Search NASA⌕ Search

SEARCH · Search NASA

Results for “Ultrasonication”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 181 records · Page 10

Correlations between ultrasonic and fracture toughness factors in metallic materials

A heuristic mathematical basis is proposed for the experimental correlations found between ultrasonic propagation factors and fracture toughness factors in metallic materials. A crack extension model is proposed wherein spontaneous stress (elastic) waves produced during microcracking are instrumental in promoting the onset of unstable crack extension. Material microstructural factors involved in this process are measurable by ultrasonic probing. Experimental results indicate that ultrasonic attenuation and velocity measurements will produce significant correlations with fracture toughness properties and also yield strength.

Vary, A.↗

Broadband electrostatic acoustic transducer for ultrasonic measurements in liquids

A broadband capacitive electrostatic acoustic transducer (ESAT) has been developed for use in a liquid environment at megahertz frequencies. The ESAT basically consists of a thin conductive membrane stretched over a metallic housing. The membrane functions as the ground plate of a parallel plate capacitor, the other plate being a dc biased electrode recessed approximately 10 microns from the electrically grounded membrane. An ultrasonic wave incident on the membrane varies the membrane-electrode gap spacing and generates an electrical signal proportional to the wave amplitude. The entire assembly is sealed for immersion in a liquid environment. Calibration of the ESAT with incident ultrasonic waves of constant displacement amplitude from 1 to 15 MHz reveals a decrease in signal response with increasing frequency independent of membrane tension. The use of the ESAT as a broadband ultrasonic transducer in liquids with a predictable frequency response is promising.

Cantrell, J. H., Jr.↗

Effect of ultrasonic irradiation on mammalian cells and chromosomes in vitro

Human peripheral blood and HeLa cells were irradiated in vitro at the ultrasonic frequency of 65 kHz. The whole blood and HeLa cell suspensions were exposed to continuous and pulsed ultrasonic power levels of 0.12, 0.16, 0.72, 1.12 and 2.24 W for a period of one minute. The method of ultrasonic irradiation was carried out with the whole blood or HeLa cell suspensions coupled directly to a cylindrical transducer while heating of the cell suspensions in excess of 41 C was avoided. Irradiated and unirradiated peripheral blood lymphocyte chromosome cultures were prepared and scored for selected numerical and morphological aberrations. There was no significant difference in the frequency of chromosomal aberrations between irradiated and unirradiated cells.

Roseboro, J. A.↗

Fresnel lenses for ultrasonic inspection

Ultrasonic Fresnel lenses are effective focusing elements with potential applications in ultrasonic "contact" testing for defects in materials. Ultrasonic beams focused on concave lenses are used successfully with immersion transducers, for which test object is immersed in water bath. However, for large objects, objects that are already installed, objects on production lines, and objects that can be damaged by water, contact testing is more practical than immersion.

Kammerer, C. C.↗

Simulation of transducer-couplant effects on broadband ultrasonic signals

The increasing use of broadband, pulse-echo ultrasonics in nondestructive evaluation of flaws and material properties has generated a need for improved understanding of the way signals are modified by coupled and bonded thin-layer interfaces associated with transducers. This understanding is most important when using frequency spectrum analyses for characterizing material properties. In this type of application, signals emanating from material specimens can be strongly influenced by couplant and bond-layers in the acoustic path. Computer synthesized waveforms were used to simulate a range of interface conditions encountered in ultrasonic transducer systems operating in the 20 to 80 MHz regime. The adverse effects of thin-layer multiple reflections associated with various acoustic impedance conditions are demonstrated. The information presented is relevant to ultrasonic transducer design, specimen preparation, and couplant selection.

Vary, A.↗

Quantitative ultrasonic evaluation of engineering properties in metals, composites and ceramics

Ultrasonic technology from the perspective of nondestructive evaluation approaches to material strength prediction and property verification is reviewed. Emergent advanced technology involving quantitative ultrasonic techniques for materials characterization is described. Ultrasonic methods are particularly useful in this area because they involve mechanical elastic waves that are strongly modulated by the same morphological factors that govern mechanical strength and dynamic failure processes. It is emphasized that the technology is in its infancy and that much effort is still required before all the available techniques can be transferred from laboratory to industrial environments.

Vary, A.↗

A model for correlating damage and ultrasonic attenuation in composites

Ultrasonic attenuation data measured by the pulse-echo technique have been obtained versus load for two graphite-epoxy laminates and are presented. The attenuation-load data display distinct changes at load values associated with the initiation of transverse cracks in the weakest plies and with the knee in the bilinear stress-strain curve. It was intended to determine if a simplified diffraction model could be used to account for the attenuation changes. The basis of the diffraction model is that transverse cracks or delaminations, or both, initiating and progressing in the specimen under the area covered by the ultrasonic transducer would cause diffraction of the ultrasonic beam and changes in the measured attenuation.

