DOE OSTI · 1925138
Formation of high quality alane
Abstract
Methods for forming alane are described. The method includes addition of toluene at a temperature above the crystallization temperature of alane to a lower temperature solution that includes alane adduct, ether, and toluene. Upon the addition, a crystallization mixture is formed that is at or near the crystallization temperature of alane. The alane of the mixture crystallizes over a period of time to form a high purity alane polymorph.
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Zidan, Ragaiy, McWhorter, Christopher S., Ward, Patrick A.. 2022-09-27. Formation of high quality alane. https://www.osti.gov/biblio/1925138
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