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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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NASA NTRS1976

Skin friction reduction by slot injection at Mach 0.8

Surface skin friction, boundary layer profiles and turbulent intensity due to axially symmetric tangential slot injection into a transonic boundary layer were measured. Effects of slot height, multiple slot injection, and injection mass flow rate on the surface skin friction downstream of the the slot have been investigated. Surface skin friction was a function of the injection mass flow rate for x/s 40. Large normal pressure gradient and relatively large turbulent intensity were found near the slot with small injection mass flow rate; the region the high turbulent intensity moved downstream with increasing injection mass flow rate. The results with two slot injections indicated that the distance between slots should be less than 30 slot heights in order to achieve some benefits from the first slot. Of significant importance in the present investigation is that the skin friction reduction obtained at transonic speed is of the same order as obtained in the hypersonic regime. Additional work is required in order to formulate a correlation between the turbulent intensity and the injection mass flow rate that may be used in future analysis.

Zakkay, V.↗
NASA NTRS2009

Liquid Oxygen/Liquid Methane Test Summary of the RS-18 Lunar Ascent Engine at Simulated Altitude Conditions at NASA White Sands Test Facility

Tests were conducted with the RS18 rocket engine using liquid oxygen (LO2) and liquid methane (LCH4) propellants under simulated altitude conditions at NASA Johnson Space Center White Sands Test Facility (WSTF). This project is part of NASA s Propulsion and Cryogenics Advanced Development (PCAD) project. "Green" propellants, such as LO2/LCH4, offer savings in both performance and safety over equivalently sized hypergolic propellant systems in spacecraft applications such as ascent engines or service module engines. Altitude simulation was achieved using the WSTF Large Altitude Simulation System, which provided altitude conditions equivalent up to approx.120,000 ft (approx.37 km). For specific impulse calculations, engine thrust and propellant mass flow rates were measured. Propellant flow rate was measured using a coriolis-style mass-flow meter and compared with a serial turbine-style flow meter. Results showed a significant performance measurement difference during ignition startup. LO2 flow ranged from 5.9-9.5 lbm/sec (2.7-4.3 kg/sec), and LCH4 flow varied from 3.0-4.4 lbm/sec (1.4-2.0 kg/sec) during the RS-18 hot-fire test series. Thrust was measured using three load cells in parallel. Ignition was demonstrated using a gaseous oxygen/methane spark torch igniter. Data was obtained at multiple chamber pressures, and calculations were performed for specific impulse, C* combustion efficiency, and thrust vector alignment. Test objectives for the RS-18 project are 1) conduct a shakedown of the test stand for LO2/methane lunar ascent engines, 2) obtain vacuum ignition data for the torch and pyrotechnic igniters, and 3) obtain nozzle kinetics data to anchor two-dimensional kinetics codes.

Melcher, John C., IV↗
NASA NTRS2011

Co-Flow Hollow Cathode Technology

Hall thrusters utilize identical hollow cathode technology as ion thrusters, yet must operate at much higher mass flow rates in order to efficiently couple to the bulk plasma discharge. Higher flow rates are necessary in order to provide enough neutral collisions to transport electrons across magnetic fields so that they can reach the discharge. This higher flow rate, however, has potential life-limiting implications for the operation of the cathode. A solution to the problem involves splitting the mass flow into the hollow cathode into two streams, the internal and external flows. The internal flow is fixed and set such that the neutral pressure in the cathode allows for a high utilization of the emitter surface area. The external flow is variable depending on the flow rate through the anode of the Hall thruster, but also has a minimum in order to suppress high-energy ion generation. In the co-flow hollow cathode, the cathode assembly is mounted on thruster centerline, inside the inner magnetic core of the thruster. An annular gas plenum is placed at the base of the cathode and propellant is fed throughout to produce an azimuthally symmetric flow of gas that evenly expands around the cathode keeper. This configuration maximizes propellant utilization and is not subject to erosion processes. External gas feeds have been considered in the past for ion thruster applications, but usually in the context of eliminating high energy ion production. This approach is adapted specifically for the Hall thruster and exploits the geometry of a Hall thruster to feed and focus the external flow without introducing significant new complexity to the thruster design.

