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The effect of sodium chloride on unstressed, transverse, tensile, metal specimens at elevated temperatures was determined. Results indicate that the mechanical properties of Inconel 718, Rene 41, titanium base alloy 13V-11Cr-3Al, Hastelloy X, HS25 (L605), HS188, and TDNiCr suffer degradation in tensile strength and ductility due to hot salt exposure.
Research was carried out to determine whether an oxide dispersion hardened alloy, TD-Ni, Cr, and low volume fraction gamma prime strengthened nickel-base alloy, Modified Waspaloy, were susceptible to time-dependent edge-notch sensitivity. The results were evaluated in terms of the mechanical characteristics of the alloys and the dislocation motion mechanisms operative. As far as could be determined, the results of the investigation were consistent with the following important concepts developed for Waspaloy and Inconel 718: (1) Time-dependent edge-notch sensitivity occurs when notched specimens are loaded below the approximate 0.2 percent smooth specimen offset yield strength and when data from smooth specimens indicate that small amounts of creep consume large rupture life fractions. (2) When precipitate particles are sheared by dislocations, the deformation is localized and time-dependent notch sensitivity occurs. When dislocations by-pass precipitate particles the deformation is homogeneous. Under these conditions, no time-dependent notch sensitivity has been observed.
Embrittlement, or the enhancement of crack growth by gaseous hydrogen in high strength alloys, is of primary interest in selecting alloys for various components in the space shuttle. Embrittlement is known to occur at hydrogen gas pressures ranging from fractions to several hundred atmospheres, and is most severe in the case of martensitic high strength steels. Kinetic information on subcritical crack growth in gaseous hydrogen is sparse at this time. Corroborative information on hydrogen adsorption and diffusion is inadequate to permit a clear determination of the rate controlling process and possible mechanism in hydrogen enhanced crack growth, and for estimating behavior over a range of temperatures and pressures. Therefore, coordinated studies of the kinetics of crack growth, and adsorption and diffusion of hydrogen, using identical materials, have been initiated. Comparable conditions of temperature and pressure will be used in the chemical and mechanical experiments. Inconel 718 alloy and 18Ni(200) maraging steel have been selected for these studies. Results from these studies are expected to provide not only a better understanding of the gaseous hydrogen embrittlement phenomenon itself, but also fundamental information on hydrogen adsorption and diffusion, and crack growth information that can be used directly for design.
The engineering, design, and fabrication status of the expansion joint unit (EJU) to be employed in the NaK primary coolant piping loop of the 5-kwe Reactor thermoelectric system are described. Four EJU's are needed in the NaK primary coolant piping loop. The four EJU's which will be identical, utilize bellows as the flexing member, are hermetically sealed, and provide double containment. The bellows are of a nested-formed design, and are to be constructed of 1-ply thickness of 0.010-in. Inconel 718. The EJU's provide a minimum piping load margin of safety of +0.22.
The engineering, design, and fabrication status of the volume accumulator units to be employed in the NaK primary and secondary coolant loops of the 5-kwe reactor thermoelectric system are described. Three identical VAU's are required - two for the primary coolant loop, and one for the secondary coolant loop. The VAU's utilize nested-formed bellows as the flexing member, are hermetically sealed, provide double containment and utilize a combination of gas pressure force and bellows spring force to obtain the desired pressure regulation of the coolant loops. All parts of the VAU, except the NaK inlet tube, are to be fabricated from Inconel 718.
Low temperature electrical resistivity was used to determine the material variability (1) between different manufacturers, (2) between different heats from the same manufacturer, and (3) within a given heat for Al 2024, Al-5% Mg alloys, Inconel 718, A286 stainless, and AISI 316. Generally, the coefficient of variation for solution annealed alloys ranged from 1.2 to 14% between manufacturers, 0.8 to 5.1% between heats, and 0.1 to 1.6% within a heat with stainless steels at the low ends and Al 2024 at the high ends. The variability is increased if the material is in a precipitation-hardened condition. A statistical analysis suggests that the variability within a heat is non-normal.
A disk crack detector is discussed which is intended to operate under flight conditions. It monitors the disk rim for surface cracks emanating from the blade root interface. An eddy current type sensor, with a remotely located capacitance/conductance bridge and signal analyzer, can reliably detect a simulated crack 3 mm long. The sensor was tested on a spinning turbine disk at 540 C. Tests indicate that the system is useful at disk rim velocities to 460 m/sec. By using fracture mechanics, it is shown for Inconel 718 th at a crack operating under a rim stress of 34 x ten to the 7th power N/sqm has a critical length of 18 mm.
Strain-cycling fatigue behavior of 10 different structural alloys and metals was investigated in liquid helium (4 K), in liquid nitrogen (78 K), and in ambient air (300 K). At high cyclic lives, fatigue resistance increased with decreasing temperature for all the materials investigated. At low cyclic lives, fatigue resistance generally decreased with decreasing temperature for the materials investigated. Only for Inconel 718 did fatigue resistance increase with decreasing temperature over the entire life range investigated. Comparison of the experimental fatigue behavior with that predicted by the Manson method of universal slopes showed that the fatigue behavior of these materials can be predicted for cryogenic temperatures by using material tensile properties obtained at those same temperatures.
