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DOE OSTI · 22262710

Automatic sample Dewar for MX beam-line

Charignon, T.·Tanchon, J.·Trollier, T.·Ravex, A.·Theveneau, P.
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Abstract

It is very common for crystals of large biological macromolecules to show considerable variation in quality of their diffraction. In order to increase the number of samples that are tested for diffraction quality before any full data collections at the ESRF*, an automatic sample Dewar has been implemented. Conception and performances of the Dewar are reported in this paper. The automatic sample Dewar has 240 samples capability with automatic loading/unloading ports. The storing Dewar is capable to work with robots and it can be integrated in a full automatic MX** beam-line. The samples are positioned in the front of the loading/unloading ports with and automatic rotating plate. A view port has been implemented for data matrix camera reading on each sample loaded in the Dewar. At last, the Dewar is insulated with polyurethane foam that keeps the liquid nitrogen consumption below 1.6 L/h. At last, the static insulation also makes vacuum equipment and maintenance unnecessary. This Dewar will be useful for increasing the number of samples tested in synchrotrons.

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46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICSBEAMSCRYSTALSDIFFRACTIONEUROPEAN SYNCHROTRON RADIATION FACILITYLOADINGPOLYURETHANESROBOTSSYNCHROTRONSUNLOADING

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Charignon, T., Tanchon, J., Trollier, T., Ravex, A., Theveneau, P.. 2014-01-29. Automatic sample Dewar for MX beam-line. https://doi.org/10.1063/1.4860689

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