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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 181 records · Page 10

Unlocking Metamaterials At The Macro Scale (CRADA Final Report)

This project was part of the Cyclotron Road program, which supports scientific entrepreneurs in their efforts to commercialize novel technologies with potential to address energy, manufacturing and climate related issues. The participants' technology is a lightweight cellular material system which could be applied to a range of products and markets and offer benefits of reduced weight, cost, waste, and carbon footprint. The objective of the project was to investigate potential opportunities and de-risk technical and market barriers in pursuit of successful commercialization. This project’s purpose was to find market pathways and technical roadmaps for commercializing the lightweight cellular material technology. The main problems to overcome are the risks in both tech and market. On the technical side, performance, weight, cost and speed of manufacturing, and other scaleup problems needed to be addressed. On the market side, the challenges included finding product/market fit, developing business models and go to market strategies, and developing commercial relationships within various industries. Our approach typically started with market analysis, in order to identify potential applications where our technology could solve problems and address pain points. To do this, we performed customer discovery, interviewing hundreds of industry stakeholders along all parts of the value chain for a given product or industry. From here, we would develop technoeconomic models which combined aspects of numerical modeling for structural and mechanical performance based on criteria from customers or industry guidelines such as stiffness, strength, weight, and other physical properties. Then, this would be combined with detailed cost models to translate the engineering solution into a manufacturable, scalable product. The challenge here was to have equal or better performance at lower cost and higher speed than existing solutions.

36 MATERIALS SCIENCE↗

Innovative Nuclear Materials Outboard-A Project Specimen Preparation Guide

The Innovative Nuclear Materials (INM) Program was recently established by the U.S. Department of Energy (DOE) to develop advanced material technologies for use in nuclear reactors. The INM program is presently focused on researching in-core non-fueled materials for application in fast spectrum nuclear reactors. The widespread deployment of fast reactors continues to be a prominent aspiration for advanced nuclear technology developers. However, companies working to license these reactors have no choice but to rely on historic material technologies since further optimization and advancement of these materials is impeded by the lack of fast neutron irradiation test facilities. INM-OA is a non-fueled drop-in experiment which will irradiate material specimens of interest to fast reactor applications. This experiment will be irradiated at Idaho National Laboratory (INL) in the Advanced Test Reactor (ATR) outboard-A (OA) position during normal and high temperature steady state (HTSS) cycles. It will include material specimens supplied by members of the INM program and will utilize a cadmium-lined basket to filter out incident thermal neutrons, thus simulating a faster neutron energy spectrum. Material specimens will undergo post-irradiation examination including microscopy and mechanical testing. In addition to absorption reactions, fast neutrons cause microstructural damage in materials by atom displacement, which can cause exacerbated changes in physical properties and behavior. Thus, the data obtained from the INM-OA experiment will be crucial for understanding the engineering-scale behavior of reactor materials. This document is intended for the Principal Investigators providing samples for this project. Topics included are a general description of the experiment, the irradiation experiment/capsule design, sample geometries, number of samples to be provided, documentation to be provided, a brief list potentially useful characterization methods that can be leveraged at INL, and other miscellaneous requirements specific to this project. This document is intended for informational use only.

innovative nuclear materials↗

Nonlinear Constitutive Relations for High Temperature Application, 1984

Nonlinear constitutive relations for high temperature applications were discussed. The state of the art in nonlinear constitutive modeling of high temperature materials was reviewed and the need for future research and development efforts in this area was identified. Considerable research efforts are urgently needed in the development of nonlinear constitutive relations for high temperature applications prompted by recent advances in high temperature materials technology and new demands on material and component performance. Topics discussed include: constitutive modeling, numerical methods, material testing, and structural applications.

Source record↗

Nonlinear Constitutive Relations for High Temperature Applications, 1986

The purpose of the symposium was to review the state-of-the-art in nonlinear constitutive modeling of high temperature materials for aeronautics applications and to identify the need for future research and development efforts in this area. Through this symposium, it was recognized that considerable research efforts are urgently needed in the development of nonlinear constitutive relations for high temperature applications. In the aerospace industry this need is further prompted by recent advances in high temperature materials technology and new demands on material and component performance.

