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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

A Full Spectrum of Characterization for Insight into Carbon Speciation and Removal on a Cu/BEA Catalyst During Renewable High-Octane Hydrocarbon Synthesis

Conversion of methanol and dimethyl ether to high-octane gasoline catalyzed by beta zeolite (BEA) provides an opportunity for the production of high-quality fuels from renewable carbon sources (e.g., gasified biomass). Recent research demonstrated that a Cu-modified BEA zeolite catalyst (Cu/BEA) offered advantages over the unmodified BEA catalyst due to multifunctional Cu species that enabled incorporation of co-fed H2, reactivation of light alkanes, and reduction of products from the aromatic hydrocarbon pool. The shift in hydrocarbon pool chemistry has the potential to influence the identity and relative composition of surface carbon species that are often linked to deactivation. A detailed understanding of these carbon species is important to develop an effective and efficient regeneration procedure that can enable the transition from fundamental catalyst development to commercial application. Here, we applied complementary ex situ and in situ characterization techniques to compare the structures of surface carbon species on post-reaction Cu/BEA and unmodified BEA catalysts. Both catalysts contained acyclic and aromatic hydrocarbons along with graphitic carbon species. However, the post-reaction Cu/BEA catalyst had a lower polycyclic aromatic content, and further, the graphitic species were more hydrogenated and defective. It was also found that the presence of Cu promoted carbon removal at lower temperatures than for unmodified BEA through activation of O2 by Cu during thermal oxidation. The fundamental insight into the composition of surface carbon species enabled the design of an effective and efficient regeneration strategy for the DME homologation reaction over Cu/BEA, resulting in full recovery of the catalyst activity.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗
DOE OSTI2022

Performance Advantaged Thermosets from Bioderived Amines: Benefits in Manufacturing, Performance, and End-of-Life

Biomass derived monomers can offer unique functionality, often in the forms of heteroatoms, that is not easily accessible by routine petrochemical routes. Importantly, many of these monomers offer the potential to replace the petrochemical monomers used in the manufacture of thermosets to enable expanded functionality and performance. In the present work, we leverage amine containing monomers that can be obtained via biological conversions in both epoxy and benzoxazine thermosets. These monomers have a wide degree of functionality available to them that augment the material properties. In the case of benzoxazines, monomers that contain both an amine and carboxylic acid are used and the presence of the carboxylic acid leads to an acceleration in cure kinetics and a dramatic reduction in cure temperature. For the epoxy thermosets, multifunctional amine monomers are used as a hardener and the properties of the resultant materials are found to scale with the spacing and identity between reactive centers. The amines can be further modified and reacted to produce a mixed network of triazines and epoxy-amines that enables the end-of-life degradation of these materials. Importantly, subsequent process analysis reveals that the use of bioderived amines can present dramatic reductions in both supply chain energy and GHG emissions while possessing a cost similar to their petrochemical counterparts. Overall, this work demonstrates the robust potential to use bioderived amines for performance advantaged properties.

bioderived monomers↗
DOE OSTI2023

Cold Climate Integrated Heat Pump with Energy Storage for Grid-Responsive Control

An air-source integrated heat pump (ASIHP) is a multifunctional unit, capable of space cooling, space heating, and water heating. We developed a packaged cold climate ASIHP, using a multi-stage compressor, capable of working down to -25°C, and providing 100% rated capacity down to -15°C with a heating COP > 2.2. An innovative system configuration and related controls were developed to solve charge balance in the integrated heat pump, smooth charge migration, and mode transition among multiple working modes. Extensive laboratory investigations for individual modes were performed to verify the performance. Its integrated heating capability provides speedy water heating to meet domestic hot water use and store heating energy in a phase change material ceiling/panel. The heating energy storage can be used to shift the load when the electricity price is high. Based on the performance data and a calibrated model from the laboratory testing, we conducted building energy simulations driven by a model predictive control, using EnergyPlus in one U.S. cold climate zone to investigate the grid-responsive control strategy and estimate the utility cost reduction potential.

