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NASA NTRS1985

Surface hardening of steel by boriding in a cold rf plasma

Scanning electron spectroscopy, X-ray diffractometry, Auger electron spectroscopy, and microhardness measurements, are used to study the surfaces of 4340-steel samples that have been borided in a cold RF plasma which had been initiated in a gas mixture of 2.7 percent diborane in Ar. As a result of the dislocation of the diborane in the plasma, boron is deposited on the surface of the steel substrate and two crystalline phases, tetragonal Fe2B and orthorhombic FeB, are formed. The formation of boride phases then increases the surface microhardness from 2650 MPa to a maximum value of 7740 MPa.

Finberg, I.↗

NASA NTRS1986

Surface fatigue and failure characteristics of hot forged powder metal AISI 4620, AISI 4640, and machined AISI 4340 steel spur gears

Spur gear surface fatigue endurance tests were conducted to investigate hot forged powder metal AISI 4620 and 4640 steel for use as a gear material, to determine endurance characteristics and to compare the results with machined AISI 4340 and 9310 steel gear materials. The as-forged and unground SISI 4620 gear exhibited a 10 percent fatigue life that was approximately one-fourth of that for AISI 9310 and less than one-half that for the AISI 4340 gears. The forged and finish ground AISI 4620 gears exhibited a 10 percent life, approximately 70 percent that of AISI 9310 and slightly better than that of AISI 4340. The AISI 4640 hot forged gears had less fracture toughness and slightly less fatigue life than the AISI 4620 test gears.

Townsend, D. P.↗

NASA NTRS1985

Rolling contact fatigue behavior of Cu and TiN coatings on bearing steel substrates

The resistance of copper and TiN coatings on various bearing substrates to high-load rolling contact fatigue (RCF) is investigated. Special attention is given to the lubricating characteristics of copper deposited by ion plating, and the wear resistant characteristics of TiN deposited by ion plating and magnetron sputtering techniques. RCF samples of 440C and AMS 5749 bearing steels were coated. Sputter deposited and ion plated films were on the RCF samples in a range of thickness from about 2000 A to 2 microns. Results showed a marked improvement of the RCF for pure copper tested on 440C, but a degradation for copper on AMS 5749. It is also found that the 2000 A TiN films behave favorably on the 440C and AMS 5749 bearing steels at RCF stress levels of 786 ksi. Scanning electron microscopy, X-ray diffraction, and electron spectroscopy for chemical analysis were used during the investigation.

Hochman, R. F.↗

NASA NTRS1986

Analysis of plasma-nitrided steels

The analysis of plasma nitrided steels can be divided to two main categories - structural and chemical. Structural analysis can provide information not only on the hardening mechanisms but also on the fundamental processes involved. Chemical analysis can be used to study the kinetics for the nitriding process and its mechanisms. In this paper preliminary results obtained by several techniques of both categories are presented and the applicability of those techniques to the analysis of plasma-nitrided steels is discussed.

Salik, J.↗

NASA NTRS1985

An experimental study of biaxial yield in modified 9Cr-1Mo steel at room temperature

Described are two biaxial experiments which investigated yield, hardening, and flow behavior in modified 9Cr-1Mo steel at room temperature. The aim of these experiments was to determine whether the procedures recommended in NE Standard F9-5T for inelastic design analysis are applicable for this material in normalized and tempered condition. The first experiment investigated small offset yield behavior subsequent to radial preloads (sq rt of 3 sub sigma 12 = sub sigma 11) in tension-torsion stress space. The second experiment investigated yield behavior subsequent to nonradial preloads and also the time-dependent flow occurring during 0.5 hour periods at constant stress. The results of these experiments were qualitatively similar to those obtained earlier for types 304 and 316 stainless steel. Specifically, the von Mises yield criterion was found to provide a reasonable approximation of initial yield behavior. Although the subsequent yield surfaces suffered considerable distortion from their near-circular form after both radial and nonradial preloads, the hardening behavior was to the first order kinematic in nature. The strain-time data obtained during the 0.5 hr hold periods showed characteristics typical of creep curves. As in the case of earlier experiments, the high initial flow rates diminished more rapidly than would be estimated from elevated temperature data.