Hofer, Richard R.↗
NASA NTRS2004

Module for Oxygenating Water without Generating Bubbles

A module that dissolves oxygen in water at concentrations approaching saturation, without generating bubbles of oxygen gas, has been developed as a prototype of improved oxygenators for water-disinfection and water-purification systems that utilize photocatalyzed redox reactions. Depending on the specific nature of a water-treatment system, it is desirable to prevent the formation of bubbles for one or more reasons: (1) Bubbles can remove some organic contaminants from the liquid phase to the gas phase, thereby introducing a gas-treatment problem that complicates the overall water-treatment problem; and/or (2) in some systems (e.g., those that must function in microgravity or in any orientation in normal Earth gravity), bubbles can interfere with the flow of the liquid phase. The present oxygenation module (see Figure 1) is a modified version of a commercial module that contains >100 hollow polypropylene fibers with a nominal pore size of 0.05 m and a total surface area of 0.5 m2. The module was originally designed for oxygenation in a bioreactor, with no water flowing around or inside the tubes. The modification, made to enable the use of the module to oxygenate flowing water, consisted mainly in the encapsulation of the fibers in a tube of Tygon polyvinyl chloride (PVC) with an inside diameter of 1 in. (approx.=25 mm). In operation, water is pumped along the insides of the hollow fibers and oxygen gas is supplied to the space outside the hollow tubes inside the PVC tube. In tests, the pressure drops of water and oxygen in the module were found to be close to zero at water-flow rates ranging up to 320 mL/min and oxygen-flow rates up to 27 mL/min. Under all test conditions, no bubbles were observed at the water outlet. In some tests, flow rates were chosen to obtain dissolved-oxygen concentrations between 25 and 31 parts per million (ppm) . approaching the saturation level of approx.=35 ppm at a temperature of 20 C and pressure of 1 atm (approx.=0.1 MPa). As one would expect, it was observed that the time needed to bring a flow of water from an initial low dissolved-oxygen concentration (e.g., 5 ppm) to a steady high dissolved-oxygen concentration at or near the saturation level depends on the rates of flow of both oxygen and water, among other things. Figure 2 shows the results of an experiment in which a greater flow of oxygen was used during the first few tens of minutes to bring the concentration up to approx.=25 ppm, then a lesser flow was used to maintain the concentration.

Gonzalez-Martin, Anuncia↗
NASA NTRS1986

Ion Mobility Drift Spectrometer (IMDS) as a flight analytical instrument technique

A detailed knowledge of the history and abundances of the biogenic elements and their compounds throughout the solar system can provide the exobiologists with a basis for understanding the conditions necessary for chemical evolution and the origin of life. The Ion Mobility Drift Spectrometer is an ion molecule reactor coupled with an ion drift spectrometer. Sample molecules are ionized to form product ions in the reactant region. An electric field moves the ions through a drift region against the flow of a drift gas where they are separated according to their size and structure producing an ion mobility spectrum. These spectra provide the IMDS with virtually universal sample identification capability. To conform to the rigid limits of weight, volume and consumables placed on flight instrumentation, several aspects of the IMDS must be studied and redesigned for flight use. In addition to miniaturization of the instrument, a reduction in the high flow rates used for the drift gas is an obvious necessary consideration. The effect of drastically reduced drift flow rates on IMDS spectra was investigated by lowering flow rates from 500ml/min to 50ml/min. Changes in peak shape, drift time and total spectra were studied at each flow rate.

Kojiro, D. R.↗
NASA NTRS1992

Acoustic modes in fluid networks

Pressure and flow rate eigenvalue problems for one-dimensional flow of a fluid in a network of pipes are derived from the familiar transmission line equations. These equations are linearized by assuming small velocity and pressure oscillations about mean flow conditions. It is shown that the flow rate eigenvalues are the same as the pressure eigenvalues and the relationship between line pressure modes and flow rate modes is established. A volume at the end of each branch is employed which allows any combination of boundary conditions, from open to closed, to be used. The Jacobi iterative method is used to compute undamped natural frequencies and associated pressure/flow modes. Several numerical examples are presented which include acoustic modes for the Helium Supply System of the Space Shuttle Orbiter Main Propulsion System. It should be noted that the method presented herein can be applied to any one-dimensional acoustic system involving an arbitrary number of branches.