Shen, Bo↗
DOE OSTI2011

Characterization of molecular determinants for nucleocytoplasmic shuttling of PRV UL54

The pseudorabies virus (PRV) early protein UL54 is a homologue of the herpes simplex virus 1 (HSV-1) immediate-early protein ICP27, which is a multifunctional protein and essential for HSV-1 infection. To determine if UL54 might shuttle between the nucleus and cytoplasm, as has been shown for its homologues in human herpesviruses, the molecular determinants for its nucleocytoplasmic shuttling were investigated. Heterokaryon assays demonstrated that UL54 was a nucleocytoplasmic shuttling protein and this property could not be blocked by leptomycin B, an inhibitor of chromosome region maintenance 1 (CRM1). However, TAP/NXF1 promoted the nuclear export of UL54 and interacted with UL54, suggesting that UL54 shuttles between the nucleus and the cytoplasm via a TAP/NXF1, but not CRM1, dependent nuclear export pathway. Furthermore, UL54 was demonstrated to target to the nucleus through a classic Ran-, importin {beta}1- and {alpha}5-dependent nuclear import mechanism.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2013

Potential of hybrid functionalized meso-porous materials for the separation and immobilization of radionuclides

Functionalized meso-porous materials are a class of hybrid organic-inorganic material in which a meso-porous metal oxide framework is functionalized with multifunctional organic molecules. These molecules may contain one or more anchor groups that form strong bonds to the pore surfaces of the metal oxide framework and free functional groups that can impart and or modify the functionality of the material such as for binding metal ions in solution. Such materials have been extensively studied over the past decade and are of particular interest in absorption applications because of the tremendous versatility in choosing the composition and architecture of the metal oxide framework and the nature of the functional organic molecule as well as the efficient mass transfer that can occur through a well-designed hierarchically porous network. A sorbent for nuclear applications would have to be highly selective for particular radio nuclides, it would need to be hydrolytically and radiolytically stable, and it would have to possess reasonable capacity and fast kinetics. The sorbent would also have to be available in a form suitable for use in a column. Finally, it would also be desirable if once saturated with radio nuclides, the sorbent could be recycled or converted directly into a ceramic or glass waste form suitable for direct repository disposal or even converted directly into a material that could be used as a transmutation target. Such a cradle-to- grave strategy could have many benefits in so far as process efficiency and the generation of secondary wastes are concerned.This paper will provide an overview of work done on all of the above mentioned aspects of the development of functionalized meso-porous adsorbent materials for the selective separation of lanthanides and actinides and discuss the prospects for future implementation of a cradle-to-grave strategy with such materials. (author)

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2015

Recent upgrades and new scientific infrastructure of MARIA research reactor, Otwock-Swierk, Poland

