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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 181 records · Page 10
All sourcesNASA NTRSDOE OSTI
NASA NTRS2018

Single Conductor Alloy as Diffusion Barrier System and Simulataneous OHMIC Contact to N- and P-Type Silicon Carbide

Use of a single alloy conductor to form simultaneous ohmic contacts (SOC) to n- and p-type 4H-SiC. The single alloy conductor also is an effective diffusion barrier against gold (AU) and oxygen (O.sub.2) at high temperatures (e.g., up to 800.degree. C.). The innovation may also provide an effective interconnecting metallization in a multi-level metallization device scheme.

Okojie, Robert S.↗
NASA NTRS2015

Low Temperature Shape Memory Alloys for Adaptive, Autonomous Systems Project

The objective of this joint activity between Kennedy Space Center (KSC) and Glenn Research Center (GRC) is to develop and evaluate the applicability of 2-way SMAs in proof-of-concept, low-temperature adaptive autonomous systems. As part of this low technology readiness (TRL) activity, we will develop and train low-temperature novel, 2-way shape memory alloys (SMAs) with actuation temperatures ranging from 0 C to 150 C. These experimental alloys will also be preliminary tested to evaluate their performance parameters and transformation (actuation) temperatures in low- temperature or cryogenic adaptive proof-of-concept systems. The challenge will be in the development, design, and training of the alloys for 2-way actuation at those temperatures.

Falker, John↗
NASA NTRS1986

Containerless processing of hypermonotectic and glass forming alloys using the Marshall Space Flight Center 100 meter drop tube facility

Two separate projects were carried out to study alloys whose solidification structures can be strongly influenced by the presence of a container during melting and solidifications. One project involved containerless solidification of hypermonotectic Au35Rh65 alloys. This alloy exhibits liquid immiscibility over a temperature range. It has been suggested that containerless melting might be one solution to the problem of sedimentation in the dispersions of immiscible liquid phases. However, surface tension driven flows could also lead to accumulation of the minority liquid phase at the external surface of a containerlessly melted alloy. The research underway is a first step in determining the influence of containerless, microgravity processing on immiscible alloys. Nickel-niobium alloys were studied using the drop tube facility. One alloy in this system, a Ni60Nb40 alloy, is a good candidate for the formation of a bulk metallic glass. Amorphous alloys of this composition were produced using thin film and mechanical alloying techniques. However, theory indicates that if heterogeneous nucleation can be avoided, it should be possible to produce an amorphous structure in this system using a moderate cooling rate from the melt. The containerless melting and solidification capabilities of the drop tube faciltiy provide ideal conditions for a study of this type. To date, several Ni60Nb40 samples have been levitated, melted and cooled during 4.6 seconds of free fall in the 100 meter drop tube. Structures obtained are discussed.

Andrews, J. B.↗
NASA NTRS1990

Electrochemical impedance spectroscopy of metal alloys in the space transportation system launch environment

AC impedance measurements were performed to investigate the corrosion resistance of 18 alloys under conditions similar to the Space Transportation System (STS) launch environment. The alloys were: (1) zirconium 702; (2) Hastelloy C-22, C-276, C-4, and B-2; (3) Inconel 600 and 825; (4) Ferralium 255; (5) Inco Alloy G-3; (6) 20Cb-3; (7) SS 904L, 304LN, 316L, 317L, and 304L; (8) ES 2205; and (9) Monel 400. AC impedance data were gathered for each alloy at various immersion times in 3.55 percent NaCl-0.1N HCl. Polarization resistance values were obtained for the Nyguist plots at each immersion time using the EQUIVALENT CIRCUIT software package available with the 388 electrochemical impedance software. Hastelloy C-22 showed the highest overall values for polarization resistance while Monel 400 and Inconel 600 had the lowest overall values. There was good general correlation between the corrosion performance of the alloys at the beach corrosion testing site, and the expected rate of corrosion as predicted based on the polarization resistance values obtained. The data indicate that electrochemical impedance spectroscopy can be used to predict the corrosion performance of metal alloys.

Calle, Luz↗
NASA NTRS1971

Oxidation screening at 1204 C /2200 F/ of candidate alloys for the space shuttle thermal protection system.

Evaluation of the oxidation resistance of 15 alloys under some of the environmental conditions that might be encountered by the shuttle thermal protection system. The alloys included nickel-, iron-, and cobalt-base wrought alloys. Specimens were self-resistively heated to 1204 C (2200 F) in a 10-torr still-air environment for 100 thirty-minute cycles. Specimen weight, thickness, and microstructural changes were noted, and surface scales were identified by room-temperature X-ray diffraction. Based on these observations, the behavior of the alloys was evaluated in terms of overall amount of metal consumption due to oxide formation and relative tendency toward oxide spalling and scale vaporization.

