Temporal Study 2022-2024: Sample-Based Surface Water Dissolved Inorganic Carbon, Dissolved Organic Carbon, Total Nitrogen, Stable Isotopes, and Total Suspended Solids from across Multiple Watersheds in the Yakima River Basin, Washington, USA

Garayburu-Caruso, Vanessa A. [Pacific Northwest National Laboratory] (ORCID:0000000333836237); Bakker, Erica A. H. [Washington State University] (ORCID:000000015595079X); Butler, Zachariah [Oregon State University] (ORCID:0009000708837103); Chen, Xingyuan [Pacific Northwest National Laboratory] (ORCID:0000000319285555); Cornwell, Kali [Pacific Northwest National Laboratory]; Delgado, Dillman [Pacific Northwest National Laboratory] (ORCID:0000000166526775); Forbes, Brieanne [Pacific Northwest National Laboratory] (ORCID:0000000192409687); Goldman, Amy E. [Pacific Northwest National Laboratory] (ORCID:0000000304906451); Grieger, Samantha [Pacific Northwest National Laboratory] (ORCID:0000000160001951); Kaufman, Matthew H. [Pacific Northwest National Laboratory] (ORCID:0000000314988219); Laan, Maggi [Pacific Northwest National Laboratory] (ORCID:0000000202563822); McKever, Sophia A. [Pacific Northwest National Laboratory] (ORCID:0000000328707713); Myers-Pigg, Allison N. [Pacific Northwest National Laboratory] (ORCID:0000000269056841); Otenburg, Opal [Pacific Northwest National Laboratory]; Renteria, Lupita [Pacific Northwest National Laboratory] (ORCID:0000000150355924); Scheibe, Timothy D. [Pacific Northwest National Laboratory] (ORCID:0000000288645772); Torgeson, Joshua M. [Pacific Northwest National Laboratory] (ORCID:0000000224892248); Stegen, James C. [Pacific Northwest National Laboratory] (ORCID:0000000191357424)

doi:10.15485/2562910

DOE OSTI · 2562910

Temporal Study 2022-2024: Sample-Based Surface Water Dissolved Inorganic Carbon, Dissolved Organic Carbon, Total Nitrogen, Stable Isotopes, and Total Suspended Solids from across Multiple Watersheds in the Yakima River Basin, Washington, USA

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Abstract

This dataset supports a broader study examining the drivers of temporal variability in sediment respiration rates in the Yakima River Basin. The dataset provides geochemistry data generated from samples collected at bi-weekly or monthly intervals at six sites across the Yakima River Basin in Washington, USA. Sample and sensor data from previous years (2021-2022) can be found at https://data.ess-dive.lbl.gov/datasets/doi:10.15485/1898912 and https://data.ess-dive.lbl.gov/datasets/doi:10.15485/1892054, respectively. Related sensor data from 2022-2024 will be published separately. This dataset is comprised of one main data folder containing (1) file-level metadata; (2) data dictionary; (3) readme; (4) field metadata; (5) dissolved inorganic carbon (DIC) and averages; (6) dissolved organic carbon (DOC; reported as non-purgeable organic carbon; NPOC) and averages; (7) total dissolved nitrogen (TN) and averages; (8) total suspended solids (TSS); (9) stable isotopes; (10) surface water sampling protocol; (11) sensor protocol; (12) methods codes; and (13) international generic sample number (IGSN) mapping file. All files are .csv or .pdf. For details on how to navigate data packages generated by this project, see https://data.ess-dive.lbl.gov/portals/PNNLRiverCorridorSFA/About. For data and scripts associated with "Shifts in rain-snow partitioning drive faster water transit times in the US Pacific Northwest" (Butler et al., 2026), go to https://data.ess-dive.lbl.gov/datasets/doi:10.15485/3025481

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18-O 2-H 54 ENVIRONMENTAL SCIENCES Biogeochemistry Canopy cover Deuterium DIC Dissolved inorganic carbon Dissolved organic carbon DOC EARTH SCIENCE > TERRESTRIAL HYDROSPHERE > SURFACE WATER EARTH SCIENCE > TERRESTRIAL HYDROSPHERE > SURFACE WATER > SURFACE WATER CHEMISTRY EARTH SCIENCE > TERRESTRIAL HYDROSPHERE > WATER QUALITY/WATER CHEMISTRY > ISOTOPES > STABLE ISOTOPES EARTH SCIENCE > TERRESTRIAL HYDROSPHERE > WATER QUALITY/WATER CHEMISTRY > SOLIDS > SUSPENDED SOLIDS ESS-DIVE CSV File Formatting Guidelines Reporting Format ESS-DIVE File Level Metadata Reporting Format ESS-DIVE Location Metadata Reporting Format ESS-DIVE Sample ID and Metadata Reporting Format ESS-DIVE Water-Soil-Sediment Chemistry Reporting Format Freshwater Hydrobiogeochemical function Macrophyte cover Metabolite Metabolomics Microbiology Non-purgeable organic carbon NPOC River River corridor Stream Stream metabolism TN Total dissolved nitrogen Total suspended solids TSS Vegetation Watershed

