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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 181 records · Page 10
All sourcesNASA NTRSDOE OSTI
NASA NTRS2016

Characterization of Carbon Dioxide Washout Measurement Techniques in the Mark-III Space Suit

It is essential to provide adequate carbon dioxide (CO2) washout in a space suit to reduce the risks associated with manned operations in space suits. Symptoms of elevated CO2 levels range from reduced cognitive performance and headache to unconsciousness and death at high levels of CO2. Because of this, NASA imposes limits on inspired CO2 levels for space suits when they are used in space and for ground testing. Testing and/or analysis must be performed to verify that a space suit meets CO2 washout requirements. Testing for developmental space suits has traditionally used an oronasal mask that collects CO2 samples at the left and rights sides of the mouth. Testing with this mask resulted in artificially elevated CO2 concentration measurements, which is most likely due to the dead space volume at the front of the mask. The mask also extends outward and into the supply gas stream, which may disrupt the washout effect of the suit supply gas. To mitigate these problems, a nasal cannula was investigated as a method for measuring inspired CO2 based on the assumptions that it is low profile and would not interfere with the designed suit gas flow path, and it has reduced dead space. This test series compared the performance of a nasal cannula to the oronasal mask in the Mark III space suit. Inspired CO2 levels were measured with subjects at rest and at metabolic workloads of 1000, 2000, and 3000 BTU/hr. Workloads were achieved by use of an arm ergometer or treadmill. Test points were conducted at air flow rates of 2, 4, and 6 actual cubic feet per minute, with a suit pressure of 4.3 psid. Results from this test series will evaluate the accuracy and repeatability across subjects of the nasal cannula collection method, which will provide rationale for using a nasal cannula as the new method for measuring inspired CO2 in a space suit. Proper characterization of sampling methods and of suit CO2 washout capability will better inform requirements definition and verification techniques for future CO2 washout limits in space suits

Meginnis, I↗
DOE OSTI2025

Selective chemical looping combustion of acetylene in ethylene-rich streams

Here, the requirement for C 2 H 2 concentrations below 2 parts per million (ppm) in gas streams for C 2 H 4 polymerization necessitates its semihydrogenation to C 2 H 4 . Here, we demonstrate selective chemical looping combustion of C 2 H 2 in C 2 H 4 -rich streams by Bi 2 O 3 as an alternative catalytic pathway to reduce C 2 H 2 concentration below 2 ppm. Bi 2 O 3 combusts C 2 H 2 with a first-order rate constant that is 3000 times greater than the rate constant for C 2 H 4 combustion. In successive redox cycles, the lattice O of Bi 2 O 3 can be fully replenished without discernible changes in local Bi coordination or C 2 H 2 combustion selectivity. Heterolytic activation of C–H bonds across Bi–O sites and the higher acidity of C 2 H 2 results in lower barriers for C 2 H 2 activation than C 2 H 4 , enabling selective catalytic hydrocarbon combustion leveraging differences in molecular deprotonation energies.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1982

Atomic fluorescence study of high temperature aerodynamic levitation

Ultraviolet laser induced atomic fluorescence has been used to characterize supersonic jet aerodynamic levitation experiments. The levitated specimen was a 0.4 cm sapphire sphere that was separately heated at temperatures up to 2327 K by an infrared laser. The supersonic jet expansion and thermal gradients in the specimen wake were studied by measuring spatial variations in the concentration of atomic Hg added to the levitating argon gas stream. Further applications of atomic fluorescence in containerless experiments, such as ideal gas fluorescence thermometry and containerless process control are discussed.

Nordine, P. C.↗
NASA NTRS2001

Thermal and Chemical Characterization of Non-metallic Materials Using Coupled Thermogravimetric Analysis and Infrared Spectroscopy

