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DOE OSTI2018

Tuning the Néel Temperature of Hexagonal Ferrites by Structural Distortion

To tune the magnetic properties of hexagonal ferrites, a family of magnetoelectric multiferroic materials, by atomic-scale structural engineering, we studied the effect of structural distortion on the magnetic ordering temperature ( T N ) in these materials. Using the symmetry analysis, we show that unlike most antiferromagnetic rare-earth transition-metal perovskites, a larger structural distortion leads to a higher T N in hexagonal ferrites and manganites, because the K 3 structural distortion induces the three-dimensional magnetic ordering, which is forbidden in the undistorted structure by symmetry. We also revealed a near-linear relation between T N and the tolerance factor and a power-law relation between T N and the K 3 distortion amplitude. Following the analysis, a record-high T N (185 K) among hexagonal ferrites was predicted in hexagonal ScFeO 3 and experimentally verified in epitaxially stabilized films. Furthermore these results add to the paradigm of spin-lattice coupling in antiferromagnetic oxides and suggests further tunability of hexagonal ferrites if more lattice distortion can be achieved.

36 MATERIALS SCIENCE↗

DOE OSTI2014

TH-A-BRF-10: Quantification of Subject-Specific Susceptibility-Related Geometric Distortion in Clinical Liver MRI for Radiation Therapy

Purpose: Subject-specific susceptibility-induced B0 inhomogeneity affects the geometric accuracy of MRI images, with potential impact on the accuracy of treatment planning and image guidance. This study quantifies individual distortions for patients with intrahepatic tumors. Methods: Liver MRI scans of 13 patients who were enrolled in an IRB approved study were acquired on a 3T scanner (Skyra, Siemens). Clinical contrast-enhanced images were acquired by a 3D Volume Interpolated Breath-Hold Examination (VIBE) sequence with TE/TR =1.65/4.3ms, voxel size = 2.5×2.5×3mm (axial sets) or 3.5×3.5×5mm (coronal sets), and frequency-encoding (FE) bandwidth of 440Hz/pixel. B0 inhomogeneity was evaluated by acquisition of dual gradient echoes (GRE) with TE1/TE2/TR =4.92/7.38/106ms, a voxel size of 3.5×3.5×3.75mm, a FE bandwidth of 290Hz/pixel and breath-hold. The phase difference maps from the two echoes were unwrapped using a quantitative MRI analysis software package (FSL, FMRIB, Oxford, UK). The resulting calculated B0 inhomogeneity maps (ΔB0 in Hz) were converted to voxel distortion maps in the FE direction (ΔX in mm) corresponding to the VIBE images. Results: Maximum susceptibility-induced distortions were observed in the liver dome near the diaphragm. Using results from coronal VIBE images in this study as examples, we observed clusters of voxels displaced close to or greater than ΔX=3.5mm (440 Hz in ΔB0) in the VIBE images of the liver in 3 patients, and greater than 2 mm but less than 3.5 mm in 12 patients. On average, approximately 14% of imaged liver voxels had distortions ΔX>±1mm (ΔB0>±125Hz) and 1% of the voxels had ΔX>±2mm (ΔB0>±250Hz). Conclusion: Although advanced MRI techniques, like VIBE, permit faster acquisitions allowing for breath-held examinations with limited motion-induced artifacts, this study suggests that localized distortions due to subject-specific susceptibility variations can occur and require additional advanced corrections based on measuring patient-specific B0 inhomogeneity maps. The authors would like to acknowledge funding support from NIH R01EB016079 and NIH/NCI RO1 CA132834.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2016

TU-H-206-07: Assessment of Geometric Distortion in EPI with a SPAMM Tagged Acquisition

Purpose: Echo planar imaging (EPI) is known to exhibit gross geometric distortion caused by multiple factors, including B0 inhomgeneity and transient eddy currents. However, diffusion weighted (DW) EPI has become indispensable for diagnosis and therapy assessment. We propose a methodology for quantifying distortion in EPI sequences that does not require the use of dedicated spatial accuracy phantoms, enabling flexibility in phantom design for QA of distortion effects in EPI protocols. Methods: The proposed methodology utilizes a saturation technique known as Spatial Modulation of Magnetization (SPAMM) that tags the imaging subject with saturated grid lines. Originally intended for tracking cardiac motion, these grids are applied to assess differences between diffusion weighting directions and b-values, or against a more geometrically robust sequence such as fast spin echo (FSE). The saturation preparation sequence consists of binomially weighted (e.g. 1-3-3-1) pulses interleaved with gradient blips along the frequency encode direction, followed by the same sequence with gradient blips in the phase encode direction. Three phantoms were assessed with these sequences: a spherical head-sized phantom, a large shimming phantom, and a modified PET ACR phantom that included compartments of water, air, oil, and Teflon. Each phantom was acquired with three sequences using parameters from a clinically appropriate protocol (22 cm head or 46 cm abdomen): a conventional DW-EPI sequence (3 DW directions), and both the DW-EPI and FSE sequences with tagging. Differences in grid locations were visualized with minimum intensity projection between images, and measured using intersecting locations on the grids. Results: Grid lines were clearly visualized on tagged images and enabled quantification of distortions. Maximum eddy current induced errors of 10.8 to 14.8 mm were observed in areas away from isocenter with DW gradients applied in various directions. Conclusion: SPAMM tagging provides a promising mechanism for assessing spatial distribution of distortion in EPI sequences.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2019

