Surface Morphologies and Space Weathering Features of Ryugu Samples
Surface morphologies and space weathering features of Ryugu samples
T. Matsumoto↗
Engineering topics
T. Nakamura
Publications and source records attributed to T. Nakamura.
Mineralogy and Surface Modification of Small Grains Recovered from the Asteroid 162173 Ryugu
Surface material on airless bodies exposed to the interplanetary space experienced the bombardment by low-energy (~1 keV/nucleon) solar wind particles and micrometeoroid impacts. These processes, alongside the resultant surface modifications, and spectral darkening and reddening are called space weathering [1]. Space weathering of the Moon and the asteroid 25143 Itokawa belonging to S-type asteroids have been investigated intensively [e.g. 1-5]. The Hayabusa 2 spacecraft returned samples from the asteroid 162173 Ryugu C-type asteroid. The Ryugu samples give us the first opportunity to investigate space weathering of C-type asteroids. The Mineralogy-Petrology Fine (M-P F or Sand) sub-team mainly investigates small grains (typically ~100 μm across). The main purposes of the M-P F sub-team are to understand the variationof mineralogy of the allocated grains and the nature of space weathering of the asteroid Ryugu. The M-P F sub-team is comprised of 51 members belonging to 25 universities and laboratories
T. Noguchi↗
Constraints on the surface materials of Ryugu from spectral and water analysis of experimentally-heated CI carbonaceous chondrite
We performed heating experiments of the Orgueil CI chondrite in vacuum conditions at fO2 around I/W to evaluate systematic changes in mineralogy, water contents, and visible to infrared spectral features. Our goal is to interpret the spectra of Ryugu, the target C asteroid of the Hayabusa2 mission, because Ryugu shows spectral features similar to partially dehydrated carbonaceous chondrites. However heated carbonaceous chondrites can be easily contaminated by terrestrial water, which makes it almost impossible for laboratory data to be compared with spectra of asteroids directly. Therefore, our heated samples were analyzed without exposure to the air after experimental heating to minimize the effects of terrestrial water. The depth of the 2.7-µm absorption band and the water content of the heated Orgueil form a positive correlation trend which follows the results of experimental heating of CM and Tagish Lake meteorites using our experimental procedures. It is found that 500-°C heated Orgueil sample shows the best spectral match with Ryugu in terms of the low reflectance (~2%) at visible wavelengths and a weak absorption (~10%) at around 2.72 µm owing to survival of Mg-rich phyllosilicates. We suggest that Ryugu might have experienced heating and dehydration at a temperature around 500 °C, after aqueous alteration, and presently contains a small quantity of hydrated minerals equivalent to 1-2 wt.% of water at the surface.
K. Amano↗
Experimental reproduction of space weathering of C-type asteroids by He exposure: irradiation-energy and physical-property dependence
Visible and near-infrared observations of C-type asteroid 162173 Ryugu suggest that the surface color variation seems to have resulted from a surface-correlated process which changed the color from blue to red, but the mechanism for the change is not yet identified. Space weathering is one possible mechanism responsible for the color variation, but the spectral changes of C-type asteroids from space weathering are not yet fully understood. We have carried out He exposure experiments on hydrous carbonaceous chondrites in order to understand the irradiation-energy and the physical-property dependence of space weathering of C-type asteroids. He exposure to different porosities of the same meteorite samples results in different behavior of spectral changes. In addition, the meteorite samples with the same porosity and the same surface roughness show different spectral changes when the samples are exposed to He ions with different energies. Therefore, our experiments indicate that spectral changes by space weathering of C-type asteroids depend not only on the asteroid types but also on the physical properties of the regolith surface and the solar-wind He energy.
