returned Long Duration Exposure Facility (LDEF) satellite were studied by a variety of techniques. Among the most powerful is low background Ge semiconductor detector gamma ray spectrometry. The observed radioactivities are of two origins: those radionuclides produced by nuclear reactions with the radiation field in orbit and radionuclides present initially as contaminants in materials used for construction of the spacecraft and experimental assemblies. In the first category are experiment related monitor foils and tomato seeds, and such spacecraft materials as Al, stainless steel, and Ti. In the second category are Al, Be, Ti, Va, and some special glasses. Consider that measured peak-area count rates from both categories range from a high value of about 1 count per minute down to less than 0.001 count per minute. Successful measurement of count rates toward the low end of this range can be achieved only through low background techniques, such as used to obtain the results presented here.

Smith, Alan R.↗