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DOE OSTI · 3682512

A transport-based framework for solidification cracking in Ni-based superalloys processed by laser powder bed fusion

Hyer, Holden [ORNL] (ORCID:0000000343915561)·Heimbrook, Amanda [ORNL] (ORCID:0009000792668452)·Su, Yi Feng [ORNL]·Dryepondt, Sebastien [ORNL] (ORCID:0000000312651612)
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Abstract

Solidification cracking remains a persistent barrier to laser powder bed fusion (LPBF) processing of solid-solution-strengthened (SSS) Ni-based superalloys and is commonly attributed to carbide formation, liquation-type failure, or elemental segregation. In this work, the cracking behavior of three SSS Ni-based superalloys—Inconel 625 (625), Inconel 617 (617), and Haynes 230 (230)—is examined under comparable LPBF conditions to evaluate the origins of their cracking susceptibility. Carbides were present in both 625 and 230, yet cracking behavior differed significantly. MC-type carbides in 625 remain discrete and preserve liquid connectivity, whereas Cr-rich M23C6 carbides in 230 form at cellular triple junctions that bottleneck the interdendritic liquid network, influencing cracking through liquid connectivity rather than as an independent cause. Alloy 617 exhibited anomalous segregation without resolvable secondary phases yet cracked mildly, indicating that extensive carbide formation is not a prerequisite for cracking. To rationalize these observations, a transport-limited framework is proposed in which cracking occurs when terminal-liquid feeding cannot accommodate solidification-induced strain; among the mechanisms evaluated, this framework is most consistent with the physical constraints imposed by LPBF solidification. Transport-based crack-susceptibility indexes incorporating permeability, viscosity, and solidification kinetics distinguish the alloy hierarchy; permeability ratios Krat increased from approximately 7 (625) to 11.5 (617) and 14.5 (230), with corresponding increases in the μ-weighted mushy zone risk index (CSIMZRM). These results are consistent with transport-limited liquid feeding as a rate-limiting contributor to solidification cracking in LPBF-processed SSS Ni-based superalloys, providing a physically grounded basis for alloy and process design.

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Hyer, Holden [ORNL] (ORCID:0000000343915561), Heimbrook, Amanda [ORNL] (ORCID:0009000792668452), Su, Yi Feng [ORNL], Dryepondt, Sebastien [ORNL] (ORCID:0000000312651612). 2026-08-01. A transport-based framework for solidification cracking in Ni-based superalloys processed by laser powder bed fusion. https://doi.org/10.1016/j.actamat.2026.122676

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