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NASA NTRSDate not supplied

Contamination Control for Ultra-Sensitive Life-Detection Missions

"This study report summarizes technological developments in science-required contamination control for cost-capped, life-detection missions in the Solar System. Technology advances focus on developing implementable strategies to restrict contamination of the spacecraft and instruments by the launch vehicle hardware. Secondary bake out operations during cruise further reduce molecular contaminants down to femtomolar levels in the sample path. The study validated a full-spacecraft, deployable barrier design as an effective strategy to isolate the spacecraft from the pre-launch processing and launch environment (e.g., fairing acoustic materials). It accommodates late mounting of RTGs and other required prelaunch activities. A new, high-fidelity physics, contamination-transport model for particles (including cells and their parts) and science-relevant molecules (e.g., possible biomolecules) was developed to validate the barrier concept. Importantly, this model takes into account the physics of extremely clean surfaces achieved by the best traditional contamination engineering. The ability to deal with very low levels of particulate and molecular contamination makes this model unique among standard contamination modeling approaches. Modeling also demonstrated that a high-temperature bake out during interplanetary cruise of the sample collector that comprises the largest surface area in the sample path for an Enceladus orbiter reference mission, was extremely effective. This study included the evaluation of other details necessary for an effective contamination control strategy for life detection missions including feasibility of achieving parts per trillion level cleanliness for semi-volatile hydrocarbons in nitrogen purge gas, identification of launch vehicle services required for the baseline contamination control, and defining additional contamination control measures to be taken during launch operations. Key results of the study are: • New spacecraft barrier design that accommodates RTGs is readily cleanable and repairable. Deployment of a 1/3 scale model was successfully demonstrated. • The barrier reduces particle contamination (likely biological) from fairing to spacecraft by 1e-2 to 1e-3. • On-cruise bake-out of critical surfaces significantly reduced molecular contamination (by as much as 1e-12). Subsequently, the probability of a surface contamination particle being transported to an instrument by an ice particle is less than 5.1e-5 (for microbes specifically, 4.39e-10). The report concludes that a full-spacecraft barrier designed specifically for life-detection missions that require stringent control of particulate and molecular contaminates is an effective means of mitigating risks of false positive and negative results for life signature investigations. Further, secondary cleaning steps for critical sections of the sample path can be highly effective at reducing molecular contaminants to low femtomolar levels."

contamination, life detection, barrier, modeling↗

DOE OSTI2024

Contactless Position Measurement System for Remote Alignment of Highly Reflective Objects

The Contactless Position Measurement System (CPMS) permits automatic alignment of highly-reflecting components that cannot or should not be touched by human hands, such as those used in SRF cavities. CPMS also has application during maintenance of fusion reactors, when the components in the reactor are radioactive. The length of time for which humans can handle the components in order to carry out maintenance or repairs is limited. We would like to measure the relative positions of such objects so we can bring them into alignment with motorized stages, thus eliminating the need for human contact. The CPMS is a computer vision system that measures the location of highly reflective components to within a fraction of a millimeter by finding the edges of silhouette images. This is done by placing a uniform, infrared backlight behind the components, and viewing each component with two low-aberration, infrared cameras. Each of these stereoscopic cameras are located within a coordinate system we set up with reference platforms, light sources, and survey cameras distributed around the perimeter of the string assembly room, or fusion reactor. We obtain stereoscopic silhouette images of each component, and we use these to determine the position of the component within our string assembly coordinate system. The CPMS combines the silhouette images with knowledge of the dimensions of the objects to obtain the relative positions of components in its field of view. These position measurements then allow us to mechanically maneuver the components into contact. Once we know where they are, we can move the components to where they are supposed to be with motorized stages or other mechanical means, check they are in the right place, and bolt them together. In Phase I, we built a prototype infrared backlights and cameras, tested it, wrote an analysis program to fit the images. At a range of 50 cm, we are able to measure the relative positions of two stainless steel flanges with an accuracy of 150 μm rms. The next steps are to test the analysis program with motorized stages, build a full-size prototype, and implement it in an cleanroom with SRF cavity assembly. This can be done in a cost effective way given the materials with which the system is designed. As Open Source Instruments achieved more in Phase I than anticipated, despite not receiving a Phase II SBIR grant, we hope to move forward with product development and sales with a testing partner.

