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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 181 records · Page 10
All sourcesNASA NTRSDOE OSTI
NASA NTRS2006

Probabilistic Classification Using Elemental Abundance Distributions and Lossless Image Compression in Apollo 17 Lunar Dust Samples from Mare Serenitatis

We have previously outlined a strategy for the detection of fossils [Storrie-Lombardi and Hoover, 2004] and extant microbial life [Storrie-Lombaudi and Hoover, 20051 during robotic missions to Mars using co-registered structural and chemical signatures. Data inputs included image lossless compression indices to estimate relative textural complexity and elemental abundance distributions. Two exploratory classification algorithms (principal component analysis and hierarchical cluster analysis) provide an initial tentative classification of all targets. Nonlinear stochastic neural networks are then trained to produce a Bayesian estimate of algorithm classification accuracy. The strategy previously has been successful in distinguishing regions of biotic and abiotic alteration of basalt glass from unaltered samples. [Storrie-Lombardi and Fisk, 2004; Storrie-Lombardi and Fisk, 2004] Such investigations of abiotic versus biotic alteration of terrestrial mineralogy on Earth are compromised by .the difficulty finding mineralogy completely unaffected by the ubiquitous presence of microbial life on the planet. The renewed interest in lunar exploration offers an opportunity to investigate geological materials that may exhibit signs of aqueous alteration, but are highly unlikely to contain contaminating biological weathering signatures. We here present an extension of our earlier data set to include lunar dust samples obtained during the Apollo 17 mission. Apollo 17 landed in the Taurus-Littrow Valley in Mare Serenitatis. Most of the rock samples from this region of the lunar highlands are basalts comprised primarily of plagioclase and pyroxene and selected examples of orange and black volcanic glass. SEM images and elemental abundances (C6, N7, O8, Na11, Mg12, Al13, Si14, P15, S16, Cll7, K19, Ca20, Fe26) for a series of targets in the lunar dust samples are compared to the extant cyanobacteria, fossil trilobites, Orgueil meteorite, and terrestrial basalt targets previously discussed. The data set provides a first step in producing a quantitative probabilistic methodology for geobiological analysis of returned lunar samples or in situ exploration.

Storrie-Lombardi, Michael C.↗
DOE OSTI2024

Electrofracturing of Shale at Elevated Pressure

Electrofracturing deeply buried shale formations could be used to increase reservoir permeability and improve reservoir production without requiring large volumes of freshwater. This paper describes a novel experimental system and initial test results to electrofracture shale under high confining pressures. Core-scale laboratory testing was performed on twelve rock samples recovered from a shale gas reservoir. Each sample was subjected to confining pressures of 20.7 MPa (3000 psi) or 58.6 MPa (8000 psi), representative of overburden pressures at depth. Samples were then subjected to application of high voltage until specimen fracture. The experiments produced deformed samples with multiple fracture types, both parallel and oblique to bedding planes. Electrofracturing increased permeabilities by up to nine orders of magnitude for extended time periods. Rock fracture and throughgoing fractures were demonstrated. Computed tomography images revealed the creation of fractures and tube/tunnel flow channels, which resisted closure under hydrostatic pressures up to 58.6 MPa. The breakdown energy and permeability changes in the sample were independent of applied confining pressure. The cumulative energy input required for fracture depended on applied confining pressure and sample length. The energy required to fracture samples up to 9 cm in length is generally more than 0.5 kJ/cm, but no greater than 1 kJ/cm. Our results show that electrofracture of shales under confining pressure is possible and could be a possible water-free mechanism for reservoir stimulation.

04 OIL SHALES AND TAR SANDS↗
NASA NTRS1972

Magnetic hysteresis classification of the lunar surface and the interpretation of permanent remanence in lunar surface samples

A magnetic hysteresis classification of the lunar surface is presented. It was found that there is a distinct correlation between natural remanence (NRM), saturation magnetization, and the hysteresis ratios for the rock samples. The hysteresis classification is able to explain some aspects of time dependent magnetization in the lunar samples and relates the initial susceptibility to NRM, viscous remanence, and to other aspects of magnetization in lunar samples. It is also considered that since up to 60% of the iron in the lunar soil may be super paramagnetic at 400 K, and only 10% at 100 K, the 50% which becomes ferromagnetic over the cycle has the characteristics of thermoremanence and may provide for an enhancement in measurable field on the dark side during a subsatellite magnetometer circuit.

