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DOE OSTI · 3367239

Gepta-EX: a multi-channel germanium detector for X-ray absorption fine structure

Abstract

Fluorescence-mode X-ray absorption spectroscopy (XAS) at high photon energies requires detectors with high stopping power and excellent energy resolution to measure weak element-specific signals. Traditional silicon-based detectors suffer from poor efficiency above ∼20 keV, while most high-Z materials such as cadmium telluride, cadmium zinc telluride, and gallium arsenide have focused predominantly on imaging applications with limited spectroscopic resolution. In contrast, germanium combines excellent stopping power with superior intrinsic energy resolution due to its low Fano factor and favorable charge transport properties, making it ideal for high-resolution spectroscopy in the 15 keV to 100 keV range. To address these requirements, we report on the development, fabrication, and performance evaluation of Gepta-EX, a compact multi-channel high-purity germanium (HPGe) detector system for fluorescence-mode XAS. The Gepta-EX system features a monolithic seven-channel HPGe pixel array integrated with low-noise CUBE charge-sensitive preamplifiers, housed within a thermally isolated compact cryostat operating near 90 K. The detector achieves energy resolutions of 218 eV at 5.9 keV (from a 55 Fe source) and 373 eV at 59.5 keV (from a 241 Am source), with uniform performance across all channels. By avoiding the escape peak interference commonly associated with silicon detectors and providing stable, high-resolution performance, Gepta-EX represents a powerful tool for high-energy X-ray spectroscopy.

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BibTeXRIS

Rumaiz, Abdul K. [Brookhaven National Laboratory (BNL), Upton, NY (United States). National Synchrotron Light Source II (NSLS-II)] (ORCID:000000029907299X), Capocasa, Francesca [Brookhaven National Laboratory (BNL), Upton, NY (United States). Instrumentation Department] (ORCID:0009000444031797), Kuczewski, Anthony J. [Brookhaven National Laboratory (BNL), Upton, NY (United States). National Synchrotron Light Source II (NSLS-II)] (ORCID:0009000305665298), Pinaroli, Giovanni [Brookhaven National Laboratory (BNL), Upton, NY (United States). Instrumentation Department] (ORCID:0009000065698145), Krings, Thomas [Forschungszentrum Juelich (Germany)] (ORCID:0000000222127948), Ravel, Bruce [National Inst. of Standards and Technology (NIST), Gaithersburg, MD (United States)] (ORCID:000000024126872X), Siddons, D. Peter [Brookhaven National Laboratory (BNL), Upton, NY (United States). National Synchrotron Light Source II (NSLS-II)] (ORCID:0000000314829867). 2026-05-21. Gepta-EX: a multi-channel germanium detector for X-ray absorption fine structure. https://doi.org/10.1107/s1600577526004261

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36 MATERIALS SCIENCE↗