The further development of scanning electron microscopy in the microelectronics field semiannual report, 1 jan. - 30 jun. 1968
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The vestibular end organs, after chemical fixation, were freeze dried, coated with gold and palladium, and studied in the scanning microscope. Scanning microscopy gives a good three dimensional view of the sensory areas and allows study of both gross anatomy and microstructures. Cross anatomical features of the structure of the ampullae are demonstrated. The form of the statoconia in different species of animals is shown. New aspects of the structure of the sensory hairs are revealed. The hair bundles in the central areas of the cristae and in the striola of the maculae differ structurally from the hair bundles at the periphery of the sensory regions. Furthermore, some hair bundles consisting of very short stereocilia were observed. The relationship between the cupula and the statoconial membrane to the epithelial surface is discussed.
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The paper discusses several discoveries made in the study of lunar material. In the examination of the effects of solar wind implantations the topics covered include (1) solar wind radiation damage parameters and their aging characteristics, (2) the theory of the ancient solar wind, (3) the solar wind sputtering erosion rate, (4) the physicochemical properties of amorphous coatings, (5) maturity indexes and the macroscopic properties of the lunar regolith, (6) solar wind gas bubbles, (7) the composition of very heavy nuclei in the contemporary solar wind, and (8) track aging processes. Conclusions are drawn from the results about other extraterrestrial features such as the parent bodies of the meteorites, early solar nebulas, and interstellar clouds.
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All films were deposited by resistive heated evaporation in an oil diffusion pumped vacuum system (ultimate approx. equal to 0.0000001 torr). The growth from nuclei to a continuous film is highly dependent on the deposition parameters, evaporation rate as well as substrate material and substrate temperature. The growth stages of a film and the dependence of grain size on various deposition and annealing parameters are shown. Resistivity measurements were taken on thin films to observe size effects.
A conceptual model of a lava fountain consists of a vent, spatter ramparts, fountain column, downwind plume and associated pumice deposits. Glassy particles produced by lava fountain eruptions consist primarily of sideromelane glass and minor to moderate amounts of vesicles and crystals. Particles are classified on the basis of morphology as: (1) spherical, (2) elongate, (3) glass-coated mineral grain, (4) shard, (5) reticulite, (6) composite particle, and (7) lithic fragment.
Gold and copper films (0.2-2 micron thick) are ion plated on very smooth stainless steel 304 and mica surfaces. The deposited films are examined by SEM to identify the morphological growth of defects. Three types of coating defects are distinguished: nodular growth, abnormal or runaway growth, and spits. The potential nucleation sites for defect growth are analyzed to determine the cause of defect formation. It is found that nuclear growth is due to inherent surface microdefects, abnormal or runaway growth is due to external surface inclusions, and spits are due to nonuniform evaporation and ejection of droplets. All these defects have adverse effects on the coatings.
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It was found that the in situ treatment of 001-plane single-crystal films of MgO (prepared by epitaxial growth from the vapor phase) at high temperatures with a jet of oxygen will produce a surface that is almost equivalent, for epitaxial studies, to surfaces with the same orientation prepared by vacuum cleavage of bulk single crystals. The effectiveness of the process is demonstrated by its impact on the epitaxy of silver.
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On the basis of characteristic diffuse ring diffraction patterns, much of the carbonaceous matter in a large suite of Allende acid residues has been identified as a variety of turbostratic carbon. Crystallites of this phase contain randomly stacked sp(2) hybridized carbon layers and diffraction patterns resemble those from carbon black and glassy carbon. Carbynes are probably absent, and are certainly restricted to less than 0.5% of these acid residues. The work of Ott et al. (1981) provides a basis for the possibility that turbostratic carbon is a carrier of noble gases, but an additional component - amorphous carbon - may be necessary to explain the high release temperatures of noble gases as well as the glassy character of many of the carbonaceous particles. Carbynes are considered to be questionable as important carriers of noble gases in the Allende acid residues.
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