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Thermostability of copper-oxide alloys, oxide strengthened alloys, oxidation of alloys
Phonon-drag thermopower change in Cu-Al and Cu-Si alloys at cryogenic temperature
Statistical analysis and metallographic aspects of fatigue failure mechanisms in copper alloys
Arch-shaped conductors fabricated from flat strips of beryllium oxide dispersion-strengthened copper alloy serve as flexible electrical connectors capable of operating in 1000 deg F temperature range, under vacuum conditions for periods of 10,000 hours or more without failure.
Advanced fuel cell catalysts prepared, including gold copper alloys and silver powders
A method for the production of reticles, particularly those for use in outer space, where the product is a quartz base coated with highly adherent layers of chromium, chromium-silver, and silver vacuum deposited through a mask, and then coated with an electrodeposit of copper from a copper sulfate solution followed by an electrodeposit of black chromium is described. The masks are produced by coating a beryllium-copper alloy substrate with a positive working photoresist, developing the photoresist, according to a pattern to leave a positive mask, plating uncoated areas with gold, removing the photoresist, coating the substrate with a negative working photoresist, developing the negative working photoresist to expose the base metal of the pattern, and chemically etching the unplated side of the pattern to produce the mask.
The calibration is considered of an RF antenna capacitance probe carried aboard the RAE-1 spacecraft and the correction of the probe for external effects, believed to be primarily due to local positive ion sheaths and/or photoelectron sheaths surrounding the antenna. The RAE-1 spacecraft was launched in July 1968 into a 5850-km. Circular orbit of 121-degree inclination and carried several antenna and radiometer systems covering a frequency range of 0.2 to 9.2 MHz for radio astronomical studies. The RF capacitance probe measurements discussed utilized a 37-meter electric dipole antenna formed by two monopoles made of silver-coated beryllium-copper alloy tapes formed into hollow cylindrical tubes 1.3 cm in diameter.
Consideration of the problem of ignition and combustion of structural materials, particularly metals, which may come in contact with oxygen during its production, transport, and use. Following a review of the historical development of compatibility problems and research, a detailed account is given of compatibility testing methods aimed at detecting probable ignition sources, such as mechanical impact, electric sparks or flashes, heat, sound waves, abrasion, and surface fractures. A summary is presented of the ignition and combustion research reported in the literature, dwelling particularly on papers concerning oxygen-related accidents and the compatibility of metals with high-pressure oxygen. The relative oxygen compatibility of a number of common materials is discussed, including that of nickel and copper alloys, stainless steels, aluminum alloys, and titanium alloys. Finally, an effort is made to pinpoint research areas which would enhance understanding of the compatibility of bulk materials.
A literature analysis is presented of reports, specifications, and documented experiences with the use of electroforming to produce copper and nickel structures for aerospace and other engineering applications. The literature period covered is from 1948 to 1974. Specific effort was made to correlate mechanical property data for the electrodeposited material with known electroforming solution compositions and operating conditions. From this survey, electrolytes are suggested for selection to electroform copper and nickel outer shells on regeneratively cooled thrust chamber liners, and other devices subject to thermal and pressure exposure, based on mechanical properties obtainable, performance under various thermal environments, and ease of process control for product reproducibility. Processes of potential value in obtaining sound bonds between electrodeposited copper and nickel and copper alloy substrates are also discussed.
Copper and nickel electroforming was examined for the purpose of establishing the necessary processes and procedures for repeatable, successful fabrication of the outer structures of regeneratively cooled thrust chambers. The selection of electrolytes for copper and nickel deposition is described. The development studies performed to refine and complete the processes necessary for successful chamber shell fabrication and the testing employed to verify the applicability of the processes and procedures to small scale hardware are described. Specifications were developed to afford a guideline for the electroforming of high quality outer shells on regeneratively cooled thrust chamber liners. Test results indicated repeatable mechanical properties could be produced in copper deposits from the copper sulfate electrolyte with periodic current reversal and in nickel deposits from the sulfamate solution. Use of inert, removable channel fillers and the conductivizing of such is described. Techniques (verified by test) which produce high integrity bonds to copper and copper alloy liners are discussed.
Tentatively scheduled to fly on STS-17 (41G), this get away special aims to demonstrate amateur radio transmissions to global ground stations in the English language. Experiments No. 1, 2, and 3 use the micro-gravity of space flight to study the solidification of lead-antimony and aluminum-copper alloys, the germination of radish seeds, and the growth of potassium-tetracyanoplatinate hydrate crystals in an aqueous solution. Flight results are to be compared with Earth-based data. Experiment No. 4 (the Marshall Amateur Radio Club Experiment - MARCE) features radio transmissions and also provides timing for the start of all other experiments. A microprocessor obtains real-time data from all experiments as well as temperature and pressure measurements within the GAS canister. These data are to be transmitted on previously announced amateur radio frequencies after they are converted into the English language by a digitalker for general reception. The support structure for the G #007 experiments consists of two primary plates and four bumper assemblies.
