Materials Science Work at NASA Ames Research Center
The paper discusses the following: Thermal Protection System -TPS development and testing; Material for the shuttle; Ablators; Coating; Integrated vehicle health management; Sharp leading edges.
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The paper discusses the following: Thermal Protection System -TPS development and testing; Material for the shuttle; Ablators; Coating; Integrated vehicle health management; Sharp leading edges.
The National Aeronautics & Space Administration (NASA) has identified Liquid Oxygen (LOX)/Liquid Methane (LCH4) as a potential propellant combination for future space vehicles based upon exploration studies. The technology is estimated to have higher performance and lower overall systems mass compared to existing hypergolic propulsion systems. Besides existing in-house risk reduction activities, NASA has solicited from industry their participation on component technologies based on the potential application to the lunar ascent main engine (AME). Contracted and NASA efforts have ranged from valve technologies to engine system testbeds. The application for the AME is anticipated to be an expendable, pressure-fed engine for ascent from the moon at completion of its lunar stay. Additionally, the hardware is expected to provide an abort capability prior to landing, in the event that descent systems malfunction. For the past 4 years, MSFC has been working with the Glenn Research Center and the Johnson Space Center on methane technology development. This paper will focus on efforts specific to MSFC in pursuing ignition, injector performance, chamber material assessments and cryogenic valve technologies. Ignition studies have examined characteristics for torch, spark and microwave systems. Injector testing has yielded insight into combustion performance for shear, swirl and impinging type injectors. The majority of chamber testing has been conducted with ablative and radiatively cooled chambers with planned activities for regenerative and transpiration cooled chambers. Lastly, an effort is underway to examine the long duration exposure issues of cryogenic valve internal components. The paper will summarize the status of these efforts.
An experimental investigation of boundary-layer transition and convective surface heating on wind tunnel models that simulated aeroshells comprised of multiple blocks of thermal protection system (TPS) material has been performed. Two representative entry vehicle geometries, a sphere-cone aeroshell and a sphere-cone aeroshell, were considered. Multiple cast ceramic models of each geometry were fabricated with varying fence heights or gap depths to represent gap fillers that either protrude above, or are recessed below, the TPS blocks due to differential ablation during reentry. Wind tunnel testing was performed at Mach 6 over a range of Reynolds numbers sufficient to produce laminar, transitional, and turbulent flow. Convective surface heating and boundary-layer transition onset data were obtained using global phosphor thermography. The experimental heating data are presented herein, as are comparisons to laminar and turbulent smooth-wall heat transfer distributions from computational flow field simulations.
This work discusses the ablative response of thermal protection system materials when exposed to aerothermal environments. It focuses on modeling instrumented test article assemblies tested in the Plasmatron X inductively coupled plasma wind tunnel. For this purpose, as the samples are mounted to a water-cooled arm using numerous assembly components and are embedded with thermocouples for in-depth temperature measurements, the variation in ablative response of the samples as a result of these components is studied. The aerothermal boundary conditions for Plasmatron X are obtained for hypersonic flight-relevant conditions using the multi-physics aerothermal framework built at the University of Illinois at Urbana-Champaign. For simulating the material response, a material response code, Porous Material Analysis Toolbox based on OpenFOAM (PATO) is used. In PATO, numerous configurations and materials of thermocouples were studied. The optimal configuration for obtaining temperature measurements with minimal error using embedded thermocouples was found to be the U-shaped Type S, 30 American wire gauge thermocouple configuration.
This work discusses the ablative response of thermal protection system materials when exposed to aerothermal environments. It focuses on modeling instrumented test article assemblies tested in the Plasmatron X inductively coupled plasma wind tunnel. For this purpose, as the samples are mounted to a water-cooled arm using numerous assembly components and are embedded with thermocouples for in-depth temperature measurements, the variation in ablative response of the samples as a result of these components is studied. The aerothermal boundary conditions for Plasmatron X are obtained for hypersonic flight-relevant conditions using the multi-physics aerothermal framework built at the University of Illinois at Urbana-Champaign. For simulating the material response, a material response code, Porous Material Analysis Toolbox based on OpenFOAM (PATO) is used. In PATO, numerous configurations and materials of thermocouples were studied. The optimal configuration for obtaining temperature measurements with minimal error using embedded thermocouples was found to be the U-shaped Type S, 30 American wire gauge thermocouple configuration.
