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Sparks, L. L.

Publications and source records attributed to Sparks, L. L..

At least 19 records

Thermal conductivity of evacuated perlite at low temperatures as a function of load and load history

Perlite, a powdered insulation, is commonly used in large cryogenic storage dewars. When these dewars are thermally cycled, the perlite in the evacuated space between the inner and outer vessels of the dewar experiences a changing mechanical load due to thermal expansion and contraction of the inner vessel. Thermal conductivity data were obtained using a boil-off calorimeter. The apparent thermal conductivity of evacuated perlite increases strongly with applied load. Hysteretic behavior of the conductivity was observed when perlite was subjected to cyclic mechanical loading.

Dube, W. P.

Advanced Reusable Foam Cryogenic Insulation

Lightweight, reusable cryogenic containers reduce costs of operation of advanced hypersonic airplanes and space launch vehicles. Specimens demonstrated in temperature range of negative 420 to positive 400 degrees F (negative 251 to positive 204 degrees C). Prototype reusable cryogenic foam insulation developed. Consists of two discrete layers of closed-cell polymethacrylimide foam of density 6.9 lb/ft to the 3rd power (111 kg/m to the 3rd power) bonded together with epoxy adhesive. Additionally reinforced with 0.003-in. (0.08-mm)-thick layer of fiberglass cloth. Wrapped with precut and preformed vapor-barrier cover. Such containers useful on Earth in laboratories, factories, and transportation systems.

Taylor, Allan H.

Apparatus for measurement of thermal conductivity of insulation systems subjected to extreme temperature differences

Advanced aerospace designs require thermal insulation systems which are consistent with cryogenic fluids, high thermal loads, and design restrictions such as weight and volume. To evaluate the thermal performance of these insulating systems, an apparatus capable of measuring thermal conductivity using extreme temperature differences (27 to 1100 K) is being developed. This system is described along with estimates of precision and accuracy in selected operating conditions. Preliminary data are presented.

Dube, W. P.

Apparatus for measurement of coefficient of friction

An apparatus designed to measure the coefficient of friction in certain controlled atmospheres is described. The coefficient of friction observed during high-load tests was nearly constant, with an average value of 0.56. This value is in general agreement with that found in the literature and also with the initial friction coefficient value of 0.67 measured during self-mated friction of 440C steel in an oxygen environment.

Slifka, A. J.

Small scale demand type neon liquefaction plant

Low-temperature measurement of the thermal conductivity of insulating materials is generally made using a boil-off calorimetry technique involving liquid hydrogen (LH2). Liquid neon (LNe) has nearly the same normal boiling point as LH2, but has a much larger heat of vaporization, allowing extended run times. The main drawback of using LNe has been its excessive cost; $170.00 versus $1.50/l for LH2 (1989 prices). A neon liquefaction plant has been designed and constructed to capture, purify, and refrigerate the neon boil-off from calorimetry experiments. Recycling the neon reduces operating costs to approximately $20/l. The system consists of a purification section, a heat exchanger, LNe and LH2 storage dewars, and a fully automated control system. After purification, neon is liquified in the heat exchanger by LH2 flowing countercurrently through stainless steel cooling coils. Hydrogen flow is automatically adjusted to keep the neon at its normal saturation temperature, 27 K. The liquid neon is then stored in a dewar placed directly below the heat exchanger.

Dube, W. P.

NBC boil-off calorimeter for measuring thermal conductivity of insulating materials

Modern temperature, pressure and flow sensors along with a high speed digital control system have been incorporated into an existing thermal conductivity apparatus (ASTM C745). The system has also been modified to include the use of liquid helium as the refrigerant, if desired. The apparatus can be used to study thermal conductivity in the temperature range from 4 K to room temperature. Preliminary results on insulating materials indicate that the system update has significantly improved the precision and operational characteristics of the apparatus. Basic principles of operation, sources of system error and the reduction of system error by application of digital control and modern sensors are discussed. Preliminary data are presented.

Dube, W. P.