Michalopoulos, C. D.↗
NASA NTRS2006

Design Enhancements of the Two-Dimensional, Dual Throat Fluidic Thrust Vectoring Nozzle Concept

A Dual Throat Nozzle fluidic thrust vectoring technique that achieves higher thrust-vectoring efficiencies than other fluidic techniques, without sacrificing thrust efficiency has been developed at NASA Langley Research Center. The nozzle concept was designed with the aid of the structured-grid, Reynolds-averaged Navier-Stokes computational fluidic dynamics code PAB3D. This new concept combines the thrust efficiency of sonic-plane skewing with increased thrust-vectoring efficiencies obtained by maximizing pressure differentials in a separated cavity located downstream of the nozzle throat. By injecting secondary flow asymmetrically at the upstream minimum area, a new aerodynamic minimum area is formed downstream of the geometric minimum and the sonic line is skewed, thus vectoring the exhaust flow. The nozzle was tested in the NASA Langley Research Center Jet Exit Test Facility. Internal nozzle performance characteristics were defined for nozzle pressure ratios up to 10, with a range of secondary injection flow rates up to 10 percent of the primary flow rate. Most of the data included in this paper shows the effect of secondary injection rate at a nozzle pressure ratio of 4. The effects of modifying cavity divergence angle, convergence angle and cavity shape on internal nozzle performance were investigated, as were effects of injection geometry, hole or slot. In agreement with computationally predicted data, experimental data verified that decreasing cavity divergence angle had a negative impact and increasing cavity convergence angle had a positive impact on thrust vector angle and thrust efficiency. A curved cavity apex provided improved thrust ratios at some injection rates. However, overall nozzle performance suffered with no secondary injection. Injection holes were more efficient than the injection slot over the range of injection rates, but the slot generated larger thrust vector angles for injection rates less than 4 percent of the primary flow rate.

Flamm, Jeffrey D.↗
NASA NTRS2006

Numerical Modeling of Flow Control in a Boundary-Layer-Ingesting Offset Inlet Diffuser at Transonic Mach Numbers

This paper will investigate the validation of a NASA developed, Reynolds-averaged Navier-Stokes (RANS) flow solver, OVERFLOW, for a boundary-layer-ingesting (BLI) offset (S-shaped) inlet in transonic flow with passive and active flow control devices as well as the baseline case. Numerical simulations are compared to wind tunnel results of a BLI inlet conducted at the NASA Langley 0.3-Meter Transonic Cryogenic Tunnel. Comparisons of inlet flow distortion, pressure recovery, and inlet wall pressures are performed. The numerical simulations are compared to the BLI inlet data at a freestream Mach number of 0.85 and a Reynolds number of approximately 2 million based on the length of the fan-face diameter. The numerical simulations with and without wind tunnel walls are performed, quantifying effects of the tunnel walls on the BLI inlet flow measurements. The wind tunnel test evaluated several different combinations of jet locations and mass flow rates as well as a vortex generator (VG) vane case. The numerical simulations will be performed on a single jet configuration for varying actuator mass flow rates at a fix inlet mass flow condition. Validation of the numerical simulations for the VG vane case will also be performed for varying inlet mass flow rates. Overall, the numerical simulations were able to predict the baseline circumferential flow distortion, DPCPavg, very well for comparisons made within the designed operating range of the BLI inlet. However the CFD simulations did predict a total pressure recovery that was 0.01 lower than the experiment. Numerical simulations of the baseline inlet flow also showed good agreement with the experimental inlet centerline surface pressures. The vane case showed that the CFD predicted the correct trends in the circumferential distortion for varying inlet mass flow but had a distortion level that was nearly twice as large as the experiment. Comparison to circumferential distortion measurements for a 15 deg clocked 40 probe rake indicated that the circumferential distortion levels are very sensitive to the symmetry of the flow and that a miss alignment of the vanes in the experiment could have resulted in this difference. The numerical simulations of the BLI inlet with jets showed good agreement with the circumferential inlet distortion levels for a range of jet actuator mass flow ratios at a fixed inlet mass flow rate. The CFD simulations for the jet case also predicted an average total pressure recovery that was 0.01 lower than the experiment as was seen in the baseline. Comparison of the flow features the jet case revealed that the CFD predicted a much larger vortex at the engine fan-face when compare to the experiment.

