DOE OSTI · 2571695
Extrusion‐Spheronization of Mock Energetic Materials
Abstract
The primary method for producing plastic bonded explosive (PBX) granules, or “prills”, has remained relatively unchanged for 70 years despite the complex nature of the process. In this work, we demonstrate the feasibility of using an extrusion‐spheronization technique to produce prills for PBX applications. We begin by detailing an inert formulation with similar properties of PBXs and then demonstrate the extrusion‐spheronization processing of these materials. A study is then performed where the spheronization process time of the extruded materials is varied and the resultant prills are morphologically characterized. Further, these prills are then pressed into high‐density articles and subject to compression testing to elucidate trends in process, properties, and performance. It was found that, for our formulation (95 wt.% melamine/5 wt.% polymer binder) and process, a spheronization time of 60 s yielded relatively uniform particles that exhibited improved poured, tapped, and pressed densities. Mechanical strength did not have a strong trend with process time as all spheronized materials had similar peak compression stress at failure. After further optimization, extrusion‐spheronization may be a promising path for future PBX formulation.
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Kline, Dylan J. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Sevcik, Max J. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States); Colorado School of Mines, Golden, CO (United States)], Villena, Matthew F. L. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Escobar, Aholibama [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Newton, Deirdre K. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Dobbs, Alexandra A. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States); Georgia Institute of Technology, Atlanta, GA (United States)], Gamez, Isabel A. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Zaka, Fowzia [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Goff, Aaron S. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Penczek, Evan [Colorado School of Mines, Golden, CO (United States)], Brettmann, Blair K. [Georgia Institute of Technology, Atlanta, GA (United States)], Martinez, H. Paul [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)], Eliasson, Veronica [Colorado School of Mines, Golden, CO (United States)], Sullivan, Kyle T. [Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)]. 2025-06-24. Extrusion‐Spheronization of Mock Energetic Materials. https://doi.org/10.1002/prep.70008
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