Source record↗

Advanced Materials and Manufacturing Technologies (AMMT) 2025 Roadmap

The mission of the Advanced Materials and Manufacturing Technologies (AMMT) program is to accelerate the development, qualification, demonstration, and deployment of advanced materials and manufacturing technologies in support of the United States (US) leadership in a broad range of nuclear energy applications. The vision of the AMMT program is the expansion of reliable and economical nuclear energy enabled by advanced materials and manufacturing technologies. Four major goals were set to realize the mission and vision of the AMMT program, including: (1) develop advanced materials and manufacturing technologies that have cross-reactor applications, (2) establish and demonstrate a rapid qualification framework that supports diverse materials and manufacturing technology needs, (3) evaluate materials performance in a range of nuclear environments, and (4) accelerate commercialization of new technologies through technology maturation. The program is designed to deliver solutions that support a wide range of reactor technologies.

36 MATERIALS SCIENCE↗

Space Transportation Materials and Structures Technology Workshop: Proceedings - Volume 2

The Space Transportation Materials and Structures Technology Workshop was held on September 23-26, 1991, in Newport News, Virginia. The workshop, sponsored by the NASA Office of Space Flight and the NASA Office of Aeronautics and Space Technology, was held to provide a forum for communication within the space materials and structures technology developer and user communities. Workshop participants were organized into a Vehicle Technology Requirements session and three working panels: Materials and Structures Technologies for Vehicle Systems, Propulsion Systems, and Entry Systems.

Cazier, Frank W., Jr.↗

Determination of contamination character of materials in space technology testing

The contamination characters of selected materials used in space technology testing. Specific materials were subjected to a thermal vacuum environment, and the outgases were collected on a cold test mirror surface. Approximately one-half of the surface of the mirror was subjected to ultraviolet irradiation while the outgases were being deposited on the mirror. The purpose of these experiments was to determine the effect of ultraviolet irradiation on the contaminative character of outgases from selected materials. The degree of contamination was measured in terms of degradation of the optical properties of the test mirror and the amount of deposit per unit area on quartz crystal microbalances placed near the test mirror, and by means of quadrupole mass spectral measurements of outgases from the test samples.

Haynes, D. L.↗

Materials Scorecards, Phase 1: Advanced Materials and Manufacturing Technology

This report presents preliminary material score cards (Phase 1) based on a survey of industry experts and the limited literature available on the state of advanced manufacturing of materials for nuclear applications. Seven reactor types were considered, and the data is presented in tabular form. The caveat is that the scores are based on limited data and expert judgement. Considerable work remains to be done to prioritize materials for advanced manufacturing to support existing and advanced reactors. A central database of processing conditions, resulting microstructure, post processing, properties, and performance of these materials is needed to support the accelerated adoption of advanced manufacturing by the industry.

36 MATERIALS SCIENCE↗

Composite Materials Research and Technology at NASA/MSFC

The utilization of composite materials in the Space Shuttle and Advanced Space Transportation Programs is reviewed. Topics include goals and challenges, descriptions of multi-generational launch vehicles, and an overview of composite materials research and technologies that support program objectives. A brief discussion of planned composite materials research and technology concludes the presentation.

Ledbetter, Frank E., III↗

Office of Aeronautics and Space Technology preliminary requirements for space science and applications platform studies

Needs and requirements for a free flying space science and applications platform to host groupings of compatible, extended mission experiments in earth orbit are discussed. A payload model which serves to define a typical set of mission requirements in the form of a descriptive data base is presented along with experiment leval and group level data summarizations and flight schedules. The payload descriptions are grouped by technology into the following categories: communications, materials (long term effect upon), materials technology development, power, sensors, and thermal control.