Ellis, J. R.↗

NASA NTRS1987

Surface fatigue and failure characteristics of hot-forged powder metal AISI 4620, AISI 4640, and machined AISI 4340 steel spur gears

Spur gear surface fatigue endurance tests were conducted to investigate hot forged powder metal AISI 4620 and 4640 steel for use as a gear material, to determine endurance characteristics and to compare the results with machined AISI 4340 and 9310 steel gear materials. The as-forged and unground AISI 4620 gear exhibited a 10 percent fatigue life that was approximately one-fourth of that for AISI 9310 and less than one-half that for the AISI 4340 gears. The forged and finish ground AISI 4620 gears exhibited a 10 percent life, approximately 70 percent that of AISI 9310 and slightly better than that of AISI 4340. The AISI 4640 hot forged gears had less fracture toughness and slightly less fatigue life than the AISI 4620 test gears.

Townsend, Dennis P.↗

NASA NTRS1987

Analysis of plasma nitrided steels

Salik, J.↗

NASA NTRS1988

An electrochemical study of corrosion protection by primer-topcoat systems on 4130 steel with ac impedance and dc methods

To investigate metal surface corrosion and the breakdown of metal protective coatings, the ac impedance method is applied to six systems of primer coated and primer topcoated 4130 steel. Two primers were used: a zinc-rich epoxy primer and a red lead oxide epoxy primer. The epoxy-polyamine topcoat was used in four of the systems. The EG and G-PARC Model 368 ac impedance measurement system, along with dc measurements with the same system using the polarization resistance method, were used to monitor changing properties of coated 4230 steel disks immersed in 3.5 percent NaCl solutions buffered at pH 5.4 over periods of 40 to 60 days. The corrosion system can be represented by an electronic analog called an equivalent circuit consisting of resistors and capacitors in specific arrangements. This equivalent circuit parallels the impedance behavior of the corrosion system during a frequency scan. Values for the resistors and capacitors, that can be assigned in the equivalent circuit following a least-squares analysis of the data, describe changes that occur on the corroding metal surface and in the protective coatings. Two equivalent circuits have been determined that predict the correct Bode phase and magnitude of the experimental sample at different immersion times. The dc corrosion current density data are related to equivalent circuit element parameters. Methods for determining corrosion rate with ac impedance parameters are verified by the dc method.

Mendrek, M. J.↗

NASA NTRS1989

Reaction of perfluoroalkylpolyethers (PFPE) with 440C steel in vacuum under sliding conditions at room temperature

Reactions of perfluoroalkylpolyethers (PFPE: Fomblin, Demnum and Krytox) were studied during the sliding contact of stainless steel specimens under ultrahigh vacuum conditions. All three fluids reacted with the steel specimens during sliding. Fomblin, which has acetal linkages, decomposed under the sliding conditions generating gaseous products, (COF2 and fluorinated carbons) which were detected by a quadrupole mass spectrometer. Gaseous products were not detected for the Demnum and Krytox fluids. The amount of gaseous products from Fomblin increased with increasing sliding speed. At the end of the sliding experiments, the wear scar and deposits on the specimens were examined by small spot size XPS. The oxide layer on the specimen surface was removed during sliding, and metal fluorides were formed on the worn surface. The surface of the wear scar and deposits were covered with adsorbed PFPE. Based on these results, it was concluded that the decomposition reaction on Fomblin was initiated by contacting the fluid with a fresh metal surface which was formed during sliding.

Mori, Shigeyuki↗

NASA NTRS1988

The growth of small cracks in 4340 steel

A semiempirical crack-growth model incorporating crack-closure effects has been used to predict crack growth rates and total fatigue life in notched specimens of 4340 steel having an initial defect typical of those previously noted in this steel upon subjection to both constant-amplitude and spectrum loadings. Model predictions for fatigue life are found to be in reasonable agreement with experiments and, in particular, the model was able to accurately predict total fatigue life for specimens subjected to the 'Felix/28' spectrum loading sequence on the sole basis of constant-amplitude test test results.

Swain, M. H.↗

NASA NTRS1988

Ignition of steel alloys by impact of low-velocity iron/inert particles in gaseous oxygen

The ignition of carbon steel and 316 and 304 stainless steels caused by the impact of low-velocity particles (a standard mixture consisting of 2 g of iron and 3 g of inert materials) in gaseous oxygen was investigated using NASA/White Sands Test Facility for the ignition test, and a subsonic particle impact chamber to accelerate the particles that were injected into flowing oxygen upstream of the target specimen. It was found that the oxygen velocities required to ignite the three alloys were the same as that required to ignite the particle mixture. Ignition occurred at oxygen velocities greater than 45 m/sec at 20 to 24 MPa and was found to be independent of pressure between 2 and 30 MPa. Comparison of the present results and the past results from Wegener (1964) with the Compressed Gas Association (CGA) oxygen velocity limits for safe operations indicates that the CGA limits may be excessively conservative at high pressures and too liberal at low pressures.