The MARIA reactor is open-pool type, water and beryllium moderated. It has two independent primary cooling systems: fuel and pool cooling system. Each fuel assembly is cooled down separately in pressurized channels with individual performances characterization. The fuel assemblies consist of five layers of bent plates or six concentric tubes. Currently it is one of the most powerful research reactors in Europe with operation availability at least up to 2030. Its nominal thermal power is 30 MW. It is characterized by high neutron flux density: up to 3x10{sup 14} n cm{sup -2} s{sup -1} in case of thermal neutrons, and up to 2x10{sup 13} n cm{sup -2} s{sup -1} in case of fast neutrons. The reactor is operated for ca. 4000 h per year. The reactor facility is equipped with fully equipped three hot cells with shielding up to 10{sup 15} Bq. Adjacent to the reactor facility, the radio-pharmaceutics plant (POLATOM) and Material Research Laboratory are located. They are equipped with a number of hot cells with instrumentation. The transport system of radioactive materials from reactor facility to Material Research Laboratory is available. During 2014 the MARIA reactor has been operated with three different types of fuel the same time: previous 36% enriched fuel, and two types of new LEU fuels. In the meantime, molybdenum irradiation programme has been developed. Maria is a multifunctional research tool, with a notable application in production of radioisotopes, radio-pharmaceutics manufacturing (ca. 600 TBq/y), {sup 99}Mo for medical scintigraphy (ca. 6000 TBq/y), neutron transmutation doping of silicon single crystals, wide scientific research based on neutron beams utilization. From the beginning MARIA reactor was intended for loop and fuel testing research activities. Currently it is used mostly as material testing and irradiation facility and for that reason it has wide experimental capabilities. There are eight horizontal irradiation channels from among whom six of them are equipped with instrumentation for condensed matter physics research: - H3 - spectrometer and diffractometer with double monochromator; - H4 - small angle scattering spectrometer; - H5 - polarized neutrons spectrometer; - H6, H7 - two 3-axial crystal neutron spectrometers; - H8 - neutron radiography stand. For two horizontal channels are ongoing exploitation programs: - H2 - station with epithermal neutron beam produced in uranium converter is being developed. Intelligent converter will be installed on the periphery of reactor core. The intensity of the beam will be at the level 2x10{sup 9} n cm{sup -2}s{sup -1} what makes the beam unique in the Europe. - H1 - special pneumatic horizontal mail is being developed for irradiation material samples in the vicinity of the core i.e. in the distal part of the H1 channel. The number of neutron irradiation facilities in MARIA reactor is increasing every year. Numerous of thermal neutron irradiation channels including fast hydraulic rabbit system and large size channels for fast neutron irradiation are used routinely. Recently new in-pile facility with ITER-like neutron energy spectrum for 14 MeV neutron irradiation has been constructed. Taking into account its performance and ability of almost incessant operation the facility appears as one of the most powerful 14 MeV neutron sources. The facility shall be used for material research connected with thermonuclear devices (ITER) and 4. generation nuclear reactors. The system of independent fuels channels used in MARIA reactor appear to be very flexible and very convenient to be used as irradiation channels for uranium targets for {sup 99}Mo production. Currently, MARIA reactor supplies ca. 18% world production of {sup 99}Mo. The MARIA reactor research activities are still extended. The current scientific projects are connected e.g. with silicon neutron transmutation doping, in-pile gamma heating measurements, French calculation codes implementation (TRIPOLI4, APOLLO2). The horizontal neutron beams utilization is also developed. The MARIA reactor, due to its primary application connected with loop and fuel testing, is very convenient for testing the nuclear instrumentation, control and measurement systems.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
DOE OSTI2015

Dismantling of primary shielding with prototype machines in a compact sodium cooled reactor - 15463

The Compact Sodium Cooled Reactor Facility Karlsruhe (KNK), a prototype reactor to demonstrate the Fast Breeder Reactor Technology in Germany, was in operation from 1971 to 1991. The dismantling activities started in 1991. The project aim is the green field in 2020. Most of the reactor internals as well as the primary and secondary cooling loops have already been dismantled. The contaminated sodium inventory has already been disposed of completely. Only the highly activated reactor vessel shielding structures remain. Due to their high dose rates, these structures must be dismantled remotely. For the removal of the primary shielding of the reactor vessel, 12 stacked cast iron blocks with a total mass of 90 Mg and individual masses of up to 15.5 Mg, a remote-controlled multifunctional dismantling device (HWZ) was designed, manufactured and tested in a mock-up. Since it is not possible to remove the segments in one piece for offsite treatment, a special prototype band-saw (BWZ) had to be developed for sawing the segments both horizontally and vertically into smaller pieces. The resulting sub-segments are transferred directly into repository containers. After the successful approval of the test sequences by the authorities and intensive training of the operational staff, both prototype machines were installed inside the reactor building containment for final assembly. The dismantling started in 2013. The present paper covers the successful dismantling of the primary shielding as well as the experiences gained through the development, use and improvement of these prototype machines. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
DOE OSTI2023

Structural metamaterials comprising interpenetrating lattices

Multi-body interpenetrating lattices comprise two or more lattices that interlace or interpenetrate through the same volume without any direct physical connection to each other, wherein energy transfer is controlled by surface interactions. As a result, multifunctional or composite-like responses can be achieved by additive manufacturing of the interpenetrating lattices, even with only a single print material, with programmable interface-dominated properties. As a result, the interpenetrating lattices can have unique mechanical properties, including improved toughness, multi-stable/negative stiffness, and electromechanical coupling.