Analysis on Part Distortion and Residual Stress in Big Area Additive Manufacturing with Carbon Fiber-Reinforced Thermoplastic using Dehomogenization Technique

Part distortion and bottom surface warpage often occur in extrusion-based additive manufacturing. The undesirable deformations during the printing process are due to residual stresses caused by material shrinkage. Analysis on residual stress and deformation requires accurate thermo-mechanical material properties. Polymer composites reinforced with short fibers have intrinsic inhomogeneities with nonuniform fiber orientation. Therefore, homogenized macro properties may not accurately represent the progressive damage behavior or distortion. In this study, fiber orientations in Acrylonitrile Butadiene Styrene (ABS) reinforced with 20%wt carbon fiber are calculated using a de-homogenization technique. Thermal expansion coefficients in multiple directions are obtained from Thermo-Mechanical Analysis (TMA) tests. Temperature dependent stiffness is measured, and temperature dependent strength is estimated. Thermal conductivities in multiple directions and thermal capacity are measured. The calibrated thermo-mechanical properties of the composite with de-homogenized technique are used to analyze the residual stress and distortion of a 4 ft-wide wall printed in the Big Area Additive Manufacturing (BAAM) system. For experimental measurement on the wall printing, Infra-Red (IR) camera captures the temperature field, and Linear Variable Differential Transformer (LVDT) is installed to measure the warpage at the bottom surface. The experimental data are compared to the numerical analysis results. The temperature profile and the distortion profile from experiment are close to the simulation results. Damages due to residual stress and distortion are analyzed.

Kim, Pum↗

DOE OSTI2023

Designing Quaternary and Quinary Refractory-Based High-Entropy Alloys: Statistical Analysis of Their Lattice Distortion, Mechanical, and Thermal Properties

The rapid evolution in materials science has resulted in a significant interest in high-entropy alloys (HEAs) for their unique properties. This study focuses on understanding both quaternary and quinary body-centered cubic (BCC) of 12 refractory-based HEAs, and on analysis of their electronic structures, lattice distortions, mechanical, and thermal properties. A comprehensive assessment is undertaken by means of density functional theory (DFT)-based first principles calculations. It is well known that multiple constituents lead to notable lattice distortions, especially in quinary HEAs. This distortion, in turn, has significant implications on the electronic structure that ultimately affect mechanical and thermal behaviors of these alloys such as ductility, lattice thermal conductivity, and toughness. Our in-depth analysis of their electronic structures revealed the role of valence electron concentration and its correlation with bond order and mechanical properties. Local lattice distortion (LD) was investigated for these 12 HEA models. M1 (WTiVZrHf), M7 (TiZrHfW), and M12 (TiZrHfVNb) have the highest LD whereas the models M3 (MoTaTiV), M5 (WTaCrV), M6 (MoNbTaW), and M9 (NbTaTiV) have the less LD. Furthermore, we investigated the thermal properties focusing on Debye temperature (ΘD), thermal conductivity (κ), Grüneisen parameter (γα), and dominant phonon wavelength (λdom). The NbTaTiV(M9) and TiVNbHf(M10) models have significantly reduced lattice thermal conductivities (κL). This reduction is due to the mass increase and strain fluctuations, which in turn signify lattice distortion. The findings not only provide an understanding of these promising materials but also offer guidance for the design of next-generation HEAs with properties tailored for potential specific applications.

Materials Science↗

NASA NTRS1974

Formulation of a distortion index based on peak compressor pressure ratios

In order to effectively use a compressor face total-pressure distortion index as a measure of inlet-engine compatibility, a correlation of distortion amplitude with stall margin must be developed with minimal scatter. A recent analysis of data recorded in extensive distortion screen tests with the J85-GE-13 turbojet engine has resulted in a correlation based on compressor discharge pressure ratioed to the minimum pressure at the compressor face. Simply by determining compressor stall lines with a single hub radial distortion pattern, a single tip radial pattern, and with undistorted inflow, the overall compressor pressure ratio at stall for even the most complex distortion pattern was found to be predictable.

