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DOE OSTI · 3367488

Microstructural evolution, defect mitigation, and precipitation behavior in AA6061 via laser powder bed fusion with high-temperature substrate heating

Abstract

Defects, particularly solidification cracking, remain persistent challenges in the laser powder bed fusion (LPBF) processing of AA6061 aluminum alloy. This study systematically investigates defect mitigation, microstructural evolution, and mechanical properties associated with high-temperature substrate preheating at 500 °C. Comprehensive microstructural analyses, including characterization of defects, grain structures, and precipitation behavior, were performed on samples in both as-built and T6 heat-treated states. Elevated preheating substantially reduced solidification cracking across a wide processing window, while demonstrating decreased crack sensitivity to laser parameters. Columnar cracks along the build direction were observed despite substrate preheating. Lack-of-fusion and keyhole porosity were effectively eliminated, though gas-induced microporosity persisted at higher powers. In-depth characterization of two distinct laser power and speed conditions confirmed the formation of micron-sized, non-coherent Mg 2 Si precipitates under heated substrate conditions, alongside α-AlFeCrMnSi intermetallic phases indicative of in-situ thermal effects during fabrication. Subsequent T6 heat treatment revealed the formation of fine, coherent needle-shaped β″ strengthening precipitates. Despite substantial differences in processing parameters, comparable mechanical properties were measured in the as-built samples (∼52 MPa yield strength, ∼130 MPa tensile strength), primarily due to reduced strain hardening effects and consistent precipitation characteristics. Meanwhile, the T6 heat treatment led to significant improvement in properties, enhancing yield strength by over 400%, aligning closely with the performance of conventional wrought AA6061-T6. These findings underscore that high-temperature substrate preheating offers an effective means to suppress cracks, control precipitation, and enhance mechanical performance in LPBF-processed AA6061.

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BibTeXRIS

Karna, Sivaji [Univ. of South Carolina, Columbia, SC (United States)] (ORCID:000900048824169X), Al-Aridi, Rimah [Univ. of South Carolina, Columbia, SC (United States)], Morrall, Daniel [Savannah River National Laboratory (SRNL), Aiken, SC (United States). Tritium Technology Division], Masse, Jean-Philippe [Polytechnique Montreal, QC (Canada)] (ORCID:0000000231871445), Sun, Can [Univ. of South Carolina, Columbia, SC (United States)] (ORCID:0009000608622877), Zhang, Tianyu [Univ. of South Carolina, Columbia, SC (United States)], Gross, Andrew J. [Univ. of South Carolina, Columbia, SC (United States)] (ORCID:0000000170241342), Hosseinzadeh, Hamed [Univ. of Wisconsin, Platteville, WI (United States)] (ORCID:0000000189461062), Martin, Étienne [Polytechnique Montreal, QC (Canada)], Krentz, Timothy [Savannah River National Laboratory (SRNL), Aiken, SC (United States). Tritium Technology Division], Hitchcock, Dale [Savannah River National Laboratory (SRNL), Aiken, SC (United States). Tritium Technology Division], Yuan, Lang [Univ. of South Carolina, Columbia, SC (United States)] (ORCID:0000000268945030). 2026-05-25. Microstructural evolution, defect mitigation, and precipitation behavior in AA6061 via laser powder bed fusion with high-temperature substrate heating. https://doi.org/10.1016/j.msea.2026.150474

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36 MATERIALS SCIENCE↗