ASRDI oxygen technology survey. Volume 4: Low temperature measurement

Information is presented on temperature measurement between the triple point and critical point of liquid oxygen. The criterion selected is that all transducers which may reasonably be employed in the liquid oxygen (LO2) temperature range are considered. The temperature range for each transducer is the appropriate full range for the particular thermometer. The discussion of each thermometer or type of thermometer includes the following information: (1) useful temperature range, (2) general and particular methods of construction and the advantages of each type, (3) specifications (accuracy, reproducibility, response time, etc.), (4) associated instrumentation, (5) calibrations and procedures, and (6) analytical representations.

Sparks, L. L.

Carbon thin film thermometry

The work concerning carbon thin film thermometry is reported. Optimum film deposition parameters were sought on an empirical basis for maximum stability of the films. One hundred films were fabricated for use at the Marshall Space Flight Center; 10 of these films were given a precise quasi-continuous calibration of temperature vs. resistance with 22 intervals between 5 and 80 K using primary platinum and germanium thermometers. Sensitivity curves were established and the remaining 90 films were given a three point calibration and fitted to the established sensitivity curves. Hydrogen gas-liquid discrimination set points are given for each film.

Collier, R. S.

Thermal conductivity of austenitic stainless steel, SRM 735, from 5 to 280 K

Thermal conductivity and electrical resistivity measurements were conducted on two lots of an austenitic stainless steel. Electrical resistivity measurements were performed on the second lot, both before and after the material was hot-swaged and reannealed to a size 1/10 the original diameter. These measurements indicate that this steel can be swaged and reannealed without an appreciable change in thermal conductivity. Electrical resistivity measurements as well as direct thermal conductivity measurements on several specimens from both lots indicate a material variability in these lots of less than 1% in thermal conductivity.

Hust, J. G.

Reference data for thermocouple materials below the ice point.

Standard thermoelectric data have been determined for four thermocouple combinations used below the ice point: commercial types E, K, and T and the special combination of KP vs Au-0.07 at.% Fe. Power series coefficients necessary to generate E = f(T) data for these combinations are given. In addition, extensive tests were carried out to ascertain the variability between materials from different manufacturers. Typical wires processed for low-temperature usage often have slightly thermoelectric properties (up to 1%) from those, nominally identical, wires made for high-temperature applications. Generally, type E is the most satisfactory standardized commercial combination. The Au-0.07 at.% Fe material has been examined in particular detail, because it is not yet an ISA standard material. It has excellent sensitivity in the liquid helium/liquid hydrogen temperature range and a nearly linear thermovoltage at higher temperatures.

Sparks, L. L.

Standard reference materials: Thermal conductivity of electrolytic iron, SRM 734, from 4 to 300 K

Thermal conductivity data were obtained by the axial one-dimensional heat flow method for a cylindrical rod 3.6 mm in diameter and 23 cm long with an electric heater at one end and a temperature controlled sink at the other. Variability of this iron was studied by means of electrical residual resistivity ratio measurements on 63 specimens. This study showed that with a two-hour anneal at 1000 C one can obtain a thermal conductivity Standard Reference Material that has variability of less than 1% in thermal conductivity.

Hust, J. G.

Thermal conductivity, electrical resistivity, and thermopower of aerospace alloys from 4 to 300 K. 6: Fe-22Cr-13Ni-5Mn stainless steel

The equipment and techniques for determining the thermal conductivity, electrical resistivity Lorenz ratio, and thermopower characteristics of Fe-22Cr-13Ni-5Mn stainless steel are discussed. The dimensions of the specimen and its preparation are described. The experimental data are represented by arbitrary functions over the entire range and smooth tables are generated from these functions.

Hust, J. G.

Cryogenic thermocouple calibration tables

Thermocouple calibration standards are developed for low-temperature thermocouple materials. Thermovoltage, thermopower, and the thermopower derivative are presented in tabular and graphical form.

Hall, W. J.

Cryogenic thermocouple research

Cryogenic thermocouples of various metal pairs for low temperature measurements, discussing performance tests and calibrations

Hall, W. J.