43 PARTICLE ACCELERATORS↗

NASA NTRS1980

Large space systems technology electronics: Data and power distribution

The development of hardware technology and manufacturing techniques required to meet space platform and antenna system needs in the 1980s is discussed. Preliminary designs for manned and automatically assembled space power system cables, connectors, and grounding and bonding materials and techniques are reviewed. Connector concepts, grounding design requirements, and bonding requirements are discussed. The problem of particulate debris contamination for large structure spacecraft is addressed.

Dunbar, W. G.↗

NASA NTRS1989

More On Scattering From Dirty Mirrors

Mathematical model of scattering expanded from visible to include infrared wavelengths. Paper describes extension of mathematical model of scattering from mirror slightly contaminated with particulates. Original version of model applies to scattering at visible wavelengths. Updated version used to predict scattering at wavelengths from visible through infrared, based on measurements in visible spectrum.

Wang, Yaujen↗

NASA NTRS1991

Clean room survey and assessment, volume 5, appendix H

The scope of this task is to perform a comparative analysis of the various Environmental Control Life Support System (ECLSS) options for different growth scenarios. The Space Station Freedom ECLSS design and existing ground-based clean room facilities are used as a baseline for comparison. Specifically addressed here are the ground based clean room facilities at the Marshall Space Flight Center (MSFC). Given here is an evaluation of the facilities, equipment, technologies, and procedures used to maintain specified environments in typical aerospace industrial areas. Twenty-five specific clean rooms are evaluated. The objectives were to collect, compare, and catalog data for each specified facility in the areas of engineering and design, construction materials, work stations, contamination control, particulate elimination, entry systems, and instrumentation, and to make recommendations concerning enhancements required to assure an efficient and orderly evolution of MSFC clean room environmental control facilities.

Source record↗

NASA NTRS2014

ISS Ambient Air Quality: Updated Inventory of Known Aerosol Sources

Spacecraft cabin air quality is of fundamental importance to crew health, with concerns encompassing both gaseous contaminants and particulate matter. Little opportunity exists for direct measurement of aerosol concentrations on the International Space Station (ISS), however, an aerosol source model was developed for the purpose of filtration and ventilation systems design. This model has successfully been applied, however, since the initial effort, an increase in the number of crewmembers from 3 to 6 and new processes on board the ISS necessitate an updated aerosol inventory to accurately reflect the current ambient aerosol conditions. Results from recent analyses of dust samples from ISS, combined with a literature review provide new predicted aerosol emission rates in terms of size-segregated mass and number concentration. Some new aerosol sources have been considered and added to the existing array of materials. The goal of this work is to provide updated filtration model inputs which can verify that the current ISS filtration system is adequate and filter lifetime targets are met. This inventory of aerosol sources is applicable to other spacecraft, and becomes more important as NASA considers future long term exploration missions, which will preclude the opportunity for resupply of filtration products.

ISS Air Quality↗

NASA NTRS2019

Developing an Air Quality Index for Space Vehicles and Habitats

The development of an adequate tool to help the layperson understand pollution levels in their environment is of high importance. This tool must be able to inform about the levels of pollution in a simple and understandable way but also can be used for decision-making and mitigation activities to protect the health of the exposed population. One of the most useful and up-to-date approaches for characterizing air pollution is the Air Quality Index (AQI). It is an easily-calculated, powerful, data-driven tool that summarizes a complex phenomenon, such as air pollution, in straightforward indicators. The AQI system has been developed in different countries around the world, mainly for outdoor environments, based on the results of risk assessments, epidemiological studies, and current local air pollution regulations and standards. There is a need for such a system in low gravity indoor environments where air quality is of fundamental importance to astronaut health, with concerns encompassing both gaseous contaminants and particulate matter. Earth-based AQIs cannot be extrapolated to microgravity indoor environments due to different aerosol transport characteristics and altered lung deposition in low and partial gravity. The objectives of this work are to explore what areas of expertise, types of research, and data will be required to formulate a spacecraft-specific AQI. An initial dataset is available for this effort, combined from two aerosol sampling experiments, which have characterized airborne particulate matter on the International Space Station (ISS). We outline future research needs for formulating a narrowly focused version of a widely-used metric, namely, an indoor AQI for future space missions.