Calogeras, J. E.↗

NASA NTRS1974

Instantaneous distortion in a Mach 2.5, 40-percent-internal-contraction inlet and its effect on turbojet stall margin

An experimental wind tunnel investigation was conducted to determine the effects of time-variant distortions produced in a supersonic inlet on a J85-GE-13 turbojet engine. Results are presented principally in terms of instantaneous distortion amplitudes and total-pressure contours measured through compressor stall. They indicate that, although a time-averaged distortion may be far from a stall-inducing value, corresponding instantaneous distortion amplitudes can approach or exceed this value. Seven engine stall events were studied. In six of these events instantaneous distortion peaks of sufficient magnitude to cause stall were observed in the time period shortly before stall was detected.

Burstadt, P. L.↗

NASA NTRS1974

Formulation of a distortion index based on peak compressor pressure ratios

Calogeras, J. E.↗

NASA NTRS1974

Two-stage fan. 2: Data and performance with redesigned second stage rotor uniform and distorted inlet flows

A two-stage fan with a first rotor tip speed of 1450 ft/sec (441.96 m/sec) and no inlet guide vanes was tested with uniform and distorted inlet flows, with a redesigned second rotor having a part span shroud to prevent flutter, with variable-stagger stators set in nominal positions, and without rotor casing treatment. The fan achieved a pressure ratio 2.8 at a corrected flow of 185.4 lbm/sec (84.0 kg/sec), an adiabatic efficiency of 85.0 percent, and a stall margin of 12 percent. The redesigned second rotor did not flutter. Tip radial distortion reduced the stall margin at intermediate speed, but had little effect on stall margin at high or low speeds. Hub radial distortion reduced the stall margin at design speed but increased stall margin at low speed. Circumferential distortion reduced stall pressure ratio and flow to give approximately the same stall lines with uniform inlet flow. Distortions were attenuated by the fan. For Vol. 1, see N74-11421.

Messenger, H. E.↗

NASA NTRS1974

Geometric distortions of autocollimation type scanners

One criterion of image quality is its geometric similarity to the control test. The ability of television, phototelevision, phototelegraphic, and other systems to transmit geometrically similar images is characterized by the geometric distortion coefficient. Linear distortions result from the inaccuracy of scanning mechanism element assembly, and distortions can be minimized during adjustment operations or may be easily compensated during image reception. Brief descriptions are given of the possible sources of nonlinear distortions which arise in these devices due to the scanning mechanism, objective distortion, or the nodding mirror.

Narayeva, M. K.↗

NASA NTRS1974

Distortion in a full-scale bicone inlet with internal focused compression and 45 percent internal contraction

The distortion characteristics were investigated at the subsonic diffuser exit of a full-scale, Mach 2.5, axisymmetric, mixed compression inlet. Performance and steady-state distortion characteristics were obtained at zero and maximum angle of attack and during an inlet unstart-restart sequence. For the configuration with no cowl bleed, steady-state distortion P(max)P(min)P(bar) ranged from 0.10 for critical inlet operation at 0 deg angle-of-attack to 0.306 for supercritical inlet operation at 6.84 deg angle-of-attack. Vortex generators provided a 50 percent reduction in steady-state distortion for critical operation. Bleed has a smaller effect on steady-stated distortion.

Wasserbauer, J. F.↗

NASA NTRS1974

Some observations of the effects of radial distortions on performance of a transonic rotating blade row

A single rotating blade row was tested with two magnitudes of tip radial distortion and two magnitudes of hub radial distortion imposed on the inlet flow. The rotor was about 50 centimeters (20 in.) in diameter and had a design operating tip speed of approximately 420 meters per second (1380 ft/sec). Overall performance at 60, 80, and 100 percent of equivalent design speed generally showed a decrease (compared to undistorted flow) in rotor stall margin with tip radial distortion but no change, or a slight increase, in rotor stall margin with hub radial distortion. At design speed there was a decrease in rotor overall total pressure ratio and choke flow with all inlet flow distortions. Radial distributions of blade element parameters are presented for selected operating conditions at design speed.