Wasilewski, P.↗
NASA NTRS2012

Apollo Lunar Sample Photograph Digitization Project Update

This is an update of the progress of a 4-year data restoration project effort funded by the LASER program to digitize photographs of the Apollo lunar rock samples and create high resolution digital images and undertaken by the Astromaterials Acquisition and Curation Office at JSC [1]. The project is currently in its last year of funding. We also provide an update on the derived products that make use of the digitized photos including the Lunar Sample Catalog and Photo Database[2], Apollo Sample data files for GoogleMoon[3].

Todd, N. S.↗
NASA NTRS1985

The age and emplacement of obducted oceanic crust in the Urals from Sm-Nd and Rb-Sr systematics

The Sm-Nd and Rb-Sr isotopic characteristics of two mafic-ultramafic bodies, the Kemperai Massif in the South Ural Mountains and the Voykar-syninsky Massif in the Polar Ural mountains are examined. The data are found to be consistent with the hypothesis that these bodies represent fragments of old oceanic crust. Whole rock samples of pillow basalt, troctolite, gabbros, diabase, and a metasediment give Sm-Nd values which lie on this isochron indicating that the rock units are genetically related and formed 397 My ago. Basic and ultrabasic rocks from Kempersai and Voykar-Syninsky have an initial isotopic composition at time T, epsilon Nd(397 My), of +8.4, indicating derivation for an ancient depleted mantle source. The Sr isotopic data and the correlation with epsilon Nd indicate extensive alteration by seawater which is particularly strong on ultrabasic rocks. The results show that the segments of oceanic crust formed at least 80 My before the collision that produced the Urals.

Edwards, R. L.↗
NASA NTRS1972

Apollo 14 and 15 samples - Rb-Sr ages, trace elements, and lunar evolution.

Studies concerning Rb-Sr isotopic relations are discussed together with abundance measurements regarding K, Rb, Sr, and Ba in Apollo 14 and 15 rocks and soils. The studies include age determination by the internal isochron technique on one basaltic rock sample from each of the two missions. In addition, total sample measurements have been made on samples of fines material from both missions. Trace element abundances and Rb-Sr systematics in the various grain size fractions of three of the fines have also been analyzed.

Murthy, V. R.↗
NASA NTRS1997

Raman Spectroscopy for Mineral Identification and Quantification for in situ Planetary Surface Analysis: A Point Count Method

Quantification of mineral proportions in rocks and soils by Raman spectroscopy on a planetary surface is best done by taking many narrow-beam spectra from different locations on the rock or soil, with each spectrum yielding peaks from only one or two minerals. The proportion of each mineral in the rock or soil can then be determined from the fraction of the spectra that contain its peaks, in analogy with the standard petrographic technique of point counting. The method can also be used for nondestructive laboratory characterization of rock samples. Although Raman peaks for different minerals seldom overlap each other, it is impractical to obtain proportions of constituent minerals by Raman spectroscopy through analysis of peak intensities in a spectrum obtained by broad-beam sensing of a representative area of the target material. That is because the Raman signal strength produced by a mineral in a rock or soil is not related in a simple way through the Raman scattering cross section of that mineral to its proportion in the rock, and the signal-to-noise ratio of a Raman spectrum is poor when a sample is stimulated by a low-power laser beam of broad diameter. Results obtained by the Raman point-count method are demonstrated for a lunar thin section (14161,7062) and a rock fragment (15273,7039). Major minerals (plagioclase and pyroxene), minor minerals (cristobalite and K-feldspar), and accessory minerals (whitlockite, apatite, and baddeleyite) were easily identified. Identification of the rock types, KREEP basalt or melt rock, from the 100-location spectra was straightforward.

Haskin, Larry A.↗
NASA NTRS1975

Specific gravities of lunar materials using helium pycnometry

An existing technique, helium pycnometry, has been adapted for the measurement of specific gravities of lunar samples, where surface areas are low (less than 1 sq m/g) and crushing the sample to a fine powder is highly undesirable. The technique is superior to typical liquid immersion methods, in that it is noncontaminating and, where vuggy or porous samples are concerned, should provide a more accurate (higher) absolute density value. The experimental helium pycnometry measurements have been compared in three instances for two rocks with values calculated from a normative mineral composition. The comparison appears good, however, where differences occur, the direct experimental technique appears to provide the better value and to be capable of indicating density variations within a single rock sample.

