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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 199 records · Page 11
All sourcesNASA NTRSDOE OSTI
NASA NTRS1993

Mineralogy of three slightly palagonitized basaltic tephra samples from the summit of Mauna Kea, Hawaii

The paper characterizes the mineralogy and spectral properties of three slightly palagonitized basaltic tephra samples collected near the summit of Mauna Kea in order to contribute to the basis for inferring mineralogy and processes for Martian surface materials. The mineralogy of size fractions of these samples is examined by diffuse reflectance and FIR spectroscopy, optical microscopy, X-ray diffraction, Moessbauer spectroscopy, magnetic analysis, EMPA, TEM, and SEM. For the 20-1000 micron size fraction, sample HWMK11 (red) is essentially completely oxidized and has a hematite (Ti-hematite) pigment dispersed throughout the silicate matrix. Sample HWMK12 (black) has the lowest proportion of ferric-bearing phases and is thus least weathered. For HWMK11, the amount of hematite is essentially constant, and mica is present only in the coarse clay-sized fraction; smectites are low in structural Fe.

Golden, D. C.↗
NASA NTRS1984

Fine-grained millimeter-sized objects in type 3 ordinary chondrites and their relation to chondrules and matrix

Fine-grained, opaque, silicate-rich matrix material, occurring as rims on chondrules and clasts, discrete clasts, and between chondrule and mineral fragments is a primitive component of chondrites and may resemble the material from which chondrules formed. To elucidate the relationship between chondrules and matrix and to help identify chondrule precursor material, the nimeralogy and bulk compositions of 30 mm-sized, fine-grained objects in Tieschitz (h3.6), Sharps (H3.4), Allan Hills A77299 (H3.7), Yamato 74191 (L3.6), Semarkona (LL3.0), and St. Mary's Co. (LL3.3) were studied. All are composed of submicron to micron sized material and may contain larger mineral fragments. Three texturally and mineralogically distinct types of objects were identified; all are minor components of the chondrites studied ( 1% except Sharps where melt-breccia-textured objects are approximately minus 1%). Bulk compositions of network and melt-breccia-textured objects define a rather narrow trend on a plot of Si/Al vs. Mg/Al, emphasizing a possible genetic relationship. Data show that Si/Mg is higher for network and melt-breccia-textured objects than for porphyritic and barred olivine chondrules. Melting in vaccuo of network-textured objects would cause a loss of Si relative to Mg (3), suggesting that material compositionally similar to fine grained objects could have been precursors to some chondrules.

Recca, S. I.↗
NASA NTRS2017

Unconventional Imaging with Contained Granular Media

Typically, the cost of a space-borne imaging system is driven by the size and mass of the primary aperture. The solution that we propose uses a method to construct an imaging system in space in which the nonlinear optical properties of a cloud of micron-sized particles, shaped into a specific surface by electromagnetic means, and allows one to form a very large and lightweight aperture of an optical system, hence reducing overall mass and cost. Recent work at JPL has investigated the feasibility of a granular imaging system, concluding that such a system could be built and controlled in orbit. We conducted experiments and simulation of the optical response of a granular lens. In all cases, the optical response, measured by the Modulation Transfer Function, of hexagonal reflectors was closely comparable to that of a conventional spherical mirror. We conducted some further analyses by evaluating the sensitivity to fill factor and grain shape, and found a marked sensitivity to fill factor but no sensitivity to grain shape. We have also found that at fill factors as low as 30%, the reflection from a granular lens is still excellent. Furthermore, we replaced the monolithic primary mirror in an existing integrated model of an optical system (WFIRST Coronagraph) with a granular lens, and found that the granular lens that can be useful for exoplanet detection provides excellent contrast levels. We will present our testbed and simulation results in this paper.