Time dependent notch sensitivity was observed in Udimet 700 sheet, bar, and investment castings between 1000 and 1400 F (538 -760 C), but not at 1600 F (871 C). As was the case for modified Waspaloy, Waspaloy and Inconel 718, it occurred in notched specimens loaded below the yield strength when the creep deformation was localized. For each alloy and notched specimen geometry, a stress-average particle size zone can be defined that characterizes the notch sensitive behavior.
Methods were developed for fabrication of a solid four pole alternator rotor by hot isostatic pressure welding. The rotor blanks welded in this program had complex geometrical mating interfaces and were of considerable bulk, being approximately 3-1/2 inches (0.089 meters) in diameter and 14 inches (0.356 meters) long. Magnetic end pieces were machined from AlSl 4340 steel, while the non-magnetic central section was of Inconel 718. Excellent welds were produced which were shown to be responsive to post weld heat treatments which substantially improved joint strength. Prior to welding the rotors, test specimens of complex geometry were welded to demonstrate that complex surfaces with intentional mechanical misfit could be readily joined using HIP welding. This preliminary work demonstrated not only that interface compliance is achieved during welding but that welding pressure is developed in these thick sections sufficient to produce sound joints. Integral weld-heat treatment cycles were developed that permitted the attainment of magnetic properties while minimizing residual stress associated with the allotropic transformation of 4340 steel.
A disk crack detector is discussed which is intended to operate while in flight. The crack detector monitors the disk rim for radial surface cracks emanating from the blade root interface. An eddy current type sensor with a remotely located capacitance-resistance bridge and signal analyzer is able to detect reliably a simulated crack 1/8 in. long. The sensor was tested at rim velocities of 600 fps and at 1000 F. Fracture mechanics is used to calculate the critical crack length. Knowledge of the crack growth rate permits the calculation of the number of stress cycles remaining for the detected crack to grow to critical size. A plot is presented of the remaining life as a function of the critical crack length and the operating stress. It is shown that for a disk of Inconel 718 a through-the-thickness crack operating under a rim stress of 50 kpsi has a critical length of 0.7-in. and a remaining life of 130 flights.
Five nickel-base alloys (Inconel 718, Udimet 700, Rene 41, Hastelloy X, and TD-NiCr), one cobalt-base alloy (L-605), and an iron-base alloy (A-286) were exposed in hydrogen at 0.1 MN/sq m (15 psi) at several temperatures in the range from 430 to 980 C for as long as 1000 hours. These alloys were embrittled to varying degrees by such exposures in hydrogen. Embrittlement was found to be: (1) sensitive to strain rate, (2) reversible, (3) caused by large concentrations of absorbed hydrogen, and (4) not associated with any detectable microstructural changes in the alloys. These observations are consistent with a mechanism of internal reversible hydrogen embrittlement.
Results of sustained-load environmental crack growth threshold tests performed on six spacecraft pressure vessel alloys are presented. The alloys were Inconel 718, 6Al-4V titanium, A-286 steel, AM-350 stainless steel, cryoformed AISI 301 stainless steel; and cryoformed AISI 304L steel. The test environments for the program were air, pressurized gases of hydrogen, oxygen, nitrogen, and carbon dioxide, and liquid environments of distilled water, sea water, nitrogen tetroxide, hydrazine, aerozine 50, monomethyl hydrazine, and hydrogen peroxide. Surface flaw type specimens were used with flaws located in both base metal and weld metal.
Time-dependent notch sensitivity of Udimet 700 sheet, bar, and investment castings was observed between 1000 and 1400 F (538-760 C) but not at 1600 F (871 C). As was the case for Modified Waspaloy, Waspaloy, Rene 41, Inconel 718, and TD-NiCr, it occurred when notched specimens were loaded below the yield strength and when creep deformation was localized. For each gamma-prime strengthened alloy and notched specimen geometry, a stress-average particle size zone can be defined to characterize the notch-sensitive behavior.
Stress corrosion cracking susceptability in presence of hydrazine is examined for 6061-T6, Ti-6A1-4V(STA), Inconel 718, 410 stainless steel, and 4130 steel alloys.
Study examines and reports positive findings from suitability tests of metal alloys, Inconel 718 and Ti-6A1-4V and elastomers, Ethylene propylene terpolymer rubbers, for utilization in storage vessels, fluid lines, and other system components subjected to continuous immersion in liquid anhydrous ammonia.
Unnotched and notched tensile properties of stressed and unstressed specimens of wrought 316 stainless steel, Incology 903, Monel K-500, and cast specimens of Inconel 718 were examined. Environmental tests were performed in atmospheric pressure air, high pressure nitrogen, and high pressure oxygen. Results show that oxygen did not alter the tensile properties of any of the alloys studied.
It is recognized that the use of overwrapped pressure vessels with load sharing liners may provide significant weight savings for high pressure gas containment in Space Shuttle Orbiter systems. The technology readiness to produce Kevlar wound vessels with load sharing liners of titanium 6Al-4V, Inconel 718 or cryoformed 301 steel has been demonstrated. It has been estimated that about 400 lbs can be saved in the Orbiter by using overwrapped vessels with load sharing liners instead of monolithic metal designs. Total weight of the composite vessels would be about 1350 lbs as opposed to about 1750 lbs for all-metal vessels.