Allan Brian G.↗
NASA NTRS1990

Computer code for predicting coolant flow and heat transfer in turbomachinery

A computer code was developed to analyze any turbomachinery coolant flow path geometry that consist of a single flow passage with a unique inlet and exit. Flow can be bled off for tip-cap impingement cooling, and a flow bypass can be specified in which coolant flow is taken off at one point in the flow channel and reintroduced at a point farther downstream in the same channel. The user may either choose the coolant flow rate or let the program determine the flow rate from specified inlet and exit conditions. The computer code integrates the 1-D momentum and energy equations along a defined flow path and calculates the coolant's flow rate, temperature, pressure, and velocity and the heat transfer coefficients along the passage. The equations account for area change, mass addition or subtraction, pumping, friction, and heat transfer.

Meitner, Peter L.↗
NASA NTRS2000

Hydrodynamic Suppression of Soot Formation in Laminar Coflowing Jet Diffusion Flames

Effects of flow (hydrodynamic) properties on limiting conditions for soot-free laminar non-premixed hydrocarbon/air flames (called laminar soot-point conditions) were studied, emphasizing non-buoyant laminar coflowing jet diffusion flames. Effects of air/fuel-stream velocity ratios were of particular interest; therefore, the experiments were carried out at reduced pressures to minimize effects of flow acceleration due to the intrusion of buoyancy. Test conditions included reactant temperatures of 300 K; ambient pressures of 3.7-49 8 kPa; methane-, acetylene-, ethylene-, propane-, and methane-fueled flames burning in coflowing air with fuel-port diameters of 1.7, 3.2, and 6.4 mm, fuel jet Reynolds numbers of 18-121; air coflow velocities of 0-6 m/s; and air/fuel-stream velocity ratios of 0.003-70. Measurements included laminar soot-point flame lengths, laminar soot-point fuel flow rates, and laminar liftoff conditions. The measurements show that laminar soot-point flame lengths and fuel flow rates can be increased, broadening the range of fuel flow rates where the flames remain soot free, by increasing air/fuel-stream velocity ratios. The mechanism of this effect involves the magnitude and direction of flow velocities relative to the flame sheet where increased air/fuel-stream velocity ratios cause progressive reduction of flame residence times in the fuel-rich soot-formation region. The range of soot-free conditions is limited by both liftoff, particularly at low pressures, and the intrusion of effects of buoyancy on effective air/fuel-stream velocity ratios, particularly at high pressures. Effective correlations of laminar soot- and smoke-point flame lengths were also found in terms of a corrected fuel flow rate parameter, based on simplified analysis of laminar jet diffusion flame structure. The results show that laminar smoke-point flame lengths in coflowing air environments are roughly twice as long as soot-free (blue) flames under comparable conditions due to the presence of luminous soot particles under fuel-lean conditions when smoke-point conditions are approached. This is very similar to earlier findings concerning differences between laminar smoke- and sootpoint flame lengths in still environments.

Dai, Z.↗
NASA NTRS1987

Amorphous silicon deposition diagnostics using coherent anti-Stokes Raman spectroscopy

This paper reports on an in situ silicon deposition process diagnostics, using CARS performed at state-of-the-art a-Si:H film deposition conditions in a reactor designed for a-Si:H solar cell fabrication. The diagnostics procedure measures the silane depletion in an RF plasma as a function of the silane flow rate (where the relationship is linear between 50-percent depletion, at a flow rate of 5.6 sccm, and about 8-percent depletion, at 80 sccm) and the RF power (where the silane depletion is linearly dependent on the RF power in the region of 4 to 12 W). The linear RF power dependence of the silane depletion is considered to be consistent with the mechanism of silane decomposition primarily by electron impact dissociations, while the flow rate dependence is interpreted in terms of the residence time of the SiH4 molecules in the glow discharge region, where an increase of the residence time at a low flow rate results in a high depletion ratio.

