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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 181 records · Page 10

Figure Measurements of High-Energy-X-Ray Replicated Optics

We are developing grazing incidence x-ray optics for a balloon-borne hard-x-ray telescope (HERO). The HERO mirror shells are fabricated using electroform-nickel replication off super-polished cylindrical mandrels. One of the sources for mirror resolution error is departure of the shell figure from prescription. We have modified a Vertical-scan Long Trace Profilometer (VLTP) in order to measure the figure of the inner surface of the HERO mirror shells for diameters as small as 76 mm. Mirror alignment method and sources for systematic errors will be discussed. Comparison of figure metrology of the mandrel and the shells will be presented together with results from x-ray tests.

Gubarev, Mikhail↗

Electrodeposition of High Quality Nickel Phosphorous Alloys for Pollution Reduction and Energy Conservation

NASA and the University of Alabama in Huntsville have developed ecologically friendly, versatile nickel and nickel cobalt phosphorous electroplating processes. Solutions show excellent performance with high efficiency for vastly extended throughput. Properties include, clean, low temperature operation (40 - 60 C), high Faradaic efficiency, low stress and high hardness. A variety of alloy and plating speed options are easily achieved from the same chemistry using soluble anodes for metal replacement with only 25% of the phosphorous additions required for electroless nickel. Thick deposits are easily achieved unattended, for electroforming freestanding shapes without buildup of excess orthophosphate or stripping of equipment.

Engelhaupt, Darell↗

Development of High Resolution Hard X-Ray Telescope with Multilayer Coatings

The major objective of this program is the development of a focusing hard X-ray telescope with moderately high angular resolution, i .e. comparable to the telescopes of XMM-Newton. The key ingredients of the telescope are a depth graded multilayer coatings and electroformed nickel substrates that are considerably lighter weight than those of previous missions such as XMM-Newton, which have had conventional single metal layer reflective coatings and have operated at much lower energy X-rays. The ultimate target mission for this technology is the Hard X-Ray Telescope (HXT) of the Constellation X-Ray Mission. However, it is applicable to potential SMEX and MIDEX programs as well.

Brinton, John C.↗

Electrodeposition of High Quality Nickel Phosphorous Alloys for Pollution Reduction and Energy Conservation

NASA and the University of Alabama in Huntsville have developed ecologically friendly, versatile nickel and nickel cobalt phosphorous electroplating processes. Solutions show excellent performance with high efficiency for vastly extended throughput. Properties include, clean, low temperature operation (40 - 60 C), high Faradaic efficiency, low stress and high hardness. A variety of alloy and plating speed options are easily achieved from the same chemistry using soluble anodes for metal replacement with only 25% of the phosphorous additions required for electroless nickel. Thick deposits are easily achieved unattended, for electroforming freestanding shapes without buildup of excess orthophosphate or stripping of equipment.

Engelhaupt, Darell↗

Electrocomposite of Alumina in Nickel Matrix

Nickel/aluminum oxide composite was electroformed in a sulfamate bath with 50 g/L of 0.05-micron aluminum oxide powder. Different plating methods including direct current plating, periodic pulse plating, and periodic reverse pulse plating were used. With conventional direct current plating, the maximum particle inclusion in the nickel matrix remains about 2% (wt). However, much higher percentile particle inclusions were achieved when a specific pulse reversal plating technique was applied. The particle incorporation approaches theoretical maximum when the deposit thickness per cycle approaches the particle diameter size at lower duty cycle. The highest particle incorporation achieved is 23% (by weight). Conceptual models interpreting the dramatic differences in the results of these plating methods were also proposed.

Xiong-Skiba, Pei↗

Development of High Resolution Hard X-Ray Telescope with Multi-Layer Coatings

This is the annual report for the third year of a three-year program. Previous annual reports have described progress achieved in the first and second years. The major objective of this program is the development of a focusing hard X-ray telescope with moderately high angular resolution, i.e. comparable to the telescopes of XMM-Newton. The key ingredients of the telescope are a depth graded multilayer coatings and electroformed nickel substrates that are considerably lighter weight than those of previous missions such as XMM-Newton, which have had conventional single metal layer reflective coatings and have operated at much lower energy X-rays. The ultimate target mission for this technology is the Hard X-Ray Telescope (HXT) of the Constellation X-Ray Mission. However, it is applicable to potential SMEX and MIDEX programs as well. We are building upon technology that has proven to be successful in the XMM-Newton and SWIFT missions. The improvements that we are adding are a significant reduction in mass without much loss of angular resolution and an order of magnitude extension of the bandwidth through the use of multilayer coatings. The distinctive feature of this approach compared to those of other hard X-ray telescope programs is that we expect the angular resolution to be superior than telescopes made by other methods thanks to the structural integrity of the substrates. They are thin walled complete cylinders of revolution with a Wolter Type 1 figure; the front half is a parabola, the rear half a hyperbola.