Sandercock, D. M.↗

NASA NTRS1975

The effect of circumferential distortion on fan performance at two levels of blade loading

Single stage fans designed for two levels of pressure ratio or blade loading were subjected to screen-induced circumferential distortions of 90-degree extent. Both fan rotors were designed for a blade tip speed of 425 m/sec, blade solidity of 1.3 and a hub-to-tip radius ratio of 0.5. Circumferential measurements of total pressure, temperature, static pressure, and flow angle were obtained at the hub, mean and tip radii at five axial stations. Rotor loading level did not appear to have a significant influence on rotor response to distorted flow. Losses in overall pressure ratio due to distortion were most severe in the stator hub region of the more highly loaded stage. At the near stall operating condition tip and hub regions of (either) rotor demonstrated different response characteristics to the distorted flow. No effect of loading was apparent on interactions between rotor and upstream distorted flow fields.

Hartmann, M. J.↗

NASA NTRS1975

Spline function approximation techniques for image geometric distortion representation

Least squares approximation techniques were developed for use in computer aided correction of spatial image distortions for registration of multitemporal remote sensor imagery. Polynomials were first used to define image distortion over the entire two dimensional image space. Spline functions were then investigated to determine if the combination of lower order polynomials could approximate a higher order distortion with less computational difficulty. Algorithms for generating approximating functions were developed and applied to the description of image distortion in aircraft multispectral scanner imagery. Other applications of the techniques were suggested for earth resources data processing areas other than geometric distortion representation.

Anuta, P. E.↗

NASA NTRS1975

The effect of circumferential distortion on fan performance at two levels of blade loading

Single stage fans designed for two levels of pressure ratio or blade loading (rotor tip D-factor of 0.43 and 0.54) were subjected to screen-induced circumferential distortions of 90-degree extent. Both fan rotors were designed for a blade tip speed of 425 m/sec, blade solidity of 1.3 and a hub-to-tip radius ratio of 0.5. Circumferential measurements of total pressure, temperature, static pressure, and flow angle were obtained at the hub, mean and tip radii at five axial stations (three between the screen and rotor and behind rotor and stator blade rows). Rotor loading level did not appear to have a significant influence on rotor response to distorted flow. Losses in overall pressure ratio due to distortion were most severe in the stator hub region of the more highly loaded stage. At the near stall operating condition tip and hub regions of (either) rotor demonstrated different response characteristics to the distorted flow. No effect of loading was apparent on interactions between rotor and upstream distorted flow fields.

Hartmann, M. J.↗

NASA NTRS1976

The effect of circumferential distortion on fan performance at two levels of blade loading

Single stage fans designed for two levels of pressure ratio or blade loading were subjected to screen induced circumferential distortions of 90 degree extent. Both fan rotors were designed for a blade tip speed of 425 m/sec, blade solidity of 1.3 and a hub-to-tip radius ratio of 0.5. Circumferential measurements of total pressure, temperature, static pressure, and flow angle were obtained at the hub, mean and tip radii at five axial stations. Rotor loading level did not appear to have a significant influence on rotor response to distorted flow. Losses in overall pressure ratio due to distortion were most severe in the stator hub region of the more highly loaded stage. At the near stall operating condition tip and hub regions of (either) rotor demonstrated different response characteristics to the distorted flow. No effect of loading was apparent on interactions between rotor and upstream distorted flow fields.

Hartmann, M. J.↗

NASA NTRS1976

Analysis of distortion data from TF30-P-3 mixed compression inlet test

A program was conducted to reduce and analyze inlet and engine data obtained during testing of a TF30-P-3 engine operating behind a mixed compression inlet. Previously developed distortion analysis techniques were applied to the data to assist in the development of a new distortion methodology. Instantaneous distortion techniques were refined as part of the distortion methodology development. A technique for estimating maximum levels of instantaneous distortion from steady state and average turbulence data was also developed as part of the program.

King, R. W.↗

NASA NTRS1975

Estimating maximum instantaneous distortion from inlet total pressure rms and PSD measurements

An inexpensive method is developed to determine the extreme values of instantaneous inlet distortion. This method also provides insight into the basic mechanics of unsteady inlet flow and the associated engine reaction. The analysis is based on fundamental fluid dynamics and statistical methods to provide an understanding of the turbulent inlet flow and quantitatively relate the rms level and power spectral density (PSD) function of the measured time variant total pressure fluctuations to the strength and size of the low pressure regions. The most probable extreme value of the instantaneous distortion is then synthesized from this information in conjunction with the steady state distortion. Results of the analysis show the extreme values to be dependent upon the steady state distortion, the measured turbulence rms level and PSD function, the time on point, and the engine response characteristics. Analytical projections of instantaneous distortion are presented and compared with data obtained by a conventional, highly time correlated, 40 probe instantaneous pressure measurement system.

Melick, H. C., Jr.↗