Shing, Y. H.↗
NASA NTRS2004

Spray Characteristics of a Hybrid Twin-Fluid Pressure-Swirl Atomizer

The spray performance of a fuel injection system applicable for use in main combustion chamber of an oxidizer-rich staged combustion (ORSC) cycles is presented. The experimental data reported here include mean drop size and drop size distribution, spray cone half-angle, and momentum rate (directly related to spray penetration). The maximum entropy formalism, MEF, method to predict drop size distribution is applied and compared to the experimental data. Geometric variables considered include the radius of the injector inlet orifice plate through which oxidizer flows (&) and the exposed length from the fuel inlet to the injector exit plane (L2). Operating conditions that were varied include the liquid mass flow rate and air mass flow rate. For orifices B and C there is a significant dependence of D3Z on both the air and liquid mass flow rates, as well as on L2. For the A orifice, the momentum rate of the air flow appears to exceed a threshold value above which a constant D32 is obtained. Using the MEF method, a semi-analytical process was developed to model the spray distribution using two input parameters (q = 0.4 and Dso). The momentum rate of the spray is directly related to the air and liquid mass flow rates. The cone half angle of the spray ranges from 25 to 17 degrees. The data resulting from this project will eventually be used to develop advanced rocket systems.

Durham, M. J.↗
NASA NTRS1993

Influence of heat transfer rates on pressurization of liquid/slush hydrogen propellant tanks

A multi-dimensional computational model of the pressurization process in liquid/slush hydrogen tank is developed and used to study the influence of heat flux rates at the ullage boundaries on the process. The new model computes these rates and performs an energy balance for the tank wall whereas previous multi-dimensional models required a priori specification of the boundary heat flux rates. Analyses of both liquid hydrogen and slush hydrogen pressurization were performed to expose differences between the two processes. Graphical displays are presented to establish the dependence of pressurization time, pressurant mass required, and other parameters of interest on ullage boundary heat flux rates and pressurant mass flow rate. Detailed velocity fields and temperature distributions are presented for selected cases to further illuminate the details of the pressurization process. It is demonstrated that ullage boundary heat flux rates do significantly effect the pressurization process and that minimizing heat loss from the ullage and maximizing pressurant flow rate minimizes the mass of pressurant gas required to pressurize the tank. It is further demonstrated that proper dimensionless scaling of pressure and time permit all the pressure histories examined during this study to be displayed as a single curve.

Sasmal, G. P.↗
NASA NTRS1994

Bubble Formation at a Submerged Orifice in Reduced Gravity

The dynamic regime of gas injection through a circular plate orifice into an ideally wetting liquid is considered, when successively detached bubbles may be regarded as separate identities. In normal gravity and at relatively low gas flow rates, a growing bubble is modeled as a spherical segment touching the orifice perimeter during the whole time of its evolution. If the flow rate exceeds a certain threshold value, another stage of the detachment process takes place in which an almost spherical gas envelope is connected with the orifice by a nearly cylindrical stem that lengthens as the bubble rises above the plate. The bubble shape resembles then that of a mushroom and the upper envelope continues to grow until the gas supply through the stem is completely cut off. Such a stage is always present under conditions of sufficiently low gravity, irrespective of the flow rate. Two major reasons make for bubble detachment: the buoyancy force and the force due to the momentum inflow into the bubble with the injected gas. The former force dominates the process at normal gravity whereas the second one plays a key role under negligible gravity conditions. It is precisely this fundamental factor that conditions the drastic influence on bubble growth and detachment that changes in gravity are able to cause. The frequency of bubble formation is proportional to and the volume of detached bubbles is independent of the gas flow rate in sufficiently low gravity, while at normal and moderately reduced gravity conditions the first variable slightly decreases and the second one almost linearly increases as the flow rate grows. Effects of other parameters, such as the orifice radius, gas and liquid densities, and surface tension are discussed.

Buyevich, Yu A.↗
NASA NTRS1995

Effects of Gravity on Bubble Formation at a Plate Orifice

A model of the dynamic regime of gas injection through a submerged plate orifice into an ideally wetting liquid is developed in the circumstance when successively detached bubbles may be regarded as independent objects. Two major factors favor bubble detachment: the buoyancy force and a force due to the momentum inflow into the bubble with injected gas. In normal and moderately reduced gravity, the first factor dominates. At relatively low flow rates, a growing bubble is modeled as a spherical segment touching the orifice perimeter during the whole period of its evolution till detachment. If the flow rate exceeds a critical value, another stage of bubble evolution occurs in which an almost spherical gas envelope is connected with the orifice by a nearly cylindrical gaseous stem that lengthens as the bubble rises above the plate. The bubble continues to grow until the gas supply through the stem is completely cut off, after which back flow of gas into the stem from the bubble becomes possible. In microgravity, the second factor prevails, and the latter stage is always present irrespective of the flow rate. However, the gas envelope rises and the stem lengthens very slowly. This difference in the underlying physical mechanisms provides for key properties of bubble growth and detachment being drastically different in appreciable and sufficiently reduced gravity. The frequency of bubble formation slightly decreases with and the detachment volume is almost proportional to the gas flow rate in the first case, in accordance with familiar relations. In the second case, the first variable is proportional to the flow rate whereas the second one is independent of it. Effects of other parameters, such as the orifice radius, gas and liquid densities, and surface tension are discussed.