Sanders, W. A.↗
NASA NTRS1986

A new high strength alloy for hydrogen fueled propulsion systems

This paper describes the development of a high-strength alloy (1241 MPa ultimate and 1103 MPa yield, with little or no degradation in hydrogen) for application in advanced hydrogen-fueled rocket engines. Various compositions of the Fe-Ni-Co-Cr system with elemental additions of Cb, Ti and Al are discussed. After processing, notched tensile specimens were tested in 34.5-MPa hydrogen at room temperature, as the main screening test. The H2/air notch tensile ratio was used as the selection/rejection criterion. The most promising alloys are discussed.

Mcpherson, W. B.↗
NASA NTRS2005

Blanch Resistant and Thermal Barrier NiAl Coating Systems for Advanced Copper Alloys

A method of forming an environmental resistant thermal barrier coating on a copper alloy is disclosed. The steps include cleansing a surface of a copper alloy, depositing a bond coat on the cleansed surface of the copper alloy, depositing a NiAl top coat on the bond coat and consolidating the bond coat and the NiAl top coat to form the thermal barrier coating. The bond coat may be a nickel layer or a layer composed of at least one of copper and chromium-copper alloy and either the bond coat or the NiAl top coat or both may be deposited using a low pressure or vacuum plasma spray.

Sai V Raj↗
NASA NTRS1990

Refractory metal alloys and composites for space power systems

Results are presented on recent studies of refractory-metal-alloy and refractory-metal-composite technologies for space power systems, with emphasis on work performed at the Lewis Research Center in support of the Ground Engineering System (GES) for the SP-100 reactor. Special attention is given to the mechanical properties of alloys with compositions Nb-1Zr and Nb-0.1Zr-0.1C (the PWC-11 alloy) and to advanced fiber-reinforced composites. The results to date indicate that, for the GES at a power level of about 100 kWe, the PWC-11 has attractive creep properties that will extend the capabilities of the SP-100 reactor compared to a similar system fabricated from Nb-1Zr. On the other hand, tungsten-reinforced Nb-1Zr composites were found to provide a ten-fold and four-fold creep strength over Nb-1Zr and PWC-11, respectively, at 1400 to 1500 K.

Stephens, R.↗
NASA NTRS1993

Containerless processing of undercooled melts

The investigation focused on the control of microstructural evolution in Mn-Al, Fe-Ni, Ni-V, and Au-Pb-Sb alloys through the high undercooling levels provided by containerless processing, and provided fundamental new information on the control of nucleation. Solidification analysis was conducted by means of thermal analysis, x-ray diffraction, and metallographic characterization on samples processed in a laboratory scale drop tube system. The Mn-Al alloy system offers a useful model system with the capability of phase separation on an individual particle basis, thus permitting a more complete understanding of the operative kinetics and the key containerless processing variables. This system provided the opportunity of analyzing the nucleation rate as a function of processing conditions and allowed for the quantitative assessment of the relevant processing parameters. These factors are essential in the development of a containerless processing model which has a predictive capability. Similarly, Ni-V is a model system that was used to study duplex partitionless solidification, which is a structure possible only in high under cooling solidification processes. Nucleation kinetics for the competing bcc and fcc phases were studied to determine how this structure can develop and the conditions under which it may occur. The Fe-Ni alloy system was studied to identify microstructural transitions with controlled variations in sample size and composition during containerless solidification. This work was forwarded to develop a microstructure map which delineates regimes of structural evolution and provides a unified analysis of experimental observations. The Au-Pb-Sb system was investigated to characterize the thermodynamic properties of the undercooled liquid phase and to characterize the glass transition under a variety of processing conditions. By analyzing key containerless processing parameters in a ground based drop tube study, a carefully designed flight experiment may be planned to utilize the extended duration microgravity conditions of orbiting spacecraft.

Perepezko, J. H.↗
NASA NTRS1977

Evaluation and control of environmental corrosion for aluminum and steel alloys

Corrosion protection systems for aerospace application and the effects of surface treatments and methods of controlling stress corrosion are evaluated. Chromate pigmented systems were found to be most effective for aluminum alloys; zinc-rich coatings gave the greatest protection to steel alloys. Various steel and aluminum alloys are rated for stress corrosion resistance.

Franklin, D. B.↗