Hayford, D. T.↗

Simulation of transducer-couplant effects on broadband ultrasonic signals

The increasing use of broadband, pulse-echo ultrasonics in nondestructive evaluation of flaws and material properties has generated a need for improved understanding of the way signals are modified by coupled and bonded thin-layer interfaces associated with transducers. This understanding is most important when using frequency spectrum analyses for characterizing material properties. In this type of application, signals emanating from material specimens can be strongly influenced by couplant and bond-layers in the acoustic path. Computer synthesized waveforms were used to simulate a range of interface conditions encountered in ultrasonic transducer systems operating in the 20to 80-MHz regime. The adverse effects of thin-layer multiple reflections associated with various acoustic impedance conditions are demonstrated. The information presented is relevant to ultrasonic transducer design, specimen preparation, and couplant selection.

Vary, A.↗

Concepts and techniques for ultrasonic evaluation of material mechanical properties

The ultrasonic nondestructive evaluation techniques discussed in the present paper indicate potentials for material characterization and property prediction. Stress wave interaction and material transfer function concepts are examined as a basis for explaining correlations between material mechanical behavior and ultrasonically measured quantities. It is observed that the effect and criticality of any discrete flaw, such as crack, inclusion, or any other stress raiser, is definable only in terms of its material microstructural environment. This underscores the importance of ultrasonic techniques capable of characterizing the stress wave energy transfer properties of a material.

Vary, A.↗

On the feasibility of quantitative ultrasonic determination of fracture toughness: A literature review

The three main topics covered are: (1) fracture toughness and microstructure, (2) quantitative ultrasonic and microstructure; and (3) scattering and related mathematical methods. Literature in these areas is reviewed to give insight to the search of a theoretical foundation for quantitative ultrasonic measurement of fracture toughness. The literature review shows that fracture toughness is inherently related to the microstructure and in particular, it depends upon the spacing of inclusions or second particles and the aspect ratio of second phase particles. There are indications that ultrasonic velocity attenuation measurements can be used to determine fracture toughness. The leads to a review of the mathematical models available in solving boundary value problems related to microstructural factors that govern facture toughness and wave motion. A framework towards the theoretical study for the quantitative determination of fracture toughness is described and suggestions for future research are proposed.

Fu, L. S.↗

Quantitative broadband ultrasonic backscatter - An approach to nondestructive evaluation in acoustically inhomogeneous materials

The use of a broadband backscatter technique to obtain the frequency dependence of the longitudinal-wave ultrasonic backscatter coefficient from a collection of scatterers in a solid is investigated. Measurements of the backscatter coefficient were obtained over the range of ultrasonic wave vector magnitude-glass sphere radius product between 0.1 and 3.0 from model systems consisting of dilute suspensions of randomly distributed crown glass spheres in hardened polyester resin. The results of these measurements were in good agreement with theoretical prediction. Consequently, broadband measurements of the ultrasonic backscatter coefficient may represent a useful approach toward characterizing the physical properties of scatterers in intrinsically inhomogeneous materials such as composites, metals, and ceramics, and may represent an approach toward nondestructive evaluation of these materials.

Odonnell, M.↗

Ultrasonic and mechanical characterizations of fatigue states of graphite epoxy composite laminates

Eight-ply (0, + or - 45, 0)s laminates of Hercules AS/3501-6 graphite epoxy composite are fabricated using various cure pressures ranging from 0.52 to 0.86 MPa and cure temperatures ranging from 150 C to 200 C. In general, the minimum composite void volume fraction is obtained at a cure temperature of 175 C and a cure pressure of 0.86 MPa, or at 200 C and 0.86 MPa. The ultrasonic attenuation at 4 MHz was found to correlate with the composite void volume fraction. Composite specimens were tested in flexural fatigue. Beyond 10,000 fatigue cycles, the ultrasonic attenuation at 4 MHz was found to increase and the flexural stiffness was found to decrease. The ultrasonic attenuation at 4 MHz of the as-fabricated composite can be correlated with the number of fatigue cycles to failure.