Webbon, Bruce W.↗
NASA NTRS2001

Investigation of the Flow-Induced Vibration in the E2 Test Facility

An investigation of flow induced vibration due to coupling between the fluid flow and the propellants lines (LOX and RP-1) was performed. Various flow rate conditions were studied to check whether flow induced vibration was possible due to vortex shedding in both valves and pipe lines. Resonance test was conducted for all segments of the LOX-feedline for the preburner under test. In addition, critical values of frequency and velocity are calculated using a mass damping model. A simple chart characterizing the relation between frequency and velocity is developed for each component; i.e. propellant lines, valves and flow meters. It was found that flow induced vibration occurs for various segments with flow rates of 113 lb/s, 275 lb/s and 40 lb/s. Even more interesting using critical conditions for buckling, it was found that the valve or pipe may collapse for a flow rate of 275 lb/s and valve height of 10% of pipe diameter. Furthermore, two models for the acoustic pressure acting on the segments particularly for the valve are proposed.

Castillo, Luciano↗
NASA NTRS2001

Investigation of the Flow-Induced Vibration in the E2 Test Facility

An investigation of flow induced vibration due to coupling between the fluid flow and the propellants lines (LOX and RP-1) was performed. Various flow rate conditions were studied to check whether flow induced vibration was possible due to vortex shedding in both valves and pipe lines. Resonances test was conducted for all segments of the LOX-feedline for the preburner under test. In addition, critical values of frequency and velocity are calculated using a mass damping model. A simple chart characterizing the relation between frequency and velocity is developed for each component; i.e. propellant lines, valves and flow meters. It was found that flow induced vibration occurs for various segments with flow rates of 113 1b/s, 275 lb/s and 40 lb/s. Even more interesting using critical conditions for buckling, it was found that the valve or pipe may collapse for a flow rate of 275 lb/s and valve height of 10% of pipe diameter. Furthermore, two models for the acoustic pressure acting on the segments particularly for the valve are proposed.

Castillo, Luciano↗
NASA NTRS1999

Permeation Resistance of Chlorinated Polyethylene Against Hydrazine Fuels

The permeation resistance of chlorinated polyethylene (CPE) used in chemical protective clothing against the aerospace fuels hydrazine, monomethylhydrazine (MMH), and uns-dimethylhydrazine (UDMH) was determined by measuring breakthrough times and time-averaged vapor transmission rates using an ASTM F 739 permeation cell. Two exposure scenarios were simulated: a 2 hour (h) fuel vapor exposure, and a liquid fuel "splash" followed by a 2 h vapor exposure. To simulate internal suit pressure during operation, a positive differential pressure of 0.3 in. water (75 Pa) on the collection side of the permeation apparatus was used. Breakthrough was observed after exposure to liquid MMH, and to vapor and liquid UDMH. No breakthrough was observed after exposure to vapor and liquid hydrazine, or vapor MMH. A model was then used to calculate propellant concentrations inside a totally encapsulating chemical protective suit based on the ASTM permeation data obtained in the present study. Concentrations were calculated under conditions of fixed vapor transmission rate, variable breathing air flow rate, and variable splash exposure area. Calculations showed that the maximum allowable permeation rates of hydrazine fuels through CPE were of the order of 0.05 to 0.08 ng sq cm/min for encapsulating suits with low breathing air flow rates (of the order of 5 scfm or 140 L/min). Above these permeation rates, the 10 parts per billion (ppb) threshold limit value time - weighted average could be exceeded for chemical protective suits having a CPE torso. To evaluate suit performance at ppb level concentrations, use of a sensitive analytical method such as cation exchange high performance liquid chromatography with amperometric detection was found to be essential.

Waller, J. M.↗