Sorek-Hamer, Meytar↗

NASA NTRS2019

Developing an Air Quality Index for Microgravity Indoor Environments/Space Missions

Indoor pollution sources (on Earth) that release gases or particles into the air are the primary cause of air quality problems in indoor environments. The development of an adequate tool to understand pollution levels in a certain location is of high importance. This tool must be able to inform about the levels of pollution in a simple and understandable way but also, used to take a series of predetermined measures to protect the health of the exposed population. One of the most useful and up to date approaches for characterizing air pollution is the Air Quality Index (AQI). It is an easily-calculated powerful data-driven tool, that summarizes a complex phenomenon, such as air pollution, in straightforward indicators. The AQI system has been developed in different countries around the world, mainly for outdoor environments, based on the results of risk assessments, epidemiology studies, and current local air pollution regulations and standards.Air quality in microgravity indoor environments is of fundamental importance to crew health, with concerns encompassing both gaseous contaminants and particulate matter. Although the concentration of gases in the microgravity indoor environment is well studied, aerosols remain one of the major pollutants that affect air quality and has reported adverse health effects and hasn't been reported under these unique conditions. Earth-based AQIs can't be extrapolated to microgravity indoor environments due to different aerosol characteristics and altered lung deposition in low gravity.Concurrent with the aerosol-focused AQI effort, we assess and document how the process would apply for combining particles & gases into a composite index, with the ability to query each AQI independently. All this information can be combined in a spacecraft-specific AQI for future space missions and habitats. The objective of this work are to determine what areas of expertise will contribute, what research and data will be required, and explore the scope of effort needed to formulate a spacecraft AQI in addition to analyzing ISS aerosol sampling data and incorporate results from both aerosol Sampling experiments (the only relevant data available from space).

Sorek-Hamer, Meytar↗

NASA NTRS2024

Optimizing Thin Cover Layers for Optically Clear Electrodynamic Dust Shields

This project looked at optimizing the dielectric cover layer on top of an optically clear glass electrodynamic dust shield (EDS). The EDS is a device that uses high voltage electric fields to remove dust from surfaces. Currently, the EDS uses 2000 volts to remove dust, but by optimizing the cover layer and the geometry of the EDS, this voltage can be lowered to improve safety and reduce electromagnetic interference (EMI) and the complexity of supporting systems. This project was able to demonstrate successful dust clearing on an EDS with 750 volts in high vacuum (~1E-5 torr) conditions. The EDS had a trace spacing of 500 μm, and the Parylene C cover layer had a thickness of 25 μm. There is still a substantial amount of room for improvement of these devices, which may be able to push the operating voltage even lower.

Particulate Contamination↗

NASA NTRS2010

Effects of Contamination Upon the Performance of X-Ray Telescopes

Particulate and molecular contamination can each impact the performance of x-ray telescope systems. Furthermore, any changes in the level of contamination between on-ground calibration and in-space operation can compromise the validity of the calibration. Thus, it is important to understand the sensitivity of telescope performance, especially the net effective area and the wings of the point spread function to contamination. Here, we quantify this sensitivity and discuss the flow-down of science requirements to contamination-control requirements. As an example, we apply this methodology to the International X-ray Observatory (IXO), currently under joint study by ESA, JAXA, and NASA.

