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Explore NASA and DOE materials research. Search alloys, composites and material properties, then open the original technical report for test conditions and results.

At least 1,567 records · Page 87

Investigation of the effects of NaOH dopant level on the physical and mechanical properties of carbon/phenolic composite material

The near-catastrophic erosion of the STS-8A solid rocket booster nozzle was the instigating factor in the recent, and on-going, intensive investigation of carbon/phenolic composite materials. Much of this effort has been focused on the effect of sodium contamination on the carbon fibers. It is known that sodium acts as a catalyst in the oxidation of the fibers at elevated temperatures. A study was undertaken to determine what changes were caused by variation in sodium content. Investigations were conducted in three areas: (1) phenolic resin; (2) carbon/phenolic prepreg; and (3) cured laminates. Due to the exploratory nature of the studies, a variety of tests in addition to those normally run in production facilities were considered. The experimental methodologies and results of these experiments are discussed, and recommendations for improving techniques and extending the research program are presented.

Clinton, R. G., Jr.↗

NASA/aircraft industry standard specification for graphite fiber toughened thermoset resin composite material

A standard specification for a selected class of graphite fiber/toughened thermoset resin matrix material was developed through joint NASA/Aircraft Industry effort. This specification was compiled to provide uniform requirements and tests for qualifying prepreg systems and for acceptance of prepreg batches. The specification applies specifically to a class of composite prepreg consisting of unidirectional graphite fibers impregnated with a toughened thermoset resin that produce laminates with service temperatures from -65 F to 200 F when cured at temperatures below or equal to 350 F. The specified prepreg has a fiber areal weight of 145 g sq m. The specified tests are limited to those required to set minimum standards for the uncured prepreg and cured laminates, and are not intended to provide design allowable properties.

Source record↗

Long-term thermal aging of Celion/V378A composite materials

Celion 6000/V378A graphite/bismaleimide composite materials were aged in air at temperatures of 177, 204, 232 and 260 deg C for various times up to 15,000 hours. Three unidirectional specimen types were aged: short beam shear (SBS), flexure, and 153 mm square panels. Aged specimens of V378A laminates exhibited excellent thermal stability. Extensive cracking was observed during aging on the 0 deg edges of the unidirectional laminates. These cracks penetrated as deep as 12 mm from the edge. The cracking appeared to have little or no effect on the observed properties of the laminates. The study indicates that the useful life of unrestrained unidirectional graphite/V378A laminates is 10,000 hours or greater at 177 C to 232 C and 2,000 to 2,000 hour at 260 C.

Nelson, J. B.↗

Factors influencing the ultrasonic stress wave factor evaluation of composite material structures

To demonstrate that the finite-element model can be used to investigate some of the factors influencing the ultrasonic stress wave evaluation of materials, a hypothetical case was studied in which classical vibration theory was used. Vibration analysis and experiments for the undamaged case were conducted on an isotropic aluminum plate and a unidirectional graphite-epoxy plate, using a point source to excite the plates. The finite-element solution correlated within eight percent with the exact method. The frequencies predicted by the finite-element model were observed in the experiments in both plates, although in the composite plate, additional frequencies were observed which could not be accounted for. Damaged isotropic plates were also considered. The effects of increasing damage severity with constant damage area, and increasing damage area with constant severity on the resonant frequencies were analyzed.

Rebello, C. J.↗

A three dimensional calculation of elastic equilibrium for composite materials

A compact scheme is applied to three-dimensional elasticity problems for composite materials, involving simple geometries. The mathematical aspects of this approach are discussed, in particular the iteration method. A vector processor code implementing the compact scheme is presented, and several numerical experiments are summarized.

Lustman, Liviu R.↗

Contribution to the study of composite materials and their damage

Chapter 1 describes the homogenization techniques used for defining the overall behavior of composite materials for conventional cases of linear and perfectly glued elastic constituents. Chapters 2 and 3 focus on solving the problems inherent in two types of degenerated situations: elastic media with microcavities, and elastic media containing rigid inclusions. Through suitable definitions of deformation concepts and macroscopic stresses it is shown that conventional theory results apply naturally to these limits.

Lene, F.↗

The role of damage-softened material behavior in the fracture of composites and adhesives

The failure mechanism of polymer composites and adhesives with high strain in the zone near and ahead of the crack tip is investigated analytically, summarizing the findings of Ungsuwarungsri (1986). A double-cantilever-beam specimen with the nonlinear material confined to a thin strip between two wedge-loaded elastic beams is modeled as a beam on a nonlinear foundation; the two-point boundary-value problem for stationary and propagating cracks is solved numerically; and an FEM approach is applied to study the behavior of the nonlinear strip in detail. Typical results are presented in extensive graphs, and the accuracy and efficiency of the present method are shown to be superior to those of the Berry (1963) procedure.

Ungsuwarungsri, T.↗

A three dimensional calculation of elastic equilibrium for composite materials

A compact scheme is applied to three-dimensional elasticity problems for composite materials, involving simple geometries. The mathematical aspects of this approach are discussed, in particular the iteration method. A vector processor code implementing the compact scheme is presented, and several numerical experiments are summarized.