Source record↗

Enabling propulsion materials for high-speed civil transport engines

NASA Headquarters and LeRC have advocated an Enabling Propulsion Materials Program (EPM) to begin in FY-92. The High Speed Research Phase 1 program which began in FY-90 has focused on the environmental acceptability of a High Speed Civil Transport (HSCT). Studies by industry, including Boeing, McDonnell Douglas, GE Aircraft Engines, and Pratt & Whitney Aircraft, and in-house studies by NASA concluded that NO(x) emissions and airport noise reduction can only be economically achieved by revolutionary advancements in materials technologies. This is especially true of materials for the propulsion system where the combustor is the key to maintaining low emissions, and the exhaust nozzle is the key to reducing airport noise to an acceptable level. Both of these components will rely on high temperature composite materials that can withstand the conditions imposed by commercial aircraft operations. The proposed EPM program will operate in conjunction with the HSR Phase 1 Program and the planned HSR Phase 2 program slated to start in FY-93. Components and subcomponents developed from advanced materials will be evaluated in the HSR Phase 2 Program.

Stephens, Joseph R.↗

LDRD conclusion poster - Synthesizing Heterometallic Uranium Single Crystals to Understand the Influence of the Secondary Metals on Uranyl Axial Bond Strength

Understanding how transition metals influenced the chemistry of lanthanide and actinide (f-element) materials is critical for advancing separation technologies, materials design, and coordination chemistry. This project examined how incorporating first-row transition metals affected the structural and spectroscopic properties of f-element coordination polymers. In uranium(VI)-based systems synthesized with 2,6-pyridinedicarboxylic acid (PDC) ligands, single-crystal X-ray diffraction and Raman spectroscopy revealed that the presence of transition metals shortened the uranyl axial bond and induced a blue shift in its symmetric stretching vibration—evidence of increased bond strength. Electronic structure analysis, including Density of States (DOS) calculations using density functional theory (DFT), revealed altered orbital overlaps and highlighted the role of transition metal d-orbitals in modulating bonding. Raman modes were modeled using truncated structural fragments in collaboration with the University of Notre Dame, and although the predicted frequencies were lower than experimental values, they remained within expected ranges. In parallel, similar experiments with cerium (Ce) in the presence of cobalt (Co) and PDC demonstrated multi-step single-crystal-to-single-crystal transformations—behavior not observed in the uranium systems. Initial products included light yellow, orange, and polycrystalline materials. Single-crystal X-ray diffraction studies, conducted in collaboration with the Colorado School of Mines, identified the yellow phase as monometallic Ce(PDC)2(H2O)2·4H2O and the orange phase as heterometallic Ce2Co(PDC)4(H2O)6. After standing in solution for one week, both phases fully transformed into a dark yellow crystalline phase, [Ce3(PDC)5(H2O)8].6(H2O). Remarkably, this transformation was reversible—disturbing the equilibrium by removing some crystals caused reversion to the initial Ce(PDC)2(H2O)2·4H2O phase, highlighting dynamic behavior. All three structures were previously unreported. Solid-state UV-visible and Raman spectroscopy further distinguished these phases, revealing ligand-to-metal charge transfer involving Ce and characteristic d–d transitions from Co(II). The precise mechanism driving these transformations remained unclear; however, pH-dependent experiments confirmed that the transformation did not occur when the pH decreased. Overall, the project demonstrated that transition metals could be employed to tune bonding interactions, structural dimensionality, and optical properties in f-element materials, establishing new pathways for designing functional heterometallic systems. The work resulted in several novel structural discoveries and fostered productive collaborations with the University of Notre Dame and the Colorado School of Mines.

37 - INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL C↗

Materials Scorecards, Phase 2: Advanced Materials and Manufacturing Technology

This report presents updated material score cards with detailed justification of the proposed rating provided and quantifies the readiness of the advanced manufacturing of materials for nuclear applications. Based on an expanded literature review of available data, the scores in this report (Phase 2) have either been modified or remained constant as compared with Phase 1 scoring. The rating justification are provided for each scoring criteria whereas the maturity quantification of additively manufactured alloys and the knowledge gaps are discussed with reference traceability. This report focuses on the detailed justification and traceability for the adoption of additively manufactured 316SS, SS304, Alloy 800H, Graphite C/C, Alloy N, Silicon Carbide, HT9, Alloy 617, and Alloy 718. Significant variability in data and knowledge gaps exist among the identified materials. The scorecards are therefore based on published literature data, industry response to a survey, stakeholder input collected at workshops, and expert opinion. The interpretation and assessment were somewhat challenged as experimental process parameters and methodology varied and best judgment was exercised for score quantification. This assessment reflects the overall level of technical maturity for AM materials and their deployment in Gen-VI nuclear systems. These Phase 2 scorecards are likely to be revised based on additional input from stakeholders and as new research results become available.