Thermogravimetric analysis (TGA) is widely employed in the thermal characterization of non-metallic materials, yielding valuable information on decomposition characteristics of a sample over a wide temperature range. However, a potential wealth of chemical information is lost during the process, with the evolving gases generated during thermal decomposition escaping through the exhaust line. Fourier Transform-Infrared spectroscopy (FT-IR) is a powerful analytical technique for determining many chemical constituents while in any material state, in this application, the gas phase. By linking these two techniques, evolving gases generated during the TGA process are directed into an appropriately equipped infrared spectrometer for chemical speciation. Consequently, both thermal decomposition and chemical characterization of a material may be obtained in a single sample run. In practice, a heated transfer line is employed to connect the two instruments while a purge gas stream directs the evolving gases into the FT-IR, The purge gas can be either high purity air or an inert gas such as nitrogen to allow oxidative and pyrolytic processes to be examined, respectively. The FT-IR data is collected real-time, allowing continuous monitoring of chemical compositional changes over the course of thermal decomposition. Using this coupled technique, an array of diverse materials has been examined, including composites, plastics, rubber, fiberglass epoxy resins, polycarbonates, silicones, lubricants and fluorocarbon materials. The benefit of combining these two methodologies is of particular importance in the aerospace community, where newly developing materials have little available data with which to refer. By providing both thermal and chemical data simultaneously, a more definitive and comprehensive characterization of the material is possible. Additionally, this procedure has been found to be a viable screening technique for certain materials, with the generated data useful in the selection of other appropriate analytical procedures for further material characterization.

Huff, Timothy L.↗
NASA NTRS2002

Thermal and Chemical Characterization of Non-Metallic Materials Using Coupled Thermogravimetric Analysis and Infrared Spectroscopy

Thermogravimetric analysis (TGA) is widely employed in the thermal characterization of non-metallic materials, yielding valuable information on decomposition characteristics of a sample over a wide temperature range. However, a potential wealth of chemical information is lost during the process, with the evolving gases generated during thermal decomposition escaping through the exhaust line. Fourier Transform-Infrared spectroscopy (FT-IR) is a powerful analytical technique for determining many chemical constituents while in any material state, in this application, the gas phase. By linking these two techniques, evolving gases generated during the TGA process are directed into an appropriately equipped infrared spectrometer for chemical speciation. Consequently, both thermal decomposition and chemical characterization of a material may be obtained in a single sample run. In practice, a heated transfer line is employed to connect the two instruments while a purge gas stream directs the evolving gases into the FT-IR. The purge gas can be either high purity air or an inert gas such as nitrogen to allow oxidative and pyrolytic processes to be examined, respectively. The FT-IR data is collected realtime, allowing continuous monitoring of chemical compositional changes over the course of thermal decomposition. Using this coupled technique, an array of diverse materials has been examined, including composites, plastics, rubber, fiberglass epoxy resins, polycarbonates, silicones, lubricants and fluorocarbon materials. The benefit of combining these two methodologies is of particular importance in the aerospace community, where newly developing materials have little available data with which to refer. By providing both thermal and chemical data simultaneously, a more definitive and comprehensive characterization of the material is possible. Additionally, this procedure has been found to be a viable screening technique for certain materials, with the generated data useful in the selection of other appropriate analytical procedures for further material characterization.

Huff, Timothy L.↗
NASA NTRS2004

Part 1 of a Computational Study of a Drop-Laden Mixing Layer

This first of three reports on a computational study of a drop-laden temporal mixing layer presents the results of direct numerical simulations (DNS) of well-resolved flow fields and the derivation of the large-eddy simulation (LES) equations that would govern the larger scales of a turbulent flow field. The mixing layer consisted of two counterflowing gas streams, one of which was initially laden with evaporating liquid drops. The gas phase was composed of two perfect gas species, the carrier gas and the vapor emanating from the drops, and was computed in an Eulerian reference frame, whereas each drop was tracked individually in a Lagrangian manner. The flow perturbations that were initially imposed on the layer caused mixing and eventual transition to turbulence. The DNS database obtained included transitional states for layers with various liquid mass loadings. For the DNS, the gas-phase equations were the compressible Navier-Stokes equations for conservation of momentum and additional conservation equations for total energy and species mass. These equations included source terms representing the effect of the drops on the mass, momentum, and energy of the gas phase. From the DNS equations, the expression for the irreversible entropy production (dissipation) was derived and used to determine the dissipation due to the source terms. The LES equations were derived by spatially filtering the DNS set and the magnitudes of the terms were computed at transitional states, leading to a hierarchy of terms to guide simplification of the LES equations. It was concluded that effort should be devoted to the accurate modeling of both the subgridscale fluxes and the filtered source terms, which were the dominant unclosed terms appearing in the LES equations.