Michael E Zolensky↗
Reflectance spectra measurement plan of captured samples from Ryugu: current status
Hayabusa2 spacecraft is equipped with Optical Navigation Camera (ONC) andNear-infrared Spectrometer (NIRS3), and has obtained reflectance spectra of the C-type near-Earth asteroid Ryugu over a wavelength range of 0.40–0.95 μm and 1.8–3.2 μm, respectively. It was revealed that Ryugu exhibits globally very low albedo (less than 0.02 at 0.55 and 2.0 μm), a slightly positive spectral slope, and an ubiquitous weak but sharp OH absorption band centered at 2.72 μm,showing a little regional heterogeneities. Thus, the surface material of Ryugu can be estimated as relatively similar to moderately heated carbonaceous chondrites, e.g., moderately dehydrated CI and CM, and enriched in carbon (Kitazato et al., 2019; Sugita et al., 2019; Tatsumi et al., 2020).Hayabusa2 successfully has performed twice touch down operations, and the captured sample will be brought back to the Earth in late 2020 (Morota et al., 2020; Tachibana et al., in preparation). To clarify Ryugu’s mineralogical and physicochemical properties and their varieties, effective for spectral characteristics obtained by ONC and NIRS3, several grains are planned to be distributed to several primary analysis groups. In this study, we report the current status of our spectral analysis plan in Hayabusa2 MINeralogy and PETrology of coarse grains (MIN-PET CG) team led by T. Nakamura, and the latest rehearsal analysis result using carbonaceous chondrite samples. MIN-PET CG rehearsal measurements have been performed to obtain detailed spectral properties of Ryugu grains with diverse spatial resolutions ranging from μm to mm scale or larger; using a few mm size polished CM sample with several microscopic imaging spectrometers covering various spatial range; with 200 μmor finer spatial resolution at Institut d’Astrophysique Spatiale, ~50 and 150 μm spatial resolution invisible and IR ranges at Brown University, and with 40 μm or larger spatial resolution at Tohoku University, and using mm-size CM and CI grains with a diffuse reflectance spectrometer with a few mm resolution at Tohoku University. Diffuse reflectance spectroscopy measurements undergo to use several mm-size CM or CI chondrite grains with Bruker VERTEX 70v, which covers ~0.38–15 μm in wavelength. To keep returned samples out of atmosphere avoiding any terrestrial contamination, wehave prepared an air shutoff cell to put samples and standard materials together kept in a N2 purged condition (Amano et al., 2020). Samples are Murchison CM chondrite showing typically ~5%reflectance with a strong OH absorption band at ~2.8 μm, and laboratory heated CI chondrite showing~3% reflectance, and a weak OH absorption band at ~2.7 μm. We will perform (1) fixed angle condition as laboratory standard setting at incident, emission, and phase angles of 30°, 0°, 30°, or 0°,30°, 30°, and (2) various angle conditions for photometric corrections. Future lab analyses of samples returned from Ryugu will provide direct and detailed information on the mineralogical and physicochemical properties of Ryugu, and relationship of spectral characteristics obtained by remote sensing and laboratory instruments.
M. Matsuoka↗
Current Status of DESTINY+ and Updated Undertstanding of Its Target Asteroid (3200) Phaethon
DESTINY+ is a joint mission of technology demonstration and science observation, which was selected for JAXA/ISAS small-class space program in 2017. The paper informs the current status of the mission and its target asteroid.