Gorenstein, Paul↗

Metrology for the Development of High Energy X-Ray Optics

We are developing grazing incidence x-ray optics for a balloon-borne hard-x-ray telescope (HERO). The instrument will have 200 sq cm effective collecting area at 40 keV and an angular resolution goal of 15 arcsec. The HERO mirror shells are fabricated using electroform-nickel replication off super-polished cylindrical mandrels. The angular resolution goal puts stringent requirements on the quality of x-ray mirrors and, hence, on mandrel quality. We used metrology in an iterative approach to monitor and refine the x- ray mirror fabrication process. Comparison of surface figure and microroughness measurements of the mandrel and the shells will be presented together with results from x-ray tests.

Gubarev, Mikhail↗

Alignment, Assembly and Testing of High Energy X-Ray Optics

We are developing grazing-incidence x-ray imaging optics for a balloon-borne hard x-ray telescope (HERO). The HERO payload, scheduled for launch in May 2005, currently consists of 8 mirror modules each containing 12 mirror shells fabricated using electroform-nickel replication off super-polished cylindrical mandrels. An optical system developed for aligning and assembling the shells in the modules will be described. Sources for systematic errors associated with this process will be discussed and results from on-ground x-ray testing of each module will be presented.

Gubarev, Mikhail↗

Status of MSFC X-ray Shell Optics Fabrication Capability

We present details of an MSFC development program of electroformed-nickel replicated grazing incidence optics for x-ray imaging. To date a wide variety of mirrors has been produced with diameters ranging from 2.5 cm, for small animal imaging, up to 112 meter, for x-ray astronomy. Around 100 intermediate size shells are currently aboard the HERO x-ray astronomy balloon payload awaiting launch in Fort Sumner, New mexico. Details of the program are presented together with developments currently underway to improve mirror-shell quality from the current approx. 15 arcsec resolution to below 10 arcsec for future x-ray astronomy missions.

Sthal, H. Philip↗

An Evaluation of Grazing-Incidence Optics for Neutron Imaging

The focusing capabilities of neutron imaging optic based on the Wolter-1 geometry have been successfully demonstrated with a beam of long wavelength neutrons with low angular divergence.. A test mirror was fabricated using an electroformed nickel replication process at Marshall Space Flight Center. The neutron current density gain at the focal spot of the mirror is found to be at least 8 for neutron wavelengths in the range from 6 to 20 A. Possible applications of the optics are briefly discussed.

Gubarev, M. V.↗

Mounting and Alignment of Full-Shell Replicated X-Ray Optics

We are developing grazing-incidence x-ray optics for astronomy. The optics are full-cylinder mirror shells fabricated using electroformed-nickel replication off super-polished mandrels. For space-based applications where weight is at a premium, very-thin-walled, light-weight mirrors are required. Such shells have been fabricated at MSFC with greater than 15 arcsec resolution. The challenge, however, is to preserve this resolution during mounting and assembly. We present here a status report on a mounting and alignment system currently under development at Marshall Space Flight Center to meet this challenge.

Gubarev, Mikhail↗

Periodic reverse current pulsing to form uniformly sized feed through conductors

A large number of electrically conductive solid, dense feed-through paths for the high-speed low-loss transfer of electrical signals between integrated circuits of a single silicon-on-sapphire body, or between integrated circuits of several silicon-on-sapphire bodies, are provided by an electroforming method utilizing periodic reverse-current pulsing.

Anthony, Thomas R.↗

Technology Development for Nickel X-Ray Optics Enhancement

We are developing grazing-incidence x-ray optics for high-energy astrophysics using the electroform-nickel replication process. In this process, mirror shells are fabricated by replication off super-polished cylindrical mandrels. The mirrors fabricated using this process have a demonstrated optical performance at the level of 11-12 arc seconds resolution (HPD) for 30 keV x rays. Future missions demand ever higher angular resolutions and this places stringent requirements on the quality of the mandrels, the precision of the metrology, and the mounting and alignment of the mirror shells in their housings. A progress report on recent technology developments in all these areas will be presented along with a discussion on possible post fabrication, in-situ improvement of the x-ray mirrors quality.

Bubarev, Mikhail↗

Differential Deposition Technique for Figure Corrections in Grazing Incidence X-ray Optics

A differential deposition technique is being developed to correct the low- and mid-spatial-frequency deviations in the axial figure profile of Wolter type grazing incidence X-ray optics. These deviations arise due to various factors in the fabrication process and they degrade the performance of the optics by limiting the achievable angular resolution. In the differential deposition technique, material of varying thickness is selectively deposited along the length of the optic to minimize these deviations, thereby improving the overall figure. High resolution focusing optics being developed at MSFC for small animal radionuclide imaging are being coated to test the differential deposition technique. The required spatial resolution for these optics is 100 m. This base resolution is achievable with the regular electroform-nickel-replication fabrication technique used at MSFC. However, by improving the figure quality of the optics through differential deposition, we aim at significantly improving the resolution beyond this value.