Lustman, Liviu R.↗

The strength of laminated composite materials under repeated impact loading

When low velocity and energy impact is exerted on a laminated composite material, in a perpendicular direction to the plane of the laminate, invisible damage may develop. It is shown analytically and experimentally that the invisible damage occurs during the first stage of contact between the impactor and the laminate and is a result of the contact stresses. However, the residual flexural strength changes only slightly, because it depends mainly on the outer layers, and these remain undamaged. Repeated impact intensifies the damage inside the laminate and causes larger bending under equivalent impact load. Finally, when the damage is most severe, even though it is still invisible, the laminate fails because of bending on the tension side. If the repeated impact is halted before final fracture occurs the residual strength and modulus would decrease by a certain amount.

Rotem, Assa↗

Optical properties of sputtered aluminum on graphite/epoxy composite material

Solar absorptance, emittance, and coating thickness were measured for a range of coating thicknesses from about 400 A to 2500 A. The coatings were sputtered from an aluminum target onto 1-inch-diameter substrates of T300/5209 graphite/epoxy composite material with two different surface textures. Solar absorptance and emittance values for the specimens with the smooth surface finish were lower than those for the specimens with the rough surface finish. The ratio of solar absorptance to emittance was higher for the smooth specimens, increasing from 2 to 4 over the coating thickness range, than for the rough ones, which had a constant ratio of about 1. The solar absorptance and emittance values were dependent on the thickness of the sputtered coating.

Witte, William G., Jr.↗

Nondestructive evaluation/characterization of composite materials and structures using the acousto-ultrasonic techniques

This paper introduces the nature and the underlying rational of the acousto-ultrasonic stress wave factor technique and some of its applications to composite materials and structures. Furthermore, two examples of successful application of the acousto-ultrasonic technique are presented in detail. In the first example, the acousto-ultrasonic technique is used to evaluate the adhesive bond strength between rubber layers and steel plates, and in the seocnd example the tehcnique is used to monitor progressive damage in wire rope.

Dos Reis, H. L. M.↗

Techniques for measurement of the thermal expansion of advanced composite materials

Techniques available to measure small thermal displacements in flat laminates and structural tubular elements of advanced composite materials are described. Emphasis is placed on laser interferometry and the laser interferometric dilatometer system used at the National Aeronautics and Space Administration (NASA) Langley Research Center. Thermal expansion data are presented for graphite-fiber reinforced 6061 and 2024 aluminum laminates and for graphite fiber reinforced AZ91 C and QH21 A magnesium laminates before and after processing to minimize or eliminate thermal strain hysteresis. Data are also presented on the effects of reinforcement volume content on thermal expansion of silicon-carbide whisker and particulate reinforced aluminum.

Tompkins, Stephen S.↗

Thermal-vacuum effects on polymer matrix composite materials

Results are presented on the thermal-vacuum response of a variety of fiber reinforced polymers matrix composites that comprised the UTIAS experiment on the LDEF satellite. Theoretical temperature-time predictions for this experiment are in excellent agreement with test data. Results also show quite clearly the effect of outgassing in the dimensional changes of these materials and the corresponding coefficients of thermal expansion. Finally, comparison with ground-based simulation tests are presented as well. Use of these data for design purposes are also given.

Tennyson, R. C.↗

The Iosipescu shear test method as used for testing polymers and composite materials

This paper describes a shear test method for polymers and composite materials, based on the Iosipescu (1967) shear test which was originally developed for use with homogeneous isotropic metals. Special attention is given to the loading fixture for the test, the standard specimen design and shear stress measurements. The range of the test applications is indicated. The method is in the final stages of being accepted as an ASTM standard.

Adams, Donald F.↗

Computational simulation of the creep-rupture process in filamentary composite materials

A computational simulation of the internal damage accumulation which causes the creep-rupture phenomenon in filamentary composite materials is developed. The creep-rupture process involves complex interactions between several damage mechanisms. A statistically-based computational simulation using a time-differencing approach is employed to model these progressive interactions. The finite element method is used to calculate the internal stresses. The fibers are modeled as a series of bar elements which are connected transversely by matrix elements. Flaws are distributed randomly throughout the elements in the model. Load is applied, and the properties of the individual elements are updated at the end of each time step as a function of the stress history. The simulation is continued until failure occurs. Several cases, with different initial flaw dispersions, are run to establish a statistical distribution of the time-to-failure. The calculations are performed on a supercomputer. The simulation results compare favorably with the results of creep-rupture experiments conducted at the Lawrence Livermore National Laboratory.

Slattery, Kerry T.↗

The interstellar C-H stretching band near 3.4 microns - Constraints on the composition of organic material in the diffuse interstellar medium

The composition and history of dust in the diffuse ISM was studied using 3600-2700/cm absorption spectra of objects which have widely varying amounts of visual extinctions along different lines of sight. The 3300/cm and 2950/cm features are attributed to O-H and C-H stretching vibrations, respectively. The O-H feature in OH 32.8-0.3 is suggestive of circumstellar water ice and is probably not due to material in the diffuse ISM. The features in the 3100-2700/cm region are attributed either to C-H vibrations or to M stars. The spectra of the latter show a series of narrow features in this region that are identified with photospheric OH. Objects in which these bands are seen include OH 01-477, T629-5, and the Galactic center source IRS 7. The C-H stretch feature of diffuse ISM dust has subpeaks which fall within 5/cm of C-H stretching vibrations in the -CH2- and -CH3 groups of saturated aliphatic hydrocarbons.

Sandford, S. A.↗