T. Arai↗
Progress of chemical characterization of asteroid Ryugu samples
It is believed that meteorites come from asteroids. Samples of asteroid (25143) Itokawa returned by the JAXA Hayabusa mission revealed that S-type asteroids are composed of materials consistent with the ordinary chondrite class[1,2]. The JAXA Hayabusa 2 [3]spacecraft launched on December 3rd, 2014 towards an asteroid (162173) Ryuguto clarify relationships between C-type asteroids and the carbonaceous chondrite class. Remote sensing observations from Hayabusa 2 show that (1) the albedo of Ryugu is darker than those of every known meteorite class[4, 5], (2) an absorption band at 2.72 μm indicates that phyllosilicates are ubiquitous on Ryugu [5],(3) the strength and shape of the absorption band feature suggests that Ryugu materials experienced heating above 300 °C[6], and (4) thermal inertia suggests that Ryugu materials are more porous than every known carbonaceous chondrite[7]. These results suggest that carbonaceous chondrite class materials are plausible for Ryugu materials, but no known carbonaceous chondrite completely matches the results obtained from Ryugu. *Complete abstract available in attached document
Lan Anh Ngoc Nguyen↗
Ultraviolet/Visible Reflectance Spectra of Returned Samples of (162173) Ryugu Unexposed to Earth’s Atmosphere
Following the successful return of JAXA’s Hayabusa2 sample capsule, the material from asteroid (162173) Ryugu retrieved from the spacecraft retrieval container has been the subject of multi-pronged analyses [e.g., 1]. We undertook an effort to acquire reflectance spectra covering 200- to- 1100 nm of particles from Ryugu. This region probes the near-ultraviolet (NUV) to acquire reflectance spectra that cover the 250-nm Fresnel peak that can result from increased graphitization (reduced H content) of carbon-bearing materials. Laboratory tests show that increased graphitization could result from the effects of increased temperature, an effect of space weathering of materials closer to the Sun. Some ground-based reflectance spectra and space-based photometry of Ryugu show that reflectance is increasing with decreasing wavelength, suggesting the beginning of a UV upturn [2]. We sought evidence for space weathering (graphitization) of the Ryugu material at NUV wavelengths, by acquiring reflectance spectra of surface samples.
F Vilas↗
Early History of Ryugu’s Parent Asteroid: Evidence from Return Sample
Near-Earth Cb-type asteroid (162173) Ryugu is a rubble pile asteroid made of fragments of the original parent asteroid [1-5]. It is possible that the fragments from various depths of the original asteroid are on the surface of the present-day Ryugu. Therefore, samples collected from Ryugu are expected to retain formation and evolution history of the interior of Ryugu’s parent asteroid. In this study, we will focus on understanding the early history of Ryugu’s parent asteroid. For this purpose, we need to understand: 1) when and where in the solar nebula Ryugu’s parent asteroid formed, 2) the original mineralogy and the abundance and composition of water-rich ice in the accreted materials, 3) how these materials chemically and mineralogically evolved, and 4) how the parent body was destroyed by a catastrophic collision.
T. Nakamura↗
Olivine Compositional Variation of Asteroid Ryugu Samples: Possible Precursors of Ryugu’s Parent Asteroid
JAXA’s Hayabusa2 spacecraft successfully recovered samples from Cb-type asteroid Ryugu and returned samples are now under detailed scrutiny by the international community. The ongoing initial analysis has so far revealed that the Ryugu samples are pristine primitive asteroidal materials mostly composed of secondary minerals such asphyllosilicates, carbonates, Fe sulfides and magnetite associated with organic matter [e.g., 1]. However, some samples contain small amounts of anhydrous silicates and oxides such as olivine that are thought to be the precursors of the Ryugu parent asteroid. Their sizes are mostly <5 mm, and detailed mineralogical analysis is possible using an electron microprobe with field emission gun (FE-EPMA). Here we report results of our extensive FE-EPMA analysis of an hydrous minerals focusing on olivine to compare with literature chondritic data. We also performed synchrotron XRD of olivine crystals to evaluate the shock degree of Ryugu samples. These analyses allow us to discuss the formation of Ryugu in light of the solar system early evolution.
T Mikouchi↗
Mineralogy and Space Weathering of Fine Fraction Recovered from Asteroid (162173) Ryugu
JAXA Hayabusa2 spacecraft brought back 5.4 g of samples from the near-Earth C-type asteroid (162173) Ryugu to Earth on December6th, 2020 [1]. The returned samples give us a unique opportunity to investigate material from the surface of a C-type asteroid that is expected to record space weathering. Here, we report the mineralogy of fine fraction of the Ryugu grains and a variation of their surface features related to space weathering.