We have tested the effects of neuromuscular denervation in Drosophila by laser-ablating the RP motoneurons in intact embryos before synaptogenesis. We examined the consequences of this ablation on local synaptic connectivity in both 1st and 3rd instar larvae. We find that the partial or complete loss of native innervation correlates with the appearance of alternate inputs from neighboring motor endings and axons. These collateral inputs are found at ectopic sites on the denervated target muscle fibers. The foreign motor endings are electrophysiologically functional and are observed on the denervated muscle fibers by the 1st instar larval stage. Our data are consistent with the existence of a local signal from the target environment, which is regulated by innervation and influences synaptic connectivity. Our results show that, despite the stereotypy of Drosophila neuromuscular connections, denervation can induce local changes in connectivity in wild-type Drosophila, suggesting that mechanisms of synaptic plasticity may also be involved in normal Drosophila neuromuscular development.
The Orion (CEV) thermal protection system (TPS) advanced development project (ADP) was initiated in late 2006 to reduce developmental risk by significant investment in multiple heat shield architectural solutions that can meet the needs both the Low Earth orbit (LEO) and Lunar return missions. At the same time, the CEV TPS ADP was also charged with developing a preliminary design for the heat shield to meet the PDR requirement and at the time of the PDR, transfer the design to Lockheed- Martin, the prime contractor. We reported on the developmental activities of the first 18 months at the IPPW5 in Bordeaux, France, last summer. In June 08, at the time of the IPPW6, the CEV TPS ADP would have nearly completed the preparation for the Orion PDR and would be close to the original three-year mark. We plan to report on the progress at the Atlanta workshop. In the past year, Orion TPS ADP investment in TPS Technology, especially in PICA ablative Heat-shield design, development, testing and engineering (DDTE) has paid off in enabling MSL mission to switch from SLA 561 V heat shield to PICA heat shield. CEV TPS ADP considered SLA 561 V as a candidate for LEO missions and our testing identified failure modes in SLA and as a result, we dropped SLA for further evaluation. This close synergy between two projects is a highly visible example of how investment in technology areas can and does benefit multiple missions. In addition, CEV TPS ADP has been able to revive the Apollo ablative system namely AVCOAT honeycomb architecture as an alternate to the baseline PICA architecture and we plan to report the progress we have made in AVCOAT. CEV TPS ADP has invested considerable resources in developing analytical models for PICA and AVCOAT, material property measurements that is essential to the design of the heat-shield, in arcjet testing, in understanding the differences between different arc jet facilities, namely NASA Ames, NASA JSC and Air Force's AEDC, and in Non-Destructive Evaluation (NDE), and in integration of and manufacturing heat shield as a system. The capabilities of the two heat shield systems including failure modes via testing and analysis, once established, can serve the Probe Community and future mission designers to inner and outer planetary exploration very well. For example, missions to Venus, Mars and Titan can use either one of the system by selecting the mission design parameters that utilizes the full characteristics of these system to make use of system efficiency that will result in reduced heat shield mass, system robustness that will enhance mission success and cost. We plan to present significant progresses of the past three years and highlight the significant contributions CEV TPS ADP Project has made to advance the state of the art in Thermal Protection System technology that has and will continue to benefit future entry probe missions.
Ablation and temperature data for Apollo heat shield material using Pacemaker vehicle for flight test
There are several harsh space environments that could affect thermal protection systems and in turn pose risks to the atmospheric entry vehicles. These environments include micrometeoroid impact, extreme cold temperatures, and ionizing radiation during deep space cruise, all followed by atmospheric entry heating. To mitigate these risks, different thermal protection material samples were subjected to multiple tests, including hyper velocity impact, cold soak, irradiation, and arcjet testing, at various NASA facilities that simulated these environments. The materials included a variety of honeycomb packed ablative materials as well as carbon-based non-ablative thermal protection systems. The present paper describes the results of the multiple test campaign with a focus on arcjet testing of thermal protection materials. The tests showed promising results for ablative materials. However, the carbon-based non-ablative system presented some concerns regarding the potential risks to an entry vehicle. This study provides valuable information regarding the capability of various thermal protection materials to withstand harsh space environments, which is critical to sample return and planetary entry missions.