Cadenhead, D. A.↗
NASA NTRS1988

Iridium abundance measurements across bio-event horizons in the geological record

Geochemical studies have been performed on thousands of rock samples collected across bio-event horizons in the fossil record using INAA for about 40 common and trace elements and radiochemical isolation procedures for Os, Ir, Pt, and Au on selected samples. These studies were begun soon after the Alvarez team announced their discovery of the Cretaceous-Tertiary (K-T) Ir anomaly in marine rock sequences in Europe. With their encouragement the Authors searched for the anomaly in nearby continental (freshwater coal swamp) deposits. In collaboration with scientists from the U.S.G.S. in Denver, the anomaly was located and it was observed that a floral crisis occurred at the same stratigraphic position as the Ir spike. Further work in the Raton Basin has turned up numerous well-preserved K-T boundary sections. Although the Authors have continued to study the K-T boundary and provide geochemical measurements for other groups trying to precisely locate it, the primary effort was turned to examining the other bio-events in the Phanerozoic, especially to those that are older than the terminal Cretaceous. A list of horizons that were examined in collaboration with paleontologists and geologists is given. Results are also given and discussed.

Orth, C. J.↗
NASA NTRS2005

Extracting Olivine (Fo-Fa) Compositions from Raman Spectral Peak Positions

Olivine and pyroxene are two major basaltic minerals that have been identified at Gusev Crater and Meridiani Planum by the Mars Exploration Rovers. Full petrologic characterization of a sample (rock or soil), however, requires determining the range of mineral compositions, extent of zoning, range of grain sizes, mineral associations, presence of xenocrysts, etc. Information of this sort will aid the interpretation of sample crystallization and differentiation histories and help discriminate between lithologies. In Raman spectroscopic experiments, minerals are identified by their spectral patterns and mineral compositions can be inferred from the peak positions. Instruments currently in use or slated for impending surface exploration missions provide only average elemental compositions for relatively large rock or soil targets or bulk mineral analysis. No techniques currently in use or scheduled for flight can characterize both structure and composition of individual mineral grains, in-situ, like the Mars Microbeam Raman Spectrometer (MMRS). The MMRS is designed to take 100 spectra along a 1 cm linear traverse on the surface of a sample, with contributions from one or a few mineral phases per spectrum. We presented a method to extract structural and compositional information from the Raman spectra of quadrilateral pyroxenes. The pyroxene calibration was applied to a Raman spectroscopic study of Martian meteorite EETA79001 along with a preliminary olivine calibration, where we demonstrated the capability to discriminate related lithologies using Raman point counts. This paper presents an improved olivine calibration that will further aid sample characterization and the study of alteration processes.

Kuebler, K.↗
NASA NTRS2012

Precision Subsampling System for Mars Surface Missions

The ability to analyze heterogeneous rock samples at fine spatial scales would represent a powerful addition to our planetary in situ analytical toolbox. This is particularly true for Mars, where the signatures of past environments and, potentially, habitability are preserved in chemical and morphological variations across sedimentary layers and among mineral pr.ases in a given rock specimen. On Earth, microbial life often associates with surfaces at the interface of chemical nutrients, and ultimately retains sub-millimeter to millimeter-scale layer confinement in fossilization. On Mars, and possibly other bodies, trace chemical markers (elemental, organic/molecular, isotopic, chiral, etc.) and fine-scale morphological markers (e.g., micro-fossils) may he too subtle, degraded, or ambiguous to be detected, using miniaturized instrumentation, without some concentration or isolation. This is because (i) instrument sensitivity may not be high enough to detect trace markers in bulk averages; and (ii) instrument s~lectiviry may not be sufficient to distinguish such markers from interfering/counteracting signals from the bulk. Moreover from a fundamental chemostratigraphic perspective there would be a great benefit to assessing specific chemical and stable isotopic gradients, over millimeter-to-centimeter scales and beyond, with higher precision than currently possible in situ. We have developed a precision subsampling system (PSS) that addresses this need while remaining relatively flexible to a variety of instruments that may take advantage of the capability on future missions. The PSS is relevant to a number of possible lander/rover missions, especially Mars Sample Return. Our specific PSS prototype is undergoing testing under Mars ambient conditions, on a variety of natural analog rocks and rock drill cores, using a set of complementary flight-compatible measurement techniques. The system is available for testing with other contact instruments that may benefit from precision sampling.

Mahaffy, P. R.↗
NASA NTRS1979

A summary of the petrology and geochemistry of pristine highlands rocks

The petrology and geochemistry of pristine lunar highlands rock samples consisting of ferroan anorthosites, norites, troctolites, spinel troctolites/dunite/lherzolite, and KREEP, are described. In addition, petrographic and chemical evidence is presented which shows that low-siderophile rocks are the result of endogenous igneous activity and not impact melt differentiation. For example, these rocks contain Fe-metal as a late-crystallizing phase, and have W/La ratios higher than polymict breccias.