O'Dell, Stephen L.↗

NASA NTRSDate not supplied

Transforming any Facility for Meeting Strict Cleanliness Requirements

Over the life of the James Webb Space Telescope (JWST), Integration & Test (I&T) has taken place in areas that needed considerable work to make the facility itself and/or the protocols used while working in the rooms suitable to meet JWST percent area coverage (PAC) and molecular accumulation requirements. In addition to normal particulate matter, JWST had a uniquely significant challenge: fibers! Fibers not only cause much higher PAC levels, but they also risk damaging the angstrom sized Near Infrared Spectrometer (NIRSpec) microshutter array (MSA), which is critical to NIRSpec instrument performance. The primary emphasis of this paper is to address particulate and fiber contamination. The success of the JWST mission required effective cleanrooms, protocols, and mitigations in non-cleanroom areas that were pressed into service to house contamination-sensitive optics and scientific instruments. Some presented profound challenges. These included: NASA’s 60-year-old Johnson Space Center (JSC) Chamber A, which had never been used for anything contamination-sensitive, and the European tropical launch facilities, which were designed to meet International Standard Organization (ISO) Class 8 processing for communication satellites. The final challenge for JWST, as if to stare us in the face and say, “I dare you to try and make me clean enough,” was preparing the 4 areas in the Centre Spatial Guyanais (CSG) Final Assembly Building (BAF) located in French Guiana, a building in which one entire side opens for Ariane 5 rocket ingress and egress. This paper will describe our initial evaluation processes and the actual work undertaken to transform even the most challenging areas into first class cleanrooms that met JWST particulate and fiber requirements.

James Webb Space Telescope↗

NASA NTRS1993

Molecular contamination and the calibration of AXAF

By the end of this decade, the two missions comprising the Advanced X-ray Astrophysics Facility (AXAF) will become the X-ray component of NASA's Great Observatories. In order to meet some of the ambitious scientific objectives, the AXAF team plans to calibrate the telescopes and instruments to an accuracy of a few percent. Particulate and molecular contamination potentially limit this precision, because they would likely change between ground calibration and orbital operation. To avoid this requires careful control over procedures affecting the coated optical surfaces, to ensure that neither particulate nor molecular contamination compromise the calibration. In particular, the fractional areal coverage by particulates or condensed droplets must be less than 0.005 projected onto the aperture plane; the thickness of any molecular film must be less than a few tens of angstrom.

Elsner, R. F.↗

NASA NTRS1976

Integrated Real Time Contamination Monitor IRTCM

Engineering and design work was performed on a monitoring device for particulate and gas contamination to be used in the space shuttle cargo area during launch at altitudes up to 50 km and during return phases of the flight. The gas sampling device consists of ampules filled with specific absorber materials which are opened and/or sealed at preprogrammed intervals. The design eliminates the use of valves which, according to experiments, are never sealing properly at hard vacuum. Methods of analysis including in-flight measuring possibilities are discussed.

Luttges, W. E.↗

NASA NTRS2008

Estimated Environmental Exposures for MISSE-3 and MISSE-4

Describes the estimated environmental exposure for MISSE-2 and MISSE-4. These test beds, attached to the outside of the International Space Station, were planned for 3 years of exposure. This was changed to 1 year after MISSE-1 and -2 were in space for 4 years. MISSE-3 and -4 operate in a low Earth orbit space environment, which exposes them to a variety of assaults including atomic oxygen, ultraviolet radiation, particulate radiation, thermal cycling, and meteoroid/space debris impact, as well as contamination associated with proximity to an active space station. Measurements and determinations of atomic oxygen fluences, solar UV exposure levels, molecular contamination levels, and particulate radiation are included.

Finckenor, Miria M.↗

NASA NTRS1974

Payload/orbiter contamination control requirement study, volume 1, exhibit A

This study is to identify and quantify the expected molecular and particulate on orbit contaminant environment for selected shuttle payloads as a result of major spacelab and shuttle orbiter contaminant sources. This investigation reviews individual payload susceptibilities to contamination, identifies the combined induced environment, identifies the risk of spacelab/payload critical surface(s) degradation, and provides preliminary contamination recommendations. It also establishes limiting factors which may depend upon operational activities associated with the payloads, spacelab, and the shuttle orbiter interface or upon independent payload functional activities.