Boyce, Brad↗
DOE OSTI2019

The Telbot master-arm

It is the weight lifter with maximum flexibility: The TELBOT provides high capacity and infinite rotary motion across all axes. Special jobs call for a special robot: The TELBOT from Waelischmiller Engineering. The TELBOT particularly shows its strength in places where human operators cannot work and heavy work has to be done. For example in the nuclear industry or chemical plants. The TELBOT is a multifunctional, modular and automated robotic system with unique characteristics: no cable in or on the TELBOT-arms for unlimited, fast and precise arm motions as well as maximum efficiency and highest comfort; smooth, sealed arm and joint bodies ensure maximum radiation resistance, making the TELBOT robot the perfect helper for the nuclear sector; the TELBOT can not only be utilised for an extremely long time but is also maintenance-free and easy to decontaminate. They therefore represent an investment that will still pay out in 30 years time; sophisticated engineering skill is apparent not least in the slim design with no loss of high capacity; tools can be remotely controlled with extreme precision and the high repeat accuracy and simple implementation of complex processes ensure trouble-free and intuitive operation; programmed motion sequences bring with them noticeably comfortable and speedy operation.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2016

Validation of Criticality Analysis Capability of SuperMC with ICSBEP

SuperMC is a general purpose, intelligent and multifunctional, continuous energy Monte Carlo program for the design and safety evaluation of nuclear systems. It is designed to perform the comprehensive neutronics calculation, taking the radiation transport as the core and including the depletion, radiation source term/dose/biohazard, material activation and transmutation, etc. The latest version of SuperMC can perform the simulation of neutron, photon and coupled neutron and photon transport, and also equipped with the functions of automatic modeling and visualization. SuperMC has been verified by more than 2000 benchmark models and experiments including the handbook of International Criticality Safety Benchmark Evaluation Project (ICSBEP), the Shielding Integral Benchmark Archive Database (SINBAD), etc. The fusion reactor (ITER benchmark model, FDS Fusion Reactors), fast reactors (BN600, CLEAR-I), PWR reactors (HM, BEAVRS) and cases from the International Reactor Physics handbook Evaluation Program (IRPhEP) were employed for validating the comprehensive capability for reactor applications. In this paper, the validation of SuperMC based on the handbook of ICSBEP will be presented. ICSBEP, released by OECD/NEA, contains criticality safety benchmark specifications derived from experiments that were performed at various nuclear critical facilities around the world, which was widely used to verify neutronic codes and associated nuclear data libraries for criticality safety analysis. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
DOE OSTI2024

Multi-functional cementitious materials with ultra-high damage tolerance and self-sensing ability

Cementitious materials having high damage tolerance and self-sensing ability are described herein. These materials may replace conventional concrete to serve as a major material component for infrastructure systems with greatly improved resistance to cracking, reinforcement corrosion, and other common deterioration mechanisms under service conditions, and prevents fracture failure under extreme events. These materials can also be used for the repair, retrofitting or rehabilitation of existing concrete structures or infrastructure systems. Furthermore, these materials may offer capacity for distributed and direct sensing of cracking, straining and deterioration with spatially continuous resolution wherever the material is located, without relying on installation of sensors. The present invention relates to multifunctional cementitious structural or infrastructure materials that integrate self-sensing with damage tolerance for improving safety, extending service life, and health monitoring of structures, components, and infrastructure systems.

Li, Mo↗
DOE OSTI2025

Elastomeric Nanocomposite with Solvent‐Free, One Step, In Situ Shear Exfoliation of Graphite to Graphene