When Apollo was designed to carry astronauts safely back from the Moon, at return speeds exceeding 11 km/s, it required development of a new lightweight ablative material to protect the capsule and crew from the intense heat of entry. Soon after the Apollo program, successful Mars Viking Lander missions employed a different and much lighter ablator in more benign entry conditions. On the other hand, the Pioneer-Venus and Galileo Probe missions that followed required yet another ablative system, to manage the extreme heating at those destinations, which was like flying a ballistic missile nose tip into a thermonuclear explosion. NASA had to invent a new heat-shield concept based on the rocket nozzle and ballistic missile ablative materials. In the mid 1990's, as the Science focus returned to Mars, advances in manufacturing, testing and materials technology led to innovative lightweight ablators that enabled comet and asteroid sample return missions and facilitated large lander missions such as MSL and Mars 2020. NASA's current plans for robotic and human exploration of the Moon, Mars and beyond introduce different constraints and new expectations for ablators. Human missions to Moon and Mars, sample return missions from Mars, and exploration of Uranus and Neptune, the two planets we are yet to explore, will require ablators that can withstand extreme environments, with verifiable robustness, and with raw materials and manufacturing approaches that are sustainable in the longer term. This talk will review the history of ablators as well as current ablative TPS development that addresses the requirements for future missions to Moon, Mars and beyond.
One of the primary goals of the Asteroid Threat Assessment Program (ATAP) is to understand the ablation phenomena of meteors (e.g., spallation, evaporation, melt flow, etc.). Therefore, a test campaign was executed at the Hypersonic Material Test System (HYMETS) facility on samples of an ordinary chondrite (e.g., Tamdakht) and samples of basalt from the Columbia plateau. High melt viscosities and low ablation rates are predicted for basalt due to higher concentrations of silica and alumina in the matrix phase. However, high-speed video and post-test analysis reveal that basalt experiences greater rates of ablation than Tamdakht. Post-test analysis of emission spectra reveals the presence of volatile species that may explain the discrepancy between model predictions and observed phenomena.
Identification of innovative solutions to unique materials problems is an every-day quest for members of the aerospace community. Finding a technique that will minimize costs, maximize throughput, and generate quality results is always the target. United Space Alliance Materials Engineers recently conducted such a search in their drive to return the Space Shuttle fleet to operational status. The removal of high performance thermal coatings from solid rocket motors represents a formidable task during post flight disassembly on reusable expended hardware. The removal of these coatings from unfired motors increases the complexity and safety requirements while reducing the available facilities and approved processes. A temporary solution to this problem was identified, tested and approved during the Solid Rocket Booster (SRB) return to flight activities. Utilization of ultra high-pressure liquid nitrogen (LN2) to strip the protective coating from assembled space shuttle hardware marked the first such use of the technology in the aerospace industry. This process provides a configurable stream of liquid nitrogen (LN2) at pressures of up to 55,000 psig. The performance of a one-time certification for the removal of thermal ablatives from SRB hardware involved extensive testing to ensure adequate material removal without causing undesirable damage to the residual materials or aluminum substrates. Testing to establish appropriate process parameters such as flow, temperature and pressures of the liquid nitrogen stream provided an initial benchmark for process testing. Equipped with these initial parameters engineers were then able to establish more detailed test criteria that set the process limits. Quantifying the potential for aluminum hardware damage represented the greatest hurdle for satisfying engineers as to the safety of this process. Extensive testing for aluminum erosion, surface profiling, and substrate weight loss was performed. This successful project clearly demonstrated that the liquid nitrogen jet possesses unique strengths that align remarkably well with the unusual challenges that space hardware and missile manufacturers face on a regular basis. Performance of this task within the confines of a critical manufacturing facility marks a milestone in advanced processing.