Benz, Frank J.↗

NASA NTRS1988

Wear of liquid nitrogen-cooled 440C bearing steels in an oxygen environment

This paper presents up-to-date findings of the research being conducted to understand the mechanism of sliding wear in unlubricated 440C bearing steels under oxidative conditions. A sliding wear test rig has been designed and built with a cylinder-on-flat geometry. The equipment is capable of testing specimens under high axial loads and sliding speeds in a simulated LOX environment. Samples of 440C steel, quenched and tempered to a hardness of Rc 56, were tested under a load of 890 N and a sliding speed of 2.05 m/sec for total sliding distances of up to 5.54 km. Flash temperatures during these tests were measured with an IR camera and a fast digital recorder. Microstructural and microanalytical data from the worn surfaces and the debris particles are analyzed extensively, along with wear rates, flash temperatures, surface profiles, hardnesses, and residual stresses, in the context of oxidation and wear theories.

Chaudhuri, Dilip K.↗

NASA NTRS1989

Rapid rotational/translational maneuvering experiments of a flexible steel beam

Future space manipulators may need translational base motion to expand the access region of a manipulator. An experiment was conducted to demonstrate slewing of flexible structures with coupled rotational and translational axes while simultaneously suppressing vibrational motion during the maneuver. In the experiment, a flexible steel beam carried by a translational cart was maneuvered by an active controller to perform position-control tasks. Experimental results are presented to show how the flexibility of the steel beam influences the multi-input multi-output feedback controller.

Juang, Jer-Nan↗

NASA NTRS1988

Surface metallurgical and tribological characteristics of TiN-coated bearing steels

The rolling contact fatigue (RCF) characteristics of an aerospace bearing steel 440C coated with TiN films of various thicknesses are studied. The wear and corrosion properties of the film-substrate system are examined as well as how these properties correlate with the RCF behavior. It is found that TiN coatings with thicknesses below 1 micron resulted in significant improvements in the RCF lives of base steel substrates under both mild and heavy loading conditions.

Erdemir, A.↗

NASA NTRS1990

Nondestructive Technique To Assess Embrittlement In Steels

Recent research at NASA Langley Research Center led to identification of nondestructive technique for detection of temper embrittlement in HY80 steel. Measures magnetoacoustic emission associated with reversible motion of domain walls at low magnetic fields. Of interest to engineers responsible for reliability and safety of various dynamically loaded and/or thermally cycled steel parts. Applications include testing of landing gears, naval vessels, and parts subjected to heat, such as those found in steam-pipe fittings, boilers, turbine rotors, and nuclear pressure vessels.

Allison, Sidney G.↗

NASA NTRS1992

Casting Stainless-Steel Models Around Pressure Tubes

Survivability of thin-wall stainless-steel tubing increased to nearly 100 percent. Improves state of art in pressure-model castings and reduces cost associated with machining complete model from stainless-steel blank.

Vasquez, Peter↗

NASA NTRS1992

Electrochemical Impedance Of Inorganic-Zinc-Coated Steel

Report describes preliminary experiments to evaluate both direct-current and alternating-current electrochemical impedance measurements as candidate techniques for use in accelerated corrosion testing of mild-steel panels coated with inorganic zinc-rich primers and exposed to seaside air. Basic idea behind experiments to compare electrochemical impedance measurements with anticorrosion performances of coating materials to determine whether measurements can be used to predict performances. Part of continuing program to identify anticorrosion coating materials protecting steel panels adequately for as long as 5 years and beyond.

Macdowell, Louis G.↗

NASA NTRS1990

Application of magnetoacoustic emission technique to temper embrittlement characterization of HY-80 steel

Magnetoacoustic phenomena associated with the use of the magnetoacoustic emission technique for the temper embrittlement characterization of HY-80 steel are investigated in an attempt to explain some peculiarities observed in highly embrittled HY-80 samples. In particular, attention is given to the effects of the ac magnetic field frequency and shape. The peak amplitude of the magnetoacoustic burst, which is directly related to the width of the pulse height distribution, is shown to be a critical parameter in the determination of the degree of temper embrittlement in the steel.

Denale, R.↗