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Garayburu-Caruso, Vanessa A. [Pacific Northwest National Laboratory] (ORCID:0000000333836237), Bakker, Erica A. H. [Washington State University] (ORCID:000000015595079X), Butler, Zachariah [Oregon State University] (ORCID:0009000708837103), Chen, Xingyuan [Pacific Northwest National Laboratory] (ORCID:0000000319285555), Cornwell, Kali [Pacific Northwest National Laboratory], Delgado, Dillman [Pacific Northwest National Laboratory] (ORCID:0000000166526775), Forbes, Brieanne [Pacific Northwest National Laboratory] (ORCID:0000000192409687), Goldman, Amy E. [Pacific Northwest National Laboratory] (ORCID:0000000304906451), Grieger, Samantha [Pacific Northwest National Laboratory] (ORCID:0000000160001951), Kaufman, Matthew H. [Pacific Northwest National Laboratory] (ORCID:0000000314988219), Laan, Maggi [Pacific Northwest National Laboratory] (ORCID:0000000202563822), McKever, Sophia A. [Pacific Northwest National Laboratory] (ORCID:0000000328707713), Myers-Pigg, Allison N. [Pacific Northwest National Laboratory] (ORCID:0000000269056841), Otenburg, Opal [Pacific Northwest National Laboratory], Renteria, Lupita [Pacific Northwest National Laboratory] (ORCID:0000000150355924), Scheibe, Timothy D. [Pacific Northwest National Laboratory] (ORCID:0000000288645772), Torgeson, Joshua M. [Pacific Northwest National Laboratory] (ORCID:0000000224892248), Stegen, James C. [Pacific Northwest National Laboratory] (ORCID:0000000191357424). 2025-04-18. Temporal Study 2022-2024: Sample-Based Surface Water Dissolved Inorganic Carbon, Dissolved Organic Carbon, Total Nitrogen, Stable Isotopes, and Total Suspended Solids from across Multiple Watersheds in the Yakima River Basin, Washington, USA. https://doi.org/10.15485/2562910

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DOE OSTI2020

WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Surface Water FTICR-MS, NPOC, TN, Anions, Stable Isotopes, Bacterial Abundance, and Dissolved Inorganic Carbon (v8)

The WHONDRS Summer 2019 Sampling (S19S) Campaign collected samples in 97 globally distributed river corridor systems between July and September 2019. Surficial streambed sediments were collected at three locations within each site (upstream, midstream, and downstream). Surface water was collected at the downstream site. This dataset includes a portion of the data types produced from the surface water samples and does not include any results from the sediment. Sediment data can be found at https://data.ess-dive.lbl.gov/view/doi:10.15485/1729719. The S19S campaign was designed with the science community to ask questions associated with links among core/transient metabolomes, microbial metabolism, biogeochemical function, and physical properties of watershed and river corridor systems. This data package was originally published in March 2020. It was updated in October 2020 (v2, new and modified files), July 2021 (v3, new and modified files), January 2023 (v4, new and modified files), February 2023 (v5, new and modified files), August 2023 (v6, new and modified files), July 2025 (v7,new and modified files), and August 2026 (v8, new and modified files). Version 8 includes major restructuring of the files and their formats. See the change history section in readme for more details. In addition to a readme, this data package also includes a file-level metadata (FLMD) file that describes each file and a data dictionary (DD) that describes all column/row headers and variable definitions. This dataset contains (1) readme, (2) data dictionary, (3) file level metadata, (4) sampling protocol, (5) a data checks report, (6) field metadata, (7) international generic sample number (IGSN) mapping file, (8) joint genome institute (JGI) mapping file, and (9) a folder of sample data. The sample data folder contains (1) dissolved organic carbon (DOC, measured as non-purgeable organic carbon, NPOC) and FTICR methods, (2) dissolved inorganic carbon (DIC), (3) stable water isotopes (O and H), (4) specific conductivity, (5) total dissolved nitrogen (TN), (6) anions, (7) flow cytometry bacterial abundance data, (8) laboratory methods, and (9) a folder containing unaligned, peak-picked high resolution characterization of dissolved organic matter from sediment via 12 Tesla Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) through the Environmental Molecular Sciences Laboratory (EMSL, https://www.pnnl.gov/environmental-molecular-sciences-laboratory), and (12) a folder containing processed FTICR-MS data. All files are .msa, .txt, .spx, .xml, .csv, .pdf, .txt, .html, .jpg, or .jpeg.

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WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Surface Water FTICR-MS, NPOC, TN, Anions, Stable Isotopes, Bacterial Abundance, and Dissolved Inorganic Carbon (v8)