36 MATERIALS SCIENCE↗

Integrated optics technology study

The status and near term potential of materials and processes available for the fabrication of single mode integrated electro-optical components are discussed. Issues discussed are host material and orientation, waveguide formation, optical loss mechanisms, wavelength selection, polarization effects and control, laser to integrated optics coupling fiber optic waveguides to integrated optics coupling, sources, and detectors. Recommendations of the best materials, technology, and processes for fabrication of integrated optical components for communications and fiber gyro applications are given.

Chen, B.↗

Optical coating technology for the EUV

Advances in optical coating and materials technology are one of the key motivators for the development of missions such as the Far Ultraviolet Spectroscopic Explorer recently selected by NASA for an Explorer class mission in the mid 1990's. The performance of a range of candidate coatings are reviewed for normal-incidence and glancing-incidence applications, and attention is given to strengths and problem areas for their use in space. The importance of recent developments in multilayer films, chemical-vapor deposited SiC (CVD-SiC) mirrors, and SiC films are discussed in the context of EUV instrumentation design. For example, the choice of optical coatings is a design driver for the selection of the average glancing angle for the FUSE telescope, and impacts efficiency, short-wavelength cut-off, and physical size.

Osantowski, J. F.↗

The Scientific Case for Concurrent Neutron and X-ray Scattering and Spectroscopy

The interrogation of materials with X-rays or neutrons to determine the structure, energetics, and dynamics of materials is fundamental to advancing materials' physical and chemical science and developing innovative material technologies. A transcending challenge in developing novel materials is that progress hinges on understanding the structure and dynamics across multiple time and length scales in complex materials that feature multiple components, interfaces, and compositions. Despite the ever-growing demands on materials’ characterization, existing approaches are almost exclusively based on isolated X-ray or neutron scattering, i.e., an approach commensurate with the more narrowly defined needs of fifty years ago. A three-day workshop sponsored by the U.S. National Science Foundation (NSF) analyzed the demand for concurrent neutron and X-ray (NeX) experiments. It was held at the Spring Hill Suites, San Jose, California, from June 2 to 4, 2022. In this workshop, 70 national and international experts ascertained the crucial need to establish NeX capabilities to advance the science of complex materials and systems in the US. Here, we illustrate the need for NeX scattering and spectroscopy experiments by showcasing examples that span areas as diverse as biomaterials, energy science, soft matter, and nanomaterials. To provide NeX capability will require new instrumentation that enables concurrent experiments. Affected areas include chemistry, soft matter, quantum materials, pure and applied chemistry, bioscience, geoscience, and applied materials. NeX benefits research outcomes due to the complementarity of the two techniques, which is essential for better model refinement. While joint refinement of data from separate neutron and X-ray experiments is critical to avoid ambiguities, especially in multiphase-multicomponent materials, concurrent experiments overcome scientific and technical barriers associated with single measurements, separated by location and, thus, time. Among all the examples, these factors introduce uncertainties in the results that complicate data analysis. [1,2] [3] While models are strongly sample-dependent, the principles of joint refinement are generally applicable to these disciplines, including the development of advanced parameterization, modeling, and analysis techniques that also consider the temporal and spatial resolutions of the two methods, leading to unambiguous data interpretation. Solutions for technical barriers must be found to realize NeX experiments, including developing robust sample environments that meet the optical requirements of neutrons and X-rays.

36 MATERIALS SCIENCE↗

An Evaluation of the Patent Portfolio Funded by the U.S. Department of Energy's Critical Materials Innovation Hub

This report describes the results of an analysis of critical materials research funded by the U.S. Department of Energy Critical Materials Innovation Hub (CMI Hub, formerly the Critical Materials Institute). The purpose of the report is to assess various characteristics of patents awarded for CMI Hub-funded innovations in critical materials technology and to determine the extent to which CMI Hub-funded research has influenced subsequent technological developments both within and beyond critical materials.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