Okong'o, Nora A.↗
NASA NTRS1973

Ecology and thermal inactivation of microbes in and on interplanetary space vehicle components

An experimental sterilization facility was developed to simulate conditions that will be encountered during terminal sterilization of space vehicles. The system consists of a temperature controlled oven with a nitrogen gas stream containing a known concentration of water. Moisture analyzers are utilized to monitor the gas flowing over spore samples contained in the oven. In its original configuration, no provision was made for the control of water vapor during the sterilization cycle. Because moisture profoundly influences the thermal inactivation of bacterial spores, an upper limit for the moisture content in the gas used to sterilize the space vehicle was established (25% RH at 0 C STP). Accordingly, a controller was developed and installed to provide these conditions in the experimental sterilization facility.

Wimsatt, J. C.↗
NASA NTRS1979

Chemical-vapor-deposition reactor

Reactor utilizes multiple stacked trays compactly arranged in paths of horizontally channeled reactant gas streams. Design allows faster and more efficient deposits of film on substrates, and reduces gas and energy consumption. Lack of dead spots that trap reactive gases reduces reactor purge time.

Chern, S.↗
NASA NTRS1959

Experimental Investigation of Coaxial Jet Mixing of Two Subsonic Streams at Various Temperature, Mach Number, and Diameter Ratios for Three Configurations

An experimental investigation of the mixing of two coaxial gas streams was conducted over a range of subsonic jet Mach numbers and temperatures. Three configurations were investigated. One had no innerbody in the primary or inner pipe and was designed to give flat velocity profiles at the exit of the primary pipe. The other two configurations had innerbodies in the primary pipe. These were designed to give velocity profiles similar to those existing at the inlet of propulsive systems such as afterburners. Curves of axial velocity and temperature profiles across the radius are presented at various axial stations. For the two configurations with the innerbody, data are shown at stations out to approximately 8 primary-pipe diameters from the exit of the primary pipe. For the flat-velocity-profile configuration, data are shown at distances extending downstream at 22 primary-pipe diameters from the exit of the primary pipe.

Burley, Richard R.↗
NASA NTRS1965

Instrument calibrates low gas-rate flowmeters

Electronically measuring the transit time of a soap bubble carried by the gas stream between two fixed points in a burette calibrates flowmeters used for measuring low gas-flow rates.

Copeland, A. C.↗
NASA NTRS1988

Mass flow in the interacting binary TX Ursae Majoris

Twenty-two far-ultraviolet and 23 near-ultraviolet high resolution IUE spectra of the interactive Algol-type binary TX Ursae Majoris (B8 V + F-K III-IV) were analyzed in order to determine the nature of the mass flow occurring in this system. Absorption features due to high-temperature ions of Si IV, C IV, and N V are always present. The resonance lines of Al III, Fe II, Mg II and Si IV show strong phase and secular variations indicative of gas streaming and circumstellar/circumbinary material. Radial velocities as high as 500 to 600 km/sec are present. The gas flow is particularly prominent in 1985 between phases 0.7 and 0.0. The system is more active than U Sagittae and as active as U Cephei.

Mccluskey, G. E., Jr.↗
DOE OSTI2025

Investigation of the Mechanical Degradation of Zinc-Based Cold Spray Coatings for Steel Pipelines

Internal corrosion in wet natural gas is a big challenge in the oil and gas industry due to corrosive constituents such as carbon dioxide (CO2), hydrogen sulfide (H2S), other forms of sulfur, and water in the gas stream. To mitigate internal corrosion, zinc-based cold spray coatings were designed for use in natural gas pipelines to increase the lifespan of the pipeline network. However, one of the requirements in designing internal coatings is the resistance of the coatings to mechanical forces applied on the pipeline's internal wall during pigging operations. These forces are primarily compressive and shear/friction forces. This study examines material properties that must be considered when evaluating mechanical considerations.

adhesion↗
DOE OSTI2025

Investigation of the Mechanical Degradation of Zinc-Based Cold Spray Coatings for Steel Pipelines

Internal corrosion in wet natural gas is a big challenge in the oil and gas industry due to corrosive constituents such as carbon dioxide (CO2), hydrogen sulfide (H2S), other forms of sulfur, and water in the gas stream. To mitigate internal corrosion, zinc-based cold spray coatings were designed for use in natural gas pipelines to increase the lifespan of the pipeline network. However, one of the requirements in designing internal coatings is the resistance of the coatings to mechanical forces applied on the pipeline's internal wall during pigging operations. These forces are primarily compressive and shear/friction forces. This study examines material properties that must be considered when evaluating mechanical considerations. To determine the viability of the developed coatings with respect to the shear/friction forces, the shear adhesion and wear resistance of the materials have been evaluated. Shear adhesion testing was performed with modified clevises to determine the shear stress required to cause adhesion failure at the coating/substrate interface. Scanning electron microscopy was utilized to characterize the interfaces after failure. Wear testing was performed on coatings and pipeline materials utilizing pin-on-drum testing. These tests display the stress limitations and wear that the coatings can tolerate from pigging.