Williams, J. H., Jr.↗

Ultrasonic and mechanical characterizations of fatigue states of graphite epoxy composite laminates

Results of an exploration of the relationship between ultrasonic attenuation and fatigue survivability of graphite fiber epoxy composites fabricated under different cure conditions are reported. A total of 9 27 x 40 cm eight-ply graphite epoxy laminated specimens were formed, and fatigue tests were run on five partial samples at 73.5 N varying at 30 Hz, with tests ending at a 1.27 cm deflection. A pulsed oscillator generated sinusoidal waves and transducers recorded the passage of the ultrasonic waves for display on oscilloscopes. Cure pressures ranged from 0.52-0.85 MPa and cure temperatures were in the 150-200 C interval. Ultrasonic through-transmission at 4 MHz was performed prior to and during fatigue testing. The minimum void volume fraction occurred at 175 C and 0.86 MPa. The flexural stiffness decreased with the number of fatigue cycles past 10,000, when the attenuation also increased. Correlations were found between the 4.0 MHz signal attenuation and the void volume fraction, and between the number of fatigue cycles to failure and the 4.0 MHz signal attenuation.

Williams, J. H., Jr.↗

Ultrasonic Bonding of Solar-Cell Leads

Rolling ultrasonic spot-bonding method successfully joins aluminum interconnect fingers to silicon solar cells with copper metalization. Technique combines best features of ultrasonic rotary seam welding and ultrasonic spot bonding: allows fast bond cycles and high indexing speeds without use of solder or flux. Achieves reliable bonds at production rates without damage to solar cells. Bonding system of interest for all solar-cell assemblies and other assemblies using flat leads (rather than round wires).

Frasch, W.↗

Acousto-ultrasonic characterization of fiber reinforced composites

The advantageous aspects of acoustic emission and ultrasonic methodologies are combined in a technique which operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is quite complex, but it can be quantitized in terms of a "stress wave factor". The stress wave factor, which can be defined in a number of ways, is essentially a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect will appear in the stress wave factor.

Vary, A.↗

Ultrasonic attenuation of a void-containing medium for very long wavelengths

Ultrasonic longitudinal through-thickness attenuation in an isotropic medium due to scattering by randomly distributed voids is considered analytically. The attenuation is evaluated on the assumption of no interaction between voids. The scattered power is assumed to be entirely lost, thus accounting for the ultrasonic attenuation. The scattered power due to the presence of a void is described in terms of the scattering cross section of the void. An exact solution exists for the scattering cross section of a spherical void. An approximate solution for the scattering cross section of an ellipsoidal void is developed based on the so-called Born approximation commonly used in quantum mechanics. This approximate solution is valid for k sub p a sub i 1, where k sub p is the wave number of the incident longitudinal wave and a sub i is the largest dimension of the void. It is found that the shape of the void has negligible effect on the scattering cross section and that only the volume of the void is important. Thus, it is noted that in cases where k sup p a sub i 1, the exact scattering cross section of a spherical void having the same volume as an arbitrarily shaped void can be used for evaluating ultrasonic attenuation.

Williams, J. H., Jr.↗

Ultrasonic attenuation of a void-containing medium for very long wavelengths

Ultrasonic longitudinal through-thickness attenuation in an isotropic medium due to scattering by randomly distributed voids is considered analytically. The attenuation is evaluated on the assumption of no interaction between voids. The scattered power is assumed to be entirely lost, thus accounting for the ultrasonic attenuation. The scattered power due to the presence of a void is described in terms of the scattering cross section of the void. An exact solution exists for the scattering cross section of a spherical void. An approximate solution for the scattering cross section of an ellipsoidal void is developed based on the so-called Born approximation commonly used in quantum mechanics. This approximate solution is valid for k sub p a sub i much less than 1, where k sub p is the wave number of the incident longitudinal wave and a sub i is the largest dimension of the void. It is found that the shape of the void has negligible effect on the scattering cross section and that only the volume of the void is important. Thus, it is noted that in cases where k sub p a sub i is much less than 1, the exact scattering cross section of a spherical void having the same volume as an arbitrarily shaped void can be used for evaluating ultrasonic attenuation. Previously announced in STAR as N83-28466

Williams, J. H., Jr.↗

Ultrasonic inspection of carbon fiber reinforced plastic by means of sample-recognition methods

In the case of carbon fiber reinforced plastic (CFRP), it has not yet been possible to detect nonlocal defects and material degradation related to aging with the aid of nondestructive inspection method. An approach for overcoming difficulties regarding such an inspection involves an extension of the ultrasonic inspection procedure on the basis of a use of signal processing and sample recognition methods. The basic concept involved in this approach is related to the realization that the ultrasonic signal contains information regarding the medium which is not utilized in conventional ultrasonic inspection. However, the analytical study of the phyiscal processes involved is very complex. For this reason, an empirical approach is employed to make use of the information which has not been utilized before. This approach uses reference signals which can be obtained with material specimens of different quality. The implementation of these concepts for the supersonic inspection of CFRP laminates is discussed.

Bilgram, R.↗