A graphene nanoflake (GNF)‐enhanced elastomeric nanocomposite (G‐EMC) is fabricated following an innovative, cost‐effective, single‐step, in situ shear exfoliation (ISE) method from low‐cost bulk material, graphite, where uniform mixing happens simultaneously within the elastomer matrix. Electron microscopy, atomic force microscopy, and photo‐induced force microscopy results show good dispersion of GNFs with exfoliation to a few layers and uniform distribution in the elastomer matrix. X‐ray photoelectron spectroscopy analysis shows less than 1% oxygen‐containing functional groups/impurity, enhanced bonding through the formation of edge sites as fracture occurs across the GNF basal plane, and pi‐pi interactions with newly exfoliated planar basal plane surfaces of the GNFs. Raman spectroscopy results confirm the formation of GNFs with only a few layers of graphene formed by the ISE process. Fabricated 10 wt.% G‐EMC nanocomposites show a 400%–500% increase in strength and fracture toughness. And 35 wt.% G‐EMCs provide an electrical conductivity of 25.64 S m −1 and a sensor gauge factor of 45. The resulting intrinsic piezo resistivity of the fabricated nanocomposite has been exploited to fabricate a multi‐functional wired and wireless sensor for detecting different body movements, speech, human vital functions, solvents, and biomolecules.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Role of Carbon Bridge Length of Organosilicate Precursors on the Atmospheric Plasma Deposition of Transparent Bilayer Protective Coatings on Plastics

Here, we demonstrate the deposition of transparent organosilicate protective bilayer coatings on poly methyl methacrylate (PMMA) substrates with different carbon chain length dipodalsilane precursors using atmospheric plasma deposition in ambient air. The bottom adhesive layer was a hybrid organosilicate coating deposited using either only carbon bridge organosilicate precursor or accompanied with a ring structure 1,5-cyclooctadiene precursor. The top layer was a dense silica coating with high elastic modulus and hardness deposited with only carbon bridge precursor. The adhesion energy of bottom layer increased with increasing carbon bridge length of precursors while the density, hardness, and elastic modulus of top hard layer decreased. The deposited bilayer structure showed ~3 times the adhesion energy and four times the elastic modulus of commercial polysiloxane sol–gel coatings.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Multiscale mechanical design of the lightweight, stiff, and damage-tolerant cuttlebone: A computational study

Cuttlebone, the endoskeleton of cuttlefish, offers an intriguing biological structural model for designing low-density cellular ceramics with high stiffness and damage tolerance. Cuttlebone is highly porous (porosity ~93%) and lightweight (density less than 20% of seawater), constructed mainly by brittle aragonite (95 wt%), but capable of sustaining hydrostatic water pressures over 20 atmospheres and exhibits energy absorption capability under compression comparable to many metallic foams (~4.4 kJ/kg). Here, in this work, we computationally investigate how such remarkable mechanical efficiency is enabled by the multiscale structure of cuttlebone. Using the common cuttlefish, Sepia Officinalis, as a model system, we first conducted high-resolution synchrotron micro-computed tomography (µ-CT) and quantified the cuttlebone's multiscale geometry, including the 3D asymmetric shape of individual walls, the wall assembly patterns, and the long-range structural gradient of walls across the entire cuttlebone (ca. 38 chambers). The acquired 3D structural information enables systematic finite-element simulations, which further reveal the multiscale mechanical design of cuttlebone: at the wall level, wall asymmetry provides optimized energy absorption while maintaining high structural stiffness; at the chamber level, variation of walls (number, pattern, and waviness amplitude) contributes to progressive damage; at the entire skeletal level, the gradient of chamber heights tailors the local mechanical anisotropy of the cuttlebone for reduced stress concentration. Our results provide integrated insights into understanding the cuttlebone's multiscale mechanical design and provide useful knowledge for the designs of lightweight cellular ceramics.

36 MATERIALS SCIENCE↗
DOE OSTI2019

NiMo-ceria-zirconia-based anode for solid oxide fuel cells operating on gasoline surrogate

A multi-functional NiMo-ceria-zirconia composite was developed as an anode for a solid oxide fuel cell (SOFC) running on isooctane that is a commonly used model fuel for gasoline. The anode layer was fabricated on an electrolyte-supported single cell using yttria-stabilized zirconia (YSZ) as the electrolyte and La0.6Sr0.4Co0.2Fe0.8O3-d as the cathode. Our results indicated that the single NiMo-ceria-zirconia layer possessed a dual-functionality: the first function was to internally convert complex hydrocarbons into a synthesis gas and the second function was to electrochemically oxidize the synthesis gas mixture for electric power generation. The addition of Mo to the Ni-ceria-zirconia allowed direct conversion of isooctane in SOFC. It significantly suppressed carbon deposition in the anode and improved the lifetime of a single cell. Additionally, the presence of Mo in the Ni-ceria-zirconia anode appeared to facilitate a higher degree of sintering, which increased the electrical conductivity and maximum power density of the single cell. When operating on isooctane at 800 °C, single cell with the 5 wt.% Mo in the Ni-ceria-zirconia-based anode displayed a maximum power density of 212 mW cm-2 at 0.48V which was higher than that of a single cell with the Ni-YSZ-based anode without the Mo promoter (49 mW cm-2 at 0.48 V).