PROJECT EXPLORER is a program that will fly student-developed experiments onboard the Space Shuttle in NASA's Get-Away Special (GAS) containers. The program is co-sponsored by the Alabama Space and Rocket Center, the Alabama-Mississippi Section of the American Institute of Aeronautics and Astronautics, Alabama A&M University and requires extensive support by the University of Alabama in Huntsville. A unique feature of this project will demonstrate transmissions to ground stations on amateur radio frequencies in English language. Experiments Nos. 1, 2, and 3 use the microgravity of space flight to study the solidification of lead-antimony and aluminum-copper alloys, the growth of potassium-tetracyanoplatinate hydrate crystals in an aqueous solution, and the germination of radish seeds. Flight results will be compared with Earth-based data. Experiment No. 4 features radio transmission and will also provide timing for the start of all other experiments. A microprocessor will obtain real-time data from all experiments as well as temperature and pressure measurements taken inside the canister. These data will be transmitted on previously announced amateur radio frequencies after they have been converted into the English language by a digitalker for general reception.
Experimental investigations on erosion of a copper alloy, phosphor bronze, under cavitation attack in a viscous mineral oil are presented. The details of pit formation and erosion were studied using scanning electron microscopy. The mean depth of penetration, the variations in surface roughness, and the changes in erosion pit size were studied. Cavitation pits formed initially over the grain boundaries while the surface grains were plastically deformed. Erosion of surface grains occurred largely by ductile fracture involving microcracking and removal in layers. The ratio h/a of the depth h to half width a of cavitation pits increased with test duration from 0.047 to 0.55.
Process makes coating with unusual properties. Coating is copper or copper alloy with controlled dispersion of oxide or carbide particles. Process results in coating that has thermal expansion similar to base material, increased resistance to abrasion when hot, and high thermal conductivity. Coatings resistant to wear used in variety of applications ranging from earth-moving equipment to space vehicles.
The selection of materials for mechanism components used in ground support equipment so that failures resulting from stress corrosion cracking will be prevented is described. A general criteria to be used in designing for resistance to stress corrosion cracking is also provided. Stress corrosion can be defined as combined action of sustained tensile stress and corrosion to cause premature failure of materials. Various aluminum, steels, nickel, titanium and copper alloys, and tempers and corrosive environment are evaluated for stress corrosion cracking.
A liquid oxygen (LOX) turbopump with an 860 R gaseous oxygen (GOX) turbine drive was designed for a 3750 lb thrust dual expander cycle rocket engine. This turbopump, which requires no interpropellant seals or system purges, features a 156 hp, single stage, full admission, impulse turbine; an axial flow inducer; a two-stage centrifugal pump with unshrouded impellers; long-life, LOX-lubricated, self-aligning, hydrostatic bearings; and a subcritical rotor design. It is constructed of Monel, a nickel-copper alloy, which has low ignition potential in oxygen. The pump was designed to deliver 34.7 gpm of 4655 psia liquid oxygen at a shaft speed of 75,000 rpm. The dual expander cycle rocket engine and the performance it requires of the LOX turbopump will be discussed as well as the design of the pump, turbine, bearings, and the turbopump rotordynamics. The test program and preliminary test results will also be presented.
A ceramic superconductivity part, such as a wire, is produced through the partial oxidation of a specially formulated copper alloy in a core. The alloys contains low level of quantities of rare earth and alkaline earth dopant elements. Upon oxidation at high temperatures, and superconducting oxide phases are formed as a thin film.
Results of material compatibility experiments using hydrocarbon fuels in contact with copper-based combustion chamber liner materials are presented. Mil-Spec RP-1, n- dodecane, propane, and methane fuels were tested in contact with OFHC, NASA-Z, and ZrCu coppers. Two distinct test methods were employed. Static tests, in which copper coupons were exposed to fuel for long durations at constant temperature and pressure, provided compatibility data in a precisely controlled environment. Dynamic tests, using the Aerojet Carbothermal Test Facility, provided fuel and copper compatibility data under realistic booster engine service conditions. Tests were conducted using very pure grades of each fuel and fuels to which a contaminant, e.g., ethylene or methyl mercaptan, was added to define the role played by fuel impurities. Conclusions are reached as to degradation mechanisms and effects, methods for the elimination of these mechanisms, selection of copper alloy combustion chamber liners, and hydrocarbon fuel purchase specifications.