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Zepeda-Alarcon, Eloisa

Publications and source records attributed to Zepeda-Alarcon, Eloisa.

Optical Relays for Imaging Scintillators

Cygnus is a dual beam high-energy radiographic x-ray source. Ten years ago, three large zoom lenses were assembled to collect images from 200 mm x 200 mm square scintillators. The zoom capability allows zooming down to a 60 mm x 60 mm picture from the scintillator. Current radiographic imaging needs now require larger 270 mm x 270 mm square scintillators and the capability to use both 92 mm x 92 mm and 62 mm x 62 mm CCD cameras, and a new lens design to meet these needs. This zoom lens incorporates 11 elements and is designed to be telecentric. It images a scintillator emitting light peaking at 435 nm, so special glass types are required for the lens elements. Much larger elliptical pellicles are needed to deflect the scintillator light out of the x-ray path into the lens. The optical axis of the imaging system must be colinear with the x-ray axis. Two scintillators are positioned in each of two Cygnus x-ray axes, for a total of four scintillators and four lens systems. An optional configuration will be shown, enabling two lens systems imaging opposite sides of a single scintillator, for a total of four lenses and two scintillators. Although this configuration has advantages, it suffers from crosstalk. Care must be taken to analyze the anti-reflection coatings applied to all the elements in the imaging chain, including the CCD array and

62 RADIOLOGY AND NUCLEAR MEDICINE↗

Crystallographic texture formation in Fe-9wt%Si alloy during deformation and phase transition at high pressure

SUMMARY The seismic anisotropy of the Earth's solid inner core has been the topic of much research. It could be explained by the crystallographic preferred orientation (CPO) developing during convection. The likely phase is hexagonal close-packed iron (hcp), alloyed with nickel and some lighter elements. Here we use high energy synchrotron X-rays to study CPO in Fe-9wt%Si, uniaxially compressed in a diamond anvil cell in radial geometry. The experiments reveal that strong preferred orientation forms in the low-pressure body-centred cubic (bcc) phase that appears to be softer than pure iron. CPO is attributed to dominant {110}<111> slip. The onset of the bcc→hcp transition occurs at a pressure of ≈15 GPa, and the alloy remains in a two phase bcc + hcp state up to 40 GPa. The hcp phase forms first with a distinct {11$\bar{2}$0} maximum perpendicular to compression. Modelling shows that this is a transformation texture, which can be described by Burgers orientation relationship with variant selection. Experimental results suggest that bcc grains oriented with <100> parallel to compression transform into hcp first. The CPO of the hcp changes only slowly during further pressure and deviatoric stress increase at ambient temperature. After heating to 1600 K, a change in the hcp CPO is observed with alignment of (0001) planes perpendicular to compression that can be interpreted as dominant (0001)<11$\bar{2}$0> slip, combined with {10$\bar{1}$2}<$\bar{1}$011> mechanical twinning, which is similar to the deformation modes suggested previously for pure hcp iron at inner core conditions.

Vasin, Roman N.↗

Our teams design high-resolution MeV x-ray radiography systems for National security missions [Poster]

The NNSS has been at the forefront of custom high-fidelity x-ray/gamma radiographic imaging solutions that serve our national security for over five decades. Our radiography team utilizes expertise in physics modeling and analysis, along with optical, mechanical, and electrical design, in close collaboration with our customers, to develop imaging methods and capabilities that go beyond their needs. Conceptual designs are developed through R&D efforts to provide solutions for the specific problem at hand. Field systems are designed and built in-house, then qualified utilizing a range of facilities across the National Security Enterprise. Radiographic imaging systems are deployed by our team in the most challenging environments. The NNSS has a strong math and programming team that provides novel on-site image analysis methods that extract crucial information from data returned in field tests.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Crystal plasticity modeling of strain-induced martensitic transformations to predict strain rate and temperature sensitive behavior of 304 L steels: Applications to tension, compression, torsion, and impact