NiMo-Ceria-Zirconia composite, Single layer multif↗
DOE OSTI2024

Coal-derived conductive pavement for winter de-icing: prototype, modeling, and simulation

Existing pavement de-icing methods result in high installation and maintenance costs, traffic delays, excessive weariness and corrosion, and negative environmental and safety impacts. To overcome these challenges, this paper presents an innovative pathway to designing and constructing smart self-heating pavements using a low-cost coal-char bearing asphalt material. The conductive asphalt incorporates coal char, i.e., a key byproduct of the coal pyrolysis process, into the Stone Mastic Asphalt (SMA) mixture. This asphalt containing coal-derived solid carbon exhibits highly tailorable electrical conductivity, satisfactory mechanical and thermophysical properties, and superior cost-efficiency as compared to other conductive pavement materials. The de-icing performance was also demonstrated by laboratory experiments on a bench-scale prototype. Furthermore, an efficient thermal network model was developed and validated by experiments to investigate the transient thermal behavior and energy performance of the Ohmic heating pavement system. Furthermore, the whole-year energy simulation case studies were conducted on a bridge pavement with an annual energy use of 24.6–1444.8 kWh/m 2 , showcasing its potential in field applications across cool humid, cold humid, and subarctic/arctic climate zones.

42 ENGINEERING↗
DOE OSTI2015

Encapsulation of superparamagnetic Fe 3 O 4 @SiO 2 core/shell nanoparticles in MnO 2 microflowers with high surface areas

Microflowers made of interconnected MnO2 nanosheets have been successfully synthesized in a microwave reactor through a hydrothermal reduction of KMnO4 with aqueous HCl at elevated temperatures in the presence of superparamagnetic Fe3O4@SiO2 core-shell nanoparticles. Due to the chemical compatibility between SiO2 and MnO2, the heterogeneous reaction leads to the spontaneous encapsulation of the Fe3O4@SiO2 core-shell nanoparticles in the MnO2 microflowers. The resulting hybrid particles exhibit multiple properties including high surface area associated with the MnO2 nanosheets and superparamagnetism originated from the Fe3O4@SiO2 core-shell nanoparticles, which are beneficial for applications requiring both high surface area and magnetic separation. (C) 2014 Yu-Gang Sun.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Factors affecting direct lightning strike damage to fiber reinforced composites: A review

In recent years, Carbon Fiber Reinforced Plastics (CFRP) or Glass Fiber Reinforced Plastics (GFRPs) have become a very common material for aircraft and wind turbine structures. These structures are often protected from lightning strikes using conventional metal-based protective films/foils. Non-conventional, non-metallic lightning strike protection (LSP) technologies have not yet been fully realized, but research on non-conventional LSP systems for CFRPs has gained momentum in the last few years. The discovery of new structural conductive materials and improvements in the processing of carbon nano-filler based composites have challenged the conventional metal-based LSP systems by providing the potential for lightweight, non-metallic alternatives. However, a major challenge in using non-conventional LSP is the complex nature of a lightning strike event and its complicated thermal and mechanical impact on CFRP structures. Understanding the direct effect of a lightning strike on a CFRP structure requires understanding multiple transient loads, such as electrical, thermal, magnetic, acoustics, shock, and inertia. This review article focuses on new findings and discusses the complex direct effects of lightning on CFRPs. Specifically, the focus is to find the important factors that regulate and control the damage to FRPs are classified and discussed with the help of available literature based on experimental results. Finally, possibilities and limitations to these new findings are discussed.

36 MATERIALS SCIENCE↗

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