Kilaru, Kiranmayee↗

Hard X-ray Optics Technology Development for Astronomy at the Marshall Space Flight Center

Grazing-incidence telescopes based on Wolter 1 geometry have delivered impressive advances in astrophysics at soft-x-ray wavelengths, while the hard xray region remains relatively unexplored at fine angular resolution and high sensitivities. The ability to perform ground-breaking science in the hard-x-ray energy range had been the motivation for technology developments aimed at fabricating low-cost, light-weight, high-quality x-ray mirrors. Grazing-incidence x-ray optics for high-energy astrophysical applications is being developed at MSFC using the electroform-nickel replication process.

Gubarev, Mikhail↗

Miniature Scroll Pumps Fabricated by LIGA

Miniature scroll pumps have been proposed as roughing pumps (low - vacuum pumps) for miniature scientific instruments (e.g., portable mass spectrometers and gas analyzers) that depend on vacuum. The larger scroll pumps used as roughing pumps in some older vacuum systems are fabricated by conventional machining. Typically, such an older scroll pump includes (1) an electric motor with an eccentric shaft to generate orbital motion of a scroll and (2) conventional bearings to restrict the orbital motion to a circle. The proposed miniature scroll pumps would differ from the prior, larger ones in both design and fabrication. A miniature scroll pump would include two scrolls: one mounted on a stationary baseplate and one on a flexure stage (see figure). An electromagnetic actuator in the form of two pairs of voice coils in a push-pull configuration would make the flexure stage move in the desired circular orbit. The capacitance between the scrolls would be monitored to provide position (gap) feedback to a control system that would adjust the drive signals applied to the voice coils to maintain the circular orbit as needed for precise sealing of the scrolls. To minimize power consumption and maximize precision of control, the flexure stage would be driven at the frequency of its mechanical resonance. The miniaturization of these pumps would entail both operational and manufacturing tolerances of <1 m. Such tight tolerances cannot be achieved easily by conventional machining of high-aspect-ratio structures like those of scroll-pump components. In addition, the vibrations of conventional motors and ball bearings exceed these tight tolerances by an order of magnitude. Therefore, the proposed pumps would be fabricated by the microfabrication method known by the German acronym LIGA ( lithographie, galvanoformung, abformung, which means lithography, electroforming, molding) because LIGA has been shown to be capable of providing the required tolerances at large aspect ratios.

Wiberg, Dean↗

Development and Testing of High Surface Area Iridium Anodes for Molten Oxide Electrolysis

Processing of lunar regolith into oxygen for habitat and propulsion is needed to support future space missions. Direct electrochemical reduction of molten regolith is an attractive method of processing, because no additional chemical reagents are needed. The electrochemical processing of molten oxides requires high surface area, inert anodes. Such electrodes need to be structurally robust at elevated temperatures (1400-1600 C), be resistant to thermal shock, have good electrical conductivity, be resistant to attack by molten oxide (silicate), be electrochemically stable and support high current density. Iridium with its high melting point, good oxidation resistance, superior high temperature strength and ductility is the most promising candidate for anodes in high temperature electrochemical processes. Several innovative concepts for manufacturing such anodes by electrodeposition of iridium from molten salt electrolyte (EL-Form process) were evaluated. Iridium electrodeposition to form of complex shape components and coating was investigated. Iridium coated graphite, porous iridium structure and solid iridium anodes were fabricated. Testing of electroformed iridium anodes shows no visible degradation. The result of development, manufacturing and testing of high surface, inert iridium anodes will be presented.

Shchetkovskiy, Anatoliy↗

Development and Testing of High Surface Area Iridium Anodes for Molten Oxide Electrolysis

Processing of lunar regolith into oxygen for habitat and propulsion is needed to support future space missions. Direct electrochemical reduction of molten regolith is an attractive method of processing, because no additional chemical reagents are needed. The electrochemical processing of molten oxides requires high surface area, inert anodes. Such electrodes need to be structurally robust at elevated temperatures (1400-1600?C), be resistant to thermal shock, have good electrical conductivity, be resistant to attack by molten oxide (silicate), be electrochemically stable and support high current density. Iridium with its high melting point, good oxidation resistance, superior high temperature strength and ductility is the most promising candidate for anodes in high temperature electrochemical processes. Several innovative concepts for manufacturing such anodes by electrodeposition of iridium from molten salt electrolyte (EL-Form? process) were evaluated. Iridium electrodeposition to form of complex shape components and coating was investigated. Iridium coated graphite, porous iridium structure and solid iridium anodes were fabricated. Testing of electroformed iridium anodes shows no visible degradation. The result of development, manufacturing and testing of high surface, inert iridium anodes will be presented.

Shchetkovskiy, Anatoliy↗