Search NASA⌕ Search

DOE OSTI · 2560808

Automated Image Segmentation and Processing Pipeline Applied to X–Ray Computed Tomography Studies of Pitting Corrosion in Aluminum Wires

Abstract

Understanding pitting corrosion is critical, yet its kinetics and morphology remain challenging to study from X-ray computed tomography (XCT) due to manual segmentation barriers. To address this, an automated pipeline leveraging deep learning for efficient large-scale XCT analysis is developed, revealing new corrosion insights. The pipeline enables pit segmentation, 3D reconstruction, statistical characterization, and a topological transformation for visualization. Here, the pipeline is applied to 87 648 XCT images capturing commercial purity aluminum (1100 Al) wire exposed to sodium chloride (NaCl) salt particles over a period of 122 h. The pipeline achieves complete feature extraction and statistical quantification across the entire XCT dataset, leveraging distributed computing environment for high efficiency. Global growth kinetics such as high-level stepwise sigmoidal volume loss patterns and granular individual pit developments are both captured for 36 detected pits. By combining automation, computer vision, and extensive XCT datasets, this research accelerates precise corrosion assessment to enable materials science discoveries at scale.

Explore related subjects

Keep this discovery

Explore connections, maps & timelines

BibTeXRIS

Kalutotage, Maliesha S. [Case Western Reserve University, Cleveland, OH (United States)] (ORCID:0009000964408180), Ciardi, Thomas G. [Case Western Reserve University, Cleveland, OH (United States)] (ORCID:0009000609422666), Tripathi, Pawan K. [Case Western Reserve University, Cleveland, OH (United States)] (ORCID:0000000286047744), Huang, Liangyi [Case Western Reserve University, Cleveland, OH (United States)], Jimenez, Jayvic Cristian [Case Western Reserve University, Cleveland, OH (United States)] (ORCID:0000000223425648), Noell, Philip J. [Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)], Bruckman, Laura S. [Case Western Reserve University, Cleveland, OH (United States)] (ORCID:0000000312711072), French, Roger H. [Case Western Reserve University, Cleveland, OH (United States)] (ORCID:0000000261620532), Sehirlioglu, Alp [Case Western Reserve University, Cleveland, OH (United States)] (ORCID:0000000297084049). 2025-01-13. Automated Image Segmentation and Processing Pipeline Applied to X–Ray Computed Tomography Studies of Pitting Corrosion in Aluminum Wires. https://doi.org/10.1002/adem.202401699

Cite the original work for its findings. Save a collection to share your selection of sources.

KEEP EXPLORING

Related reports

Cyclic moisture reactivation of calcium sorbents for long duration thermochemical energy storage

The transition to a flexible and reliable energy infrastructure, using electro-thermal energy generation technologies such as geothermal, concentrated solar power, and nuclear, usually demands simultaneous advancement of thermal energy storage (TES) to support on-demand electricity generation and industrial applications while mitigating the inherent intermittency of renewable energy sources and power outages from direct energy generation. Among TES technologies, thermochemical energy storage (TCES) based on calcium looping emerges as a compelling high-power energy storage candidate due to its high reaction enthalpy, compatibility with elevated operating temperatures, and abundance of low-cost materials. However, the long-term durability of calcium-based sorbents for TCES is hindered by surface sintering and particle aggregation, leading to performance degradation over repeated thermal cycles. This study explores a moisture hydration-based strategy to regenerate a degraded calcium sorbent and mitigate performance degradation for long duration TCES. The addition of moisture transforms calcium oxide into calcium hydroxide and produces intercalation water layers, associated with a regenerated surface area and reduced calcium oxide crystallite size. Both these effects are beneficial in restoring the sorbents' reactivity for carbonization. Additionally, an optimized hydration-assisted reactivation protocol balances the recovered energy storage capacity with heating penalty required for moisture removal from hydrated samples, resulting in an enhanced energy storage capacity up to 176% compared to benchmark sorbents that undergo cycling without reactivation after 60 cycles. In conclusion, these results highlight the potential of hydration-assisted reactivation to enhance the long-term performance of TCES, providing an effective pathway to advancing electro-thermal storage technologies.

36 MATERIALS SCIENCE↗