T. Noguchi↗
Direct Measurement of the Composition of Aqueous Fluids from the Parent Body of Asteroid 162173 Ryugu
Imaging using X-ray absorption contrast by synchrotron nano-computed tomography (47.4 nm/voxel, 7keV) of a Ryugu pyrrhotite crystal (C0002-FC012-from the second touch-down site) revealed probable fluid inclusions (Fig. 1A,B) [1]. The inclusions were completely encapsuled in pyrrhotite, suggesting the fluids were trapped in the early stages of crystal growth, and filled with low-Z material. We performed Time-of Flight-Secondary Ion Mass Spectrometry (TOF-SIMS) depth profiling and high-resolution map-ping at -120°C to exposure and measure the composition of the trapped fluids in a frozen state.
M Zolensky↗
Isotopic Compositions of Noble Gases and Nitrogen in the Ryugu Samples Returned by Hayabusa2
In December 2014, the hayabusa2 spacecraft launched to visit the C-type asteroid (162173) Ryugu to bring back surface and subsurface materials to the Earth. The spacecraft arrived at Ryugu on June 27, 2018, and subsequently carried out two touchdowns (TDs) and sample collections. The 1st TD was carried out and collected surface samples, while the 2nd TD was done to collect the impact melt ejecta near the artificial crater made by the small carry-on Impactor operation in April 2019. Samples collected during the 1st and 2nd TDs were stored in Chamber A and C of the Hayabusa2 sample catcher, respectively. Our principal objective is to quantify the indigenous compositions of the Ryugu samples with as little terrestrial contamination as possible. Here we report the isotopic ratios and concentrations of noble gases and nitrogen in the Ryugu samples allocated to the Hayabusa2-initial-analysis-volatile team.
noble gas↗
Aqueous alteration of Cb-type asteroid Ryugu
The samples from the asteroid Ryugu, which returned to Earth in the winter of 2020 [1], were stored under pure Nitrogen conditions at the Extraterrestrial Materials Curation Center of ISAS. After basic description [2-3], they were distributed to six initial analysis teams in Japan in June 2021. The initial analysis "Stone" team, which was responsible for the analysis of coarse particles (>1 mm in size), consisted of about 150 scientists from Japan and abroad, and conducted a series of analyses We analyzed sixteen coarse Ryugu particles 1 ~ 8 mm in size: six from the 1st touch-down site and ten from the 2nd touch-down site. Individual coarse samples were cut by Xe-FIB or wire-saw to expose particular objects or textures to be exposed on the surface based on 3D structure and element distribution obtained by synchrotron X-ray CT analysis and XRF analysis, respectively. FE-SEM/EDS and FE-EPMA/WDS analysis were made on all polished sections. TEM observation of many FIB sections was made to see microstructures and to compare with carbonaceous chondrites. Many other analyses were carried out to characterize mineralogical and compositional properties and summary of the analysis procedures is described in [4]. X-ray CT analysis showed that all sixteen Ryugu particles are composed of fine-grained material, with no chondrules and CAIs larger than 100 μm in size. FE-EPMA observation showed that Ryugu samples are breccias, consisting of many small rock fragments of different compositions, lithologies, and histories. The most common lithology includes Mg-rich saponite and serpentine, dolomite, magnesite, hydroxyapatite, pyrrhotite, and magnetite as main constituents. The mineralogy of this major lithology supports the classification of Ryugu samples as CI chondrites, which experienced extensive aqueous alteration in Ryugu’s parent asteroid. Based on the obtained mineralogical properties, we performed chemical modeling of aqueous alteration of Ryugu’s parent asteroid [5]. Numerical simulations [6-8] to reproduce thermal history and impact-induced destruction of the Ryugu’s parent asteroid were also carried out using mineralogical and physical properties of the Ryugu samples. In the talk, I would like to explain the conditions of aqueous alteration occurred in the parent asteroid of Ryugu in order to show how the water in the asteroid changed the mineralogy and chemistry of the nebular dust.
