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Radial immunodiffusion for serum proteins quantitation adapted to capillary blood and compared with results for venous blood
Quantitative analytic composite photography, performing image density point-to-point subtraction of two negatives
Quantitative and qualitative analysis of biochemically and radiobiologically important thiols and disulfides via gas-liquid chromatography
Quantitative optical and electron probe studies of opaque phases in Apollo 11 lunar rocks
Quantitative gas-liquid chromatography of histidine, using N-TFA n-butyl ester derivatives and histidine converted trimethylsilyl derivative
Quantitative radiance measurements in visible region from ATS 1 spin-scan camera
Quantitative microluminescence analysis of lunar glasses and fines
Quantitative evaluation of multiband photographic techniques using combination of black and white and color photos
Quantitative determination of optical imperfection by mathematical analysis of Foucault knife edge test pattern in large orbiting telescope
Quantitative determination of phenylalanine in serum by gas-liquid chromatographic analysis method
Videometer instrument for solar flares quantitative measurement, eliminating red sensitive vidicon for real time operation in H alpha region
Methods were developed for quantitative analysis by X-ray diffraction of the oxides Al2O3, NiO, Cr2O3, CoO, and CoCr2O4 within a standard deviation of about 10 percent of the weight fraction reported or within 1 percent absolute. These error limits assume that the sample oxides are well characterized and that the physiochemical structure of the oxides in the samples are identical with those in the synthesized standards. Results are given for the use of one of the techniques in the analysis of spalls from a series of oxidation tests of the cobalt base alloy WI-52.
Papers on Raman and soft X-ray spectroscopy of lunar glasses and electron microscopy of lunar fines are presented. Individual particles of glasses from Apollo 11, 12, 14, and 15 samples were analyzed separately. Silicon emission shifts vary between parent rock types and can be interpreted as a range of Si-O distances from 1.612 to 1.637 A. Aluminum emission shifts relate to the amount of 4- and 6-coordinated Al in the glass. Raman spectra show broadened bands. Certain bands recur in many specimens and relate to the main normative minerals for the glass bulk composition, olivine, pyroxene, and anorthite. Quantitative size and shape analyses were carried out on six Apollo 14 and 15 samples of fines by computer evaluation of scanning electron microspace images. For the size range of 0.50 to 30 micron diameter, the distributions are log-normal on a number count basis. Aspect ratios range from 0.1 to 1.0 with an average value of about 0.6. The aspect ratios and a shape complexity factor vary only slightly among the samples.
Ultrasonic instrument has been developed for use in quantitative nondestructive evaluation of material defects such as cracks, voids, inclusions, and unbonds. Instrument is provided with standard pulse source and transducer for each frequency range selected and includes integral aids that allow calibration to prescribed standards.
Lidar uses laser energy in radar fashion to observe atmospheric backscattering as a function of range. Because of the short optical and near-optical wavelengths used, very small particles and even the gaseous molecules cause significant scattering. This can complicate the evaluation of the observations by introducing attenuation along the path as a second unknown into the lidar equation. In many cases, however, the observations may be interpreted directly on a qualitative basis and show the distribution of particulate matter in clear air or enable the dimensions of visible cloud to be measured accurately. In other cases, particularly where additional data are available, quantitative solutions can provide useful information on remote targets such as tenuous smoke clouds or haze layers. Examples of such observations are given, illustrating the computational approach to the evaluation of the volume concentration of natural dust and haze layers in the lower atmosphere and the mass concentration of a smoke plume. In both cases lidar data are related to independently obtained data on the particulate concentrations involved.
Hydrogen-induced slow crack growth, da/dt, was studied in AISI-SAE 4130 low alloy steel in gaseous hydrogen and distilled water environments as a function of applied stress intensity, K, at various temperatures, hydrogen pressures, and alloy strength levels. At low values of K, da/dt was found to exhibit a strong exponential K dependence (Stage 1 growth) in both hydrogen and water. At intermediate values of K, da/dt exhibited a small but finite K dependence (Stage 2), with the Stage 2 slope being greater in hydrogen than in water. In hydrogen, at a constant K, (da/dt) sub 2 varied inversely with alloy strength level and varied essentially in the same complex manner with temperature and hydrogen pressure as noted previously. The results of this study provide support for most of the qualitative predictions of the lattice decohesion theory as recently modified by Oriani. The lack of quantitative agreement between data and theory and the inability of theory to explain the observed pressure dependence of slow crack growth are mentioned and possible rationalizations to account for these differences are presented.
Quantitative models of the external magnetospheric field were derived by making least-squares fits to magnetic field measurements from four IMP satellites. The data were fit to a power series expansion in the solar magnetic coordinates and the solar wind-dipole tilt angle, and thus the models contain the effects of seasonal north-south asymmetries. The expansions are divergence-free, but unlike the usual scalar potential expansions, the models contain a nonzero curl representing currents distributed within the magnetosphere. Characteristics of four models are presented, representing different degrees of magnetic disturbance as determined by the range of Kp values. The latitude at the earth separating open polar cap field lines from field lines closing on the dayside is about 5 deg lower than that determined by previous theoretically-derived models. At times of high Kp, additional high latitude field lines are drawn back into the tail.
The Mead-Fairfield geomagnetic field models were used to trace field lines between the outer magnetosphere and the earth's surface. The results are presented in terms of ground latitude and local time contours projected to the equatorial plane and into the geomagnetic tail. With these contours various observations can be mapped along field lines between high and low altitudes. Low altitudes observations of the polar cap boundary, the polar cusp, the energetic electron trapping boundary and the sunward convection region are projected to the equatorial plane and compared with the results of the model and with each other. The results provide quantitative support to the earlier suggestions that the trapping boundary is associated with the last closed field line in the sunward hemisphere, the polar cusp is associated with the region of the last closed field line, and the polar cap projects to the geomagnetic tail and has a low latitude boundary corresponding to the last closed field line.