Sidick, Erkin↗
DOE OSTI2020

Unveiling 3D Morphology of Multiscale Micro-Nanosilver Sintering for Advanced Electronics Manufacturing by Ptychographic X-ray Nanotomography

The sintering processing–structure–property relationship of a multiscale silver materials is investigated: microparticles with nanofeatures, particularly on their three-dimensional (3D) morphology. The target application is to replace conventional lead-based solders in advanced electronic manufacturing. Unlike lead-based solders, silver powders are suited to satisfy increasingly demanding mechanical, electrical, and thermal requirements, meanwhile being free of health effect. Sintering the material at a low temperature and without applied pressure are desirable conditions, which results in a preferred use of silver nanoparticles, as nanofeatures have higher driving force to sinter with the decrease in particle size. However, nanosized powders present potential health/environmental effects. To address the trade-off between the benefits and shortcomings of nano-versus microparticles, this work studies a novel multiscale silver paste, namely micron-sized powders with nanosized features. To get quantitative 3D visualization of micro- and nanoscale features, ptychographic X-ray computed nanotomography is applied. The correlations between conditions (thermal aging, pressure, and substrate metallization), mechanical properties, and morphological parameters are established. Finally, using novel 3D X-ray nanoimaging technique, it is demonstrated that one can design multiscale materials while balancing complex demands required in advanced electronics manufacturing and research directions in materials design and characterization.

36 MATERIALS SCIENCE↗
NASA NTRS1992

Upper-atmosphere Aerosols: Properties and Natural Cycles

The middle atmosphere is rich in its variety of particulate matter, which ranges from meteorite debris, to sulfate aerosols, to polar stratospheric ice clouds. Volcanic eruptions strongly perturb the stratospheric sulfate (Junge) layer. High-altitude 'noctilucent' ice clouds condense at the summer mesopause. The properties of these particles, including their composition, sizes, and geographical distribution, are discussed, and their global effects, including chemical, radiative, and climatic roles, are reviewed. Polar stratospheric clouds (PSCs) are composed of water and nitric acid in the form of micron-sized ice crystals. These particles catalyze reactions of chlorine compounds that 'activate' otherwise inert chlorine reservoirs, leading to severe ozone depletions in the southern polar stratosphere during austral spring. PSCs also modify the composition of the polar stratosphere through complex physiocochemical processes, including dehydration and denitrification, and the conversion of reactive nitrogen oxides into nitric acid. If water vapor and nitric acid concentrations are enhanced by high-altitude aircraft activity, the frequency, geographical range, and duration of PSCs might increase accordingly, thus enhancing the destruction of the ozone layer (which would be naturally limited in geographical extent by the same factors that confine the ozone hole to high latitudes in winter). The stratospheric sulfate aerosol layer reflects solar radiation and increases the planetary albedo, thereby cooling the surface and possibly altering the climate. Major volcanic eruptions, which increase the sulfate aerosol burden by a factor of 100 or more, may cause significant global climate anomalies. Sulfate aerosols might also be capable of activating stratospheric chlorine reservoirs on a global scale (unlike PCSs, which represent a localized polar winter phenomenon), although existing evidence suggests relatively minor perturbations in chlorine chemistry. Nevertheless, if atmospheric concentrations of chlorine (associated with anthropogenic use of chlorofluorocarbons) continue to increase by a factor of two or more in future decades, aircraft emissions of sulfur dioxide and water vapor may take on greater significance.

Turco, Richard P.↗
NASA NTRS1995

Physical and Optical/Radiative Characteristics of Small Particles in Tropical Cirrus

Whether cirrus clouds heat or cool the Earth-atmosphere system depends on the relative importance of the cloud shortwave albedo effect and the cloud thermal greenhouse effect. Both an determined by the distribution of ice condensate with cloud particle size. The microphysics instrument package flown aboard the DC-8 In TOGA/COARE included an ice crystal replicator, a 2D Greyscale Cloud Particle Probe and a Forward Scattering Spectrometer Aerosol Probe. In combination. these instruments permitted particle size measurements between 0.5 micrometers and 2.6 mm diameter. Ice crystal replicas were used to validate signals from the electro-optical instruments. Typical results show a prevalence in tropical cirrus clouds of micron-sized particles, in addition to cloud particles that exceed 100 micrometer radius. The mechanism of their formation is growth of (hygroscopic, possibly ocean-derived) aerosol particles along the Kohler curves. The concentration of small particles is higher and less variable in space and time, and their tropospheric residence time is longer, than those of large cloud particles because of lower sedimentation velocities. Small particles shift effective cloud particle radii to sizes much smaller than the mean diameter of the cloud particles. This causes an increase in shortwave reflectivity and IR emissivity. and a decrease in transmissivity. In the cirrus outflow of tropical cyclone Oliver on 8 February, 1993, the reflectivity increases with altitude (decreasing temperature) stronger than does cloud emissivity, yielding enhanced radiative cooling at higher altitudes.