Bareiss, L. E.↗

NASA NTRS1988

Optical contamination measurements on early Shuttle missions

Two camera/photometers were included as part of the Induced Environment Contamination Monitor on STS-2,-3,-4, and -9 orbital missions to record photographically Shuttle-induced particulate and background contamination. The cameras collected stereoscopic data continuously during the on-orbit phases of these missions making exposures every 150 s. The results recorded throughout a 32-deg field-of-view indicate high particle concentrations during early mission operations. These decay to a quiescent rate of 500 particles of greater than 10-micron radius observed per orbit. Preliminary size and velocity distributions of measured particles are presented as are measurements of background brightness due to unresolved particles in the visible spectral region.

Clifton, K. Stuart↗

NASA NTRS2017

Method for the Collection, Gravimetric and Chemical Analysis of Nonvolatile Residue (NVR) on Surfaces

Nonvolatile residue (NVR), sometimes referred to as molecular contamination is the term used for the total composition of the inorganic and high boiling point organic components in particulates and molecular films deposited on critical surfaces surrounding space structures, with the particulate and NVR contamination originating primarily from pre-launch operations. The "nonvolatile" suggestion from the terminology NVR implies that the collected residue will not experience much loss under ambient conditions. NVR has been shown to have a dramatic impact on the ability to perform optical measurements from platforms based in space. Such contaminants can be detected early by the controlled application of various detection techniques and contamination analyses. Contamination analyses are the techniques used to determine if materials, components, and subsystems can be expected to meet the performance requirements of a system. Of particular concern is the quantity of NVR contaminants that might be deposited on critical payload surfaces from these sources. Subsequent chemical analysis of the contaminant samples by infrared spectroscopy and gas chromatography mass spectrometry identifies the components, gives semi-quantitative estimates of contaminant thickness, indicates possible sources of the NVR, and provides guidance for effective cleanup procedures. In this report, a method for the collection and determination of the mass of NVR was generated by the authors at NASA Langley Research Center. This report describes the method developed and implemented for collecting NVR contaminants, and procedures for gravimetric and chemical analysis of the residue obtained. The result of this NVR analysis collaboration will help pave the way for Langley's ability to certify flight hardware outgassing requirements in support of flight projects such as Stratospheric Aerosol and Gas Experiment III (SAGE III), Clouds and the Earth's Radiant Energy System (CERES), Materials International Space Station Experiment - X (MISSE-X), and Doppler Aerosol Wind Lidar (DAWN).

Gordon, Keith↗

NASA NTRS2018

The Opera Instrument: An Advanced Curation Development for Mars Sample Return Organic Contamination Monitoring

Mars Sample Return (MSR) requires strict organic contamination control (CC) and contamination knowledge (CK) as outlined by the Mars 2020 Organic Contamination Panel (OCP). This includes a need to monitor surficial organic contamination to a ng/sq. cm sensitivity level. Archiving and maintaining this degree of surface cleanliness may be difficult but has been achieved. MSR's CK effort will be very important because all returned samples will be studied thoroughly and in minute detail. Consequently, accurate CK must be collected and characterized to best interpret scientific results from the returned samples. The CK data are not only required to make accurate measurements and interpretations for carbon-depleted martian samples, but also to strengthen the validity of science investigations performed on the samples. The Opera instrument prototype is intended to fulfill a CC/CK role in the assembly, cleaning, and overall contamination history of hardware used in the MSR effort, from initial hardware assembly through post-flight sample curation. Opera is intended to monitor particulate and organic contamination using quartz crystal microbalances (QCMs), in a self-contained portable package that is cleanroom-compliant. The Opera prototype is in initial development capable of approximately 100 ng/sq. cm organic contamination sensitivity, with additional development planned to achieve 1 ng/sq. cm. The Opera prototype was funded by the 2017 NASA Johnson Space Center Innovation Charge Account (ICA), which provides funding for small, short-term projects.

Fries, M. D.↗