T. Nakamura↗
Update on Measurement of the Composition of Ryugu Fluid Inclusions
Imaging using X-ray absorption contrast by synchrotron nano-computed tomography of a Ryugu pyrrhotite crystal (C0002-FC012 - from the second Hayabusa2 spacecraft touch-down site) revealed probable fluid inclusions in the center of a crystal of pyrrhotite, suggesting the parent fluids were trapped in the early stages of crystal growth on Ryugu’s parent asteroid. We previously described the performance of Time-of Flight-Secondary Ion Mass Spectrometry (TOF-SIMS) depth profiling and high-resolution mapping at -120°C to expose and measure the composition of the trapped fluids in a frozen state in two Ryugu inclusions [1,2]. Here we report results from follow-on measurements of additional inclusions in the same pyrrhotite crystal, and the initial results of measurement of standards. The ultimate goal is to reveal the quantitative composition of the fluids that caused aqueous alteration, in particular the H2O:CO2 ratio, which will also facilitate cosmochemical modeling of the alteration process.
M Zolensky↗
Analysis of "Stone" Samples from C-Type Asteroid Ryugu
As a part of activities of initial analysis, we analyzed eighteen Ryugu “stone” samples of 1 ~ 8mm in size: seven stones from the 1st touch down site and eleven from the 2nd touch down site. Ryugu stones were analyzed first using X-rays, UV, visible, near-infrared, mid-infrared, and muon probes for surface reflectance spectra, internal 3D structure and element distribution, crystal structures, and bulk composition of light elements such as C, N, and O. Measurements for magnetic, thermal, and physical properties using some stones were also performed. TOF-SIMS analysis of fluid inclusions as being continued. Small particles separated from some stones were analyzed by IR-CT. Based on 3D-CT images of individual stones, objects of interests were identified, separated by pFIB cutting, and exposed by polishing on the surface of epoxy disks. FE-EPMA/FE-SEM analysis was made on ~40 polished epoxy disks for chemical composition and textural observation. FIB sections and small (~15 μm in size) fragments were separated from polished surface and analyzed by TEM, STXM,XRF, and nano-CT.
T. Nakamura↗
Olivine Mineralogy of Asteroid Ryugu Samples and CI Chondrites: Further Evidence for their Common Origin
Initial analysis of asteroid Ryugu samples has revealed that they were mm-mm scale brecciamostly composed of aqueously altered phases (e.g., Mg-Fe phyllosilicates, carbonates) and showed remarkablesimilarities to CI chondrites in mineralogy and chemistry [e.g., 1,2]. Our detailed analysis of Ryugu samples hasdetected small amounts (<<1 vol.%) of unaltered silicates that would escape severe aqueous alteration [3]. Olivine isthe most abundant (>90 vol%) phase among such unaltered silicates. Although most Ryugu olivine grains aresmaller than 5 mm, they bear important information about the precursors of the parent Ryugu asteroid. In thisabstract we report additional results of olivine mineralogical study of Ryugu samples, and especially compare witholivine grains in CI chondrites (Ivuna and Orgueil) to further discuss their relationship and possible common origin.
T. Mikouchi↗
Shock-Induced Deformation Recorded in the Regolith Particles from C-Type Asteroid Ryugu
The Hayabusa 2 mission successfully returned with samples of C-type near-Earth asteroid (162173) Ryugu on December of 2020. Ryugu samples contain large quantities of volatiles such as water and noble gases. Studying Ryugu samples is a great opportunity to understand the shock metamorphism on water-bearing rubble-pile asteroids. In this study, we have examined shock metamorphism on sixteen coarse mm-sized particles recovered by the Hayabusa 2 mission.
M. Kikuiri↗