Four subscale solid rocket motor tests were conducted successfully to evaluate alternate nozzle liner, insulation, and exit cone structural overwrap components for possible application to the Space Shuttle Solid Rocket Motor (SRM) nozzle asasembly. The 10,000 lb propellant motor tests were simulated, as close as practical, the configuration and operational environment of the full scale SRM. Fifteen PAN based and three pitch based materials had no filler in the phenolic resin, four PAN based materials had carbon microballoons in the resin, and the rest of the materials had carbon powder in the resin. Three nozzle insulation materials were evaluated; an aluminum oxide silicon oxide ceramic fiber mat phenolic material with no resin filler and two E-glass fiber mat phenolic materials with no resin filler. It was concluded by MTI/WD (the fabricator and evaluator of the test nozzles) and NASA-MSFC that it was possible to design an alternate material full scale SRM nozzle assembly, which could provide an estimated 360 lb increased payload capability for Space Shuttle launches over that obtainable with the current qualified SRM design.
Low-level doped solid metal/liquid metal experiments analyzed by laser ablation ICP-MS allow Henry's Law to be tested. The results indicate Henry's Law is obeyed and the experimental partition coefficients can be applied to iron meteorites. Additional information is contained in the original extended abstract.
In 2012, the entry vehicle for the Mars Science Laboratory (MSL) mission was the largest and heaviest vehicle flown to another planet, designed to be able to withstand the largest heat fluxes in the Martian atmosphere ever attempted. The heatshield material that had been successfully used for all previous Mars missions had been baselined in the design, but during the development and qualification testing demonstrated catastrophic and unexplained failures. With only 10 months remaining before the original launch date, the TPS team led by NASA Ames designed and implemented a first-ever tiled, ablative heatshield. Highlights from MSL of the testing difficulties and innovations required to execute a new heatshield design will be presented, along with a sneak peak of the Mars 2020 mission.
In 2012, the entry vehicle for the Mars Science Laboratory (MSL) mission was the largest and heaviest vehicle flown to another planet, designed to be able to withstand the largest heat fluxes in the Martian atmosphere ever attempted. The heatshield material that had been successfully used for all previous Mars missions had been baselined in the design, but during the development and qualification testing demonstrated catastrophic and unexplained failures. With only 10 months remaining before the original launch date, the TPS team led by NASA Ames designed and implemented a first-ever tiled, ablative heatshield. Highlights from MSL of the testing difficulties and innovations required to execute a new heatshield design will be presented, along with a sneak peak of the Mars 2020 mission.
In 2012, the entry vehicle for the Mars Science Laboratory (MSL) mission was the largest and heaviest vehicle flown to another planet, designed to be able to withstand the largest heat fluxes in the Martian atmosphere ever attempted. The heatshield material that had been successfully used for all previous Mars missions had been baselined in the design, but during the development and qualification testing demonstrated catastrophic and unexplained failures. With only 10 months remaining before the original launch date, the TPS team led by NASA Ames designed and implemented a first-ever tiled, ablative heatshield. Highlights from MSL of the testing difficulties and innovations required to execute a new heatshield design will be presented, along with a sneak peak of the Mars 2020 mission.
A program was initiated at the Kennedy Space Center in December 1967 and conducted through December 1969 to evaluate the performance of heat- and blast-protection materials for ground support equipment used during the Apollo/Saturn launches. Materials believed to be generally suitable for heat and blast protection were subjected to launch-exposure tests. Tests were made during the Apollo/Saturn 502, 503, and 505 launches. Tests were also made in a local laboratory, as an alternative to the restrictive requirements of launch-exposure tests, to determine the effects of torch-flame exposure on ablative materials. Five materials were found to be satisfactory in all major test categories. It was determined that torch-flame tests can probably be utilized as an acceptable substitute for the booster-engine-exhaust exposure tests for basic screening of candidate materials.