Functionally Graded Material Prepared by Microwave Induced Combustion Synthesis
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Microwave-Induced Combustion Synthesis↗
Engineering topics
Yiin, T.
Publications and source records attributed to Yiin, T..
(abstract) Microwave Induced Combustion Synthesis of Ceramic and Ceramic-Metal Composites
We have used microwaves to induce self-propagating high temperature synthesis (SHS) in the reaction 3TiO(sub 2)+3C+(4+x)Al ---> 3TiC+2Al(sub 2)O(sub 3)+xAl. The SHS process was studied for x = 0 and 4, with and without the application of uniaxial pressure. A TE102 microwave cavity mode internally ignited the samples using less than 50 watts. The resultant microstructure of the microwave processed samples were compared to SHS products obtained using a conventional hot wire ignition technique. Uniaxial stresses along the vertical axis of approximately 1400 and 200 psi were applied simultaneously as the SHS reactions were initiated in some of the conventional and microwave processed samples, respectively. SEM photomicrographs will be presented that show the different microstructural features of the products using the microwave and hot wire techniques.
ceramic microwave ceramic-metal composites microwa↗
Microwave Induced Combustion Synthesis of Ceramic and Ceramic-Metal Composites
In recent years, there has been a renewed interest in combustion synthesis reactions, commonly called self-propagating high-temperature synthesis. These reactions are an attractive, energy efficient approach to the synthesis of high temperature composite materials and metastable phases. Microwaves are used to induce self-propagating high temperature synthesis of ceramic and ceramic-metal composites.
high-temperature ceramics high-temperature synthes↗
Vibration Method for Tracking the Resonant Mode and Impedance of a Microwave Cavity
There has been a concerted effort to improve the microwave heating technique for processing materials at high temperature. Improved optimization of the energy transfer from a microwave source to the material being processed is required. A vibration technique is pre- sented to continuously maintain a mode resonance and impedance match between a constant frequency magnetron source and a resonant cavity.
microwave↗
Plasma Enhanced Microwave Joining
A new method for plasma enhanced microwave joining of high purity (99.8%) alumina has been developed. The controlled application of a plasma between the adjoining surfaces of two rods permits the initial heating of low microwave absorbing alumina to sufficiently high temperatures where they can effectively absorb microwave energy. With this technology, the adjacent surfaces of alumina rods can be melted and welded together in less than three minutes using approximately 400 watts of microwave energy. Four point bending tests measured fracture strengths of up to 132 MPa at the joined interface.
microwave↗
Vibration Method for Tracking the Resonant Mode and Impedance of a Microwave Cavity
A vibration technique his been developed to continuously maintain mode resonance and impedance much between a constant frequency magnetron source and resonant cavity. This method uses a vibrating metal rod to modulate the volume of the cavity in a manner equivalent to modulating an adjustable plunger. A similar vibrating metal rod attached to a stub tuner modulates the waveguide volume between the source and cavity. A phase sensitive detection scheme determines the optimum position of the adjustable plunger and stub turner during processing. The improved power transfer during the heating of a 99.8% pure alumina rod was demonstrated using this new technique. Temperature-time and reflected power-time heating curves are presented for the cases of no tracking, impedance tracker only, mode tracker only and simultaneous impedance and mode tracking. Controlled internal melting of an alumina rod near 2000 C using both tracking units was also demonstrated.
Barmatz, M.↗
Plasma Enhanced Microwave Joining
A new method for plasma enhanced microwave joining of high purity (99.8%) alumina has been developed. The controlled application of a plasma between the adjoining surfaces of two rods initially heats the microwave-low-absorbing alumina rods to temperatures high enough for them to absorb microwave energy efficiently. With this technology, the adjacent surfaces of alumina rods can be melted and welded together in less than three minutes using approximately 400 watts of microwave energy. Four point bending tests measured fracture strengths of up to 130 MPa at the joined interface. Optical and SEM micrographs indicated that exaggerated grain growth prevailed for all joints studied.
Yiin, T.↗
Conventional and Microwave Joining of Silicon Carbide Using Displacement Reactions
Microwave heating was used to join Silicon Carbide rods using a thin TiC /Si tape interlayer . Microwaves quickly heated the rods and tape to temperatures where solid-state displacement reactions between TiC and Si occurred.
Microwave heating↗
(abstract) Vibration Method for Tracking the Resonant Mode and Impedance of a Microwave Cavity
We have developed a vibration technique to continuously maintain mode resonance and impedance match between a constant frequency magnetron source and resonant cavity. This method uses a vibrating metal rod to modulate the volume of the cavity that is equivalent to modulating an adjustable plunger. A similar vibrating metal rod attached to a stub tuner modulates the waveguide volume between the source and cavity. A phase sensitive detection scheme determines the optimum position of the adjustable plunger and stub tuner. The improved power transfer during the heating of a 99.8% pure alumina rod was demonstrated using this new technique. Temperature-time and reflected power-time plotswill be presented for the cases of no tracking, impedance tracker only, mode tracker only, and simultaneous impedance and mode tracking. Internal melting of the alumina rod near 2000°C with both trackers on will also be discussed.
microwave↗