mechanical degradation↗
DOE OSTI2024

Integrated Off-gas System: A Preconceptual Design of an Integrated Off-Gas Treatment System

The U.S. has a vested interest in the advancement of nuclear energy to achieve aggressive net-zero goals, with reprocessing and recycling of used nuclear fuels (UNF) playing a vital role. It will not be possible to meet U.S. regulatory requirements without robust off-gas treatment, so it is crucial to advance treatment technologies to facilitate the design of future reprocessing facilities. For many years, teams of researchers across the U.S. Department of Energy (DOE) National Laboratory complex have been investigating off-gas treatment technologies for the capture and removal of volatile radionuclides (i.e., 85 Kr, Xe, 14 C, and 129 I) and oxides of nitrogen (NO X ) that are produced from reprocessing. These investigations have been focused on developing individual technologies for the capture of Kr, Xe, iodine, and CO 2 . Capture technologies for each constituent were tested independently from one another by utilizing nonradioactive surrogates to simulate simplified off-gas streams. The tests have been relatively small, laboratory-scale experiments of up to approximately 1 L/minute total gas flow rate. To increase the readiness of these technologies for deployment, an integrated test system with a larger-scale capacity is needed to bridge the gap between promising bench scale and fully scalable UNF reprocessing off-gas treatment. This document contains the goals, design basis, functional requirements, preconceptual design, and cost estimates for an integrated off-gas demonstration system for the capture and removal of NO x , Kr, Xe, CO 2 , and iodine at 10× higher throughput than earlier laboratory studies. The order-of-magnitude cost estimate for this system is approximately $\$$886,000. Next phases include conceptual design, detailed design, fabrication, and commissioning.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS1986

Experiments for the determination of convective diffusion heat/mass transfer to burner rig test targets comparable in size to jet stream diameter

The application of a recently formulated vapor transport theory to predict deposition rates of corrosive salts from alkali-seeded combustion gases of a small-capacity, high-velocity, atmospheric-pressure burner rig was hampered by the relatively large dimensions of the cylindrical deposit collector compared to the diameter of the combustion gas stream. The relative dimensions lead to a highly nonadiabatic combustion gas flow around the collector and necessitate two series of experiments. In the first series, mass transfer coefficients are determined by utilizing the naphthalene sublimation technique. The second series of experiments determines the dilution effect on the sodium species concentrations due to the entrainment of ambient air. This second series involves the measurement of the temperature variation along the surface of the collector under steady state conditions. Vapor deposition rates are determined exploiting this information and the results are found to compare favorably with experimentally obtained rates.

Santoro, G. J.↗
NASA NTRS1988

Experiments for the determination of convective diffusion heat/mass transfer to burner rig test targets comparable in size to jet stream diameter

The application of a recently formulated vapor transport theory to predict deposition rates of corrosive salts from alkali-seeded combustion gases of a small-capacity, high-velocity, atmospheric-pressure burner rig was hampered by the relatively large dimensions of the cylindrical deposit collector compared to the diameter of the combustion gas stream. The relative dimensions lead to a highly nonadiabatic combustion gas flow around the collector and necessitate two series of experiments. In the first series, mass transfer coefficients are determined by utilizing the naphthalene sublimation technique. The second series of experiments determines the dilution effect on the sodium species concentrations due to the entrainment of ambient air. This second series involves the measurement of the temperature variation along the surface of the collector under steady state conditions. Vapor deposition rates are determined exploiting this information and the results are found to compare favorably with experimentally obtained rates.

Santoro, G. J.↗
NASA NTRS1974

Research on miniature gas analysis systems

Technology for fabricating very small valves, whose function will be to introduce a small sample of the gas to be analyzed into the main carrier gas stream flowing through the chromatograph column is described. In addition, some analyses were made of the factors governing the resolution of gas chromatographs, particularly those with miniature columns. These analyses show how important the column lining thickness is in governing the ability of a miniature column to separate components of an unknown gas. A brief description of column lining factors is included. Preliminary work on a super small thermistor detector is included.

Angell, J. B.↗