Norman, M. D.↗
DOE OSTI2025

Permeability Prediction Using Vision Transformers

Accurate permeability predictions remain pivotal for understanding fluid flow in porous media, influencing crucial operations across petroleum engineering, hydrogeology, and related fields. Traditional approaches, while robust, often grapple with the inherent heterogeneity of reservoir rocks. With the advent of deep learning, convolutional neural networks (CNNs) have emerged as potent tools in image-based permeability estimation, capitalizing on micro-CT scans and digital rock imagery. This paper introduces a novel paradigm, employing vision transformers (ViTs)—a recent advancement in computer vision—for this crucial task. ViTs, which segment images into fixed-sized patches and process them through transformer architectures, present a promising alternative to CNNs. We present a methodology for implementing ViTs for permeability prediction, its results on diverse rock samples, and a comparison against conventional CNNs. The prediction results suggest that, with adequate training data, ViTs can match or surpass the predictive accuracy of CNNs, especially in rocks exhibiting significant heterogeneity. This study underscores the potential of ViTs as an innovative tool in permeability prediction, paving the way for further research and integration into mainstream reservoir characterization workflows.

58 GEOSCIENCES↗
NASA NTRS2014

Decarboxylation of Carbon Compounds as a Potential Source for CO2 and CO Observed by SAM at Yellowknife Bay, Gale Crater, Mars

Martian carbon was detected in the Sheepbed mudtsone at Yellowknife Bay, Gale Crater, Mars by the Sample Analysis at Mars (SAM) instrument onboard Curiosity, the rover of the Mars Science Laboratory missio]. The carbon was detected as CO2 thermally evolved from drilled and sieved rock powder that was delivered to SAM as a <150-micron-particle- size fraction. Most of the CO2 observed in the Cumberland (CB) drill hole evolved between 150deg and 350deg C. In the John Klein (JK) drill hole, the CO2 evolved up to 500deg C. Hypotheses for the source of the the CO2 include the breakdown of carbonate minerals reacting with HCl released from oxychlorine compounds, combustion of organic matter by O2 thermally evolved from the same oxychlorine minerals, and the decarboxylation of organic molecules indigenous to the martian rock sample. Here we explore the potential for the decarboxylation hypothesis.

Eigenbrode, J. L.↗
NASA NTRS2014

Planning Considerations Related to Collecting and Analyzing Samples of the Martian Soils

The Mars Sample Return (MSR) End-to-End International Science Analysis Group (E2E-iSAG [1]) established scientific objectives associ-ated with Mars returned-sample science that require the return and investigation of one or more soil samples. Soil is defined here as loose, unconsolidated materials with no implication for the presence or absence of or-ganic components. The proposed Mars 2020 (M-2020) rover is likely to collect and cache soil in addition to rock samples [2], which could be followed by future sample retrieval and return missions. Here we discuss key scientific consid-erations for sampling and caching soil samples on the proposed M-2020 rover, as well as the state in which samples would need to be preserved when received by analysts on Earth. We are seeking feedback on these draft plans as input to mission requirement formulation. A related planning exercise on rocks is reported in an accompanying abstract [3].

Liu, Yang↗
NASA NTRS1972

Geologic setting and petrology of Apollo 15 anorthosite /15415/.

The geological setting, petrography and history of this Apollo 15 lunar rock sample are discussed, characterizing the sample as coarse-grained anorthosite composed largely of calcic plagioclase with small amounts of three pyroxene phases. The presence of shattered and granulated minerals in the texture of the rock is traced to two or more fragmentation events, and the presence of irregular bands of coarsely recrystallized plagioclase and minor pyroxene crossing larger plagioclase grains is traced to an earlier thermal metamorphic event. It is pointed out that any of these events may have affected apparent radiometric ages of elements in this rock. A comparative summarization of data suggests that this rock is the least-deformed member of a suite of similar rocks ejected from beneath the regolith at Spur crater.

Wilshire, H. G.↗
NASA NTRS1989

Sm-Nd age of the Fiskenaesset Anorthosite Complex, West Greenland

A Sm-Nd isotopic study on samples from the Fiskenaesset Anorthosite Complex in West Greenland was conducted to estimate the age of crystallization of the complex. A five-point isochron, including data for whole-rock samples of anorthosite, metagabbro, metaperidotite, and separates of calcic plagioclase and mafic matrix from a coarse megacrystic leucogabbro, corresponds to an age of 2.86 + or - 0.05 Ga, with initial sigma(Nd) of +2.9 + or - 0.4. This implies a relatively short time interval, on the order of 70 Ma, during which anorthosite formation, tonalite emplacement, and high-grade metamorphism took place.

Ashwal, Lewis D.↗