This paper advances crystallographically-based Olson-Cohen (direct γ → α’) and deformation mechanism (indirect γ→ε→α’) phase transformation models for predicting strain-induced austenite to martensite transformation. Here, the advanced transformation models enable predictions of not only strain-path sensitive, but also of strain-rate and temperature sensitive deformation of polycrystalline stainless steels (SSs). The deformation of constituent grains in SSs is modeled as a combination of anisotropic elasticity, crystallographic slip, and phase transformation, while the hardening is based on the evolution of dislocation density and explicit shifts in phase fractions. Such grain-scale deformation is implemented within the meso-scale elasto-plastic self-consistent (EPSC) homogenization model, which is coupled with the implicit finite element (FE) method to provide a constitutive response at each FE integration point for solving boundary value problems at the macro-scale. Parameters pertaining to the hardening and transformation models within FEEPSC are calibrated and validated on a suite of data including flow curves and phase fractions for monotonic compression, tension, and torsion as a function of strain-rate and temperature for wrought and additively manufactured (AM) SS304L. To illustrate the potential and accuracy of the integrated multi-level FE-EPSC simulation framework, geometry, mechanical response, phase fractions, and texture evolution are simulated during gas-gun impact deformation of a cylinder and quasi-static tension of a notched specimen made of AM SS304L. Details of the simulation framework, comparison between experimental and simulation results, and insights from the results are presented and discussed.

304L steels↗

Assessment of the Imaging Properties of Plastic Scintillators at FP60R for Neutron Imaging Applications [Slides]

4mm thick Stilbene gives the brightest signal but at the cost of resolution. 1 and 2 cm BC412 gave the highest resolution images. The HI-LY scintillator is better suited for DD neutrons. Future work includes: measurements this summer using an event-mode imaging camera which promises sub-pixel resolution through center-of-mass techniques, opportunities for DD neutron tests during laser-driven z-pinch experiments at UNR, and assess scatter within scintillator.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

New Optical Designs for Radiation Imaging Systems [Slides]

Presentation to be presented during the first annual Prompt Radiation Detection and Imaging Workshop, hosted by the NNSS Dynamic Instruments Team, April 25–28, 2022, at NLV C-01 Auditorium and via Webex.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Neutron Imaging at LANSCE

Presentation for the 1st Annual Prompt Radiation Detection and Imaging Workshop at NLV.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Combining visible shadowgraph imaging with x-ray imaging for dynamic shock experiments

Interrogating ejecta particles launched from target materials that are undergoing dynamic shock can be done with both x-ray imaging and visible shadowgraph imaging. Our dynamic testing must be done inside a containment vessel with limited access ports available. We designed an imaging system to relay both types of imaging systems through a single port using the same optical relay and then splitting the images onto three separate high-speed imaging cameras outside the containment vessel. X-ray imaging provides ejecta density measurements. Shadowgraph imaging that is done at two wavelengths (blue and red) constrains ejecta particle size distributions and provides areal density measurements of the ejecta cloud. The ejecta particles are positioned 225 mm before the x-ray scintillators; this arrangement permits a folded mirror system to allow the shadowgraph data to bypass the x-ray scintillators. This configuration results in spatial separations between the intermediate image planes of the x-ray and shadowgraph images along the optical axis. At the position of the x-ray intermediate image plane, mirrors are positioned such that the shadowgraph images are kicked out and their images are sent on to different cameras. Positioning of the large doublet relay lenses keeps shrapnel from impacting the vessel containment windows.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Radioactive Material Dynamics @ NSLS-II [Slides]

RMD @ NSLS-II helps pave the path to a DMMSC: Developing expertise in techniques and experimental methods for DMMSC science; Improving capabilities for models to become microstructurally aware; Workforce training and development; Help refine DMMSC scientific requirements; Complementary to DMMSC XFEL science (EDXD/EXAFS)

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Deformation heterogeneity and intragrain lattice misorientation in high strength contrast, dual-phase bridgmanite/periclase

A bridgmanite/periclase aggregate is investigated due to its prevalence in the Earth’s lower mantle and its importance for understanding geodynamic processes. In dual-phase polycrystalline aggregates, both strength contrast between phases and single crystal elastic and plastic anisotropy are known to influence the development of intragrain misorientation, and the evolution of crystallographic texture. In this study, full-field crystal plasticity simulations are performed with a finite element solution method, and applied to an aggregate of a mechanically strong orthorhombic phase with perovskite structure (bridgmanite, MgSiO 3 ), and a relatively weaker cubic phase (periclase, MgO). The relative strengths of the phases are parameterized to elucidate the effect that strength contrast has on texture evolution and single-phase simulations are performed for comparison. Altogether, results indicate that the relative strength between the two phases influences the development of plasticity, and the overall texture evolution. Results are discussed in light of trends related to the evolution of plasticity and misorientation in the aggregate, and their dependence on both the strength contrast between phases as well as the spatial distribution of grains and phases.

36 MATERIALS SCIENCE↗