Pueschel, R. F.↗
NASA NTRS2014

The Gemini NICI Planet-Finding Campaign: The Offset Ring of HR 4796 A

We present J, H, CH4 short (1.578 micrometers), CH4 long (1.652 micrometers) and K(sub s)-band images of the dust ring around the 10 Myr old star HR 4796 A obtained using the Near Infrared Coronagraphic Imager (NICI) on the Gemini-South 8.1 m Telescope. Our images clearly show for the first time the position of the star relative to its circumstellar ring thanks to NICI's translucent focal plane occulting mask. We employ a Bayesian Markov chain Monte Carlo method to constrain the offset vector between the two. The resulting probability distribution shows that the ring center is offset from the star by 16.7 +/- 1.3 milliarcseconds along a position angle of 26 +/- 3deg, along the PA of the ring, 26.47 +/- 0.04deg. We find that the size of this offset is not large enough to explain the brightness asymmetry of the ring. The ring is measured to have mostly red reflectivity across the JHKs filters, which seems to indicate micron-sized grains. Just like Neptune's 3:2 and 2:1 mean-motion resonances delineate the inner and outer edges of the classical Kuiper belt, we find that the radial extent of the HR 4796 A and the Fomalhaut rings could correspond to the 3:2 and 2:1 mean-motion resonances of hypothetical planets at 54.7 AU and 97.7 AU in the two systems, respectively. A planet orbiting HR 4796 A at 54.7 AU would have to be less massive than 1.6 Jup mass so as not to widen the ring too much by stirring.

Near Infrared Coronagraphic Imager (NICI)↗
NASA NTRS1978

Particle impact tests

Particle impact tests were performed on three types of orbiter surface with a micrometeoroid facility. The test equipment electrostatically accelerated micron sized particles to high velocities simulating micrometeoroid impacts. Test particles were titanium diboride with typical velocities in the range 1 to 2.3 km x sec/1 and equivalent particle diameters in the range 4 to 16 microns. Impact angles to the material surface were 90, 60 and 30 degrees. The particle impact sites were located on the sample surfaces and craters were photographed with a magnification of 400X.

Komatsu, G. K.↗
DOE OSTI2025

Diffusion and Deformation Mechanism Maps in Li Metal from Atomistic Simulations

The rate of Li transport in the Li metal anode is important for the operation of Li metal-solid state batteries. Here, transport rates due to diffusion and creep are predicted in Li using atomistic simulations. First, molecular dynamics is used to estimate the rate of Li diffusion along dislocations and in grain boundary triple junctions. By combining this data with that from a prior study of grain boundary diffusion the dominant mechanisms and rates of self-diffusion in Li polycrystals are predicted as a function of grain size, grain shape, dislocation density, and temperature. Second, the dominant creep mechanisms are predicted and used to estimate critical current densities and void annihilation times. Grain boundary sliding and coble creep are the dominant mechanisms for micron-sized grains. Lastly, a continuum model for interfacial contact loss reveals that high dislocation densities of ∼10 12 /cm 2 enable achieving battery performance targets for Li grain sizes of ∼10 μm.

Batteries↗
NASA NTRS1991

Aerosol characterization in smoke plumes from a wetlands fire

Results are presented from airborne measurements of aerosol mass loading, size distribution, and elemental composition obtained in a smoke plume from a fire at a Florida wildlife refuge. It is found that there was a high concentration of carbon-containing aerosols and salt crystals in the 0.1-0.2 micron size range; the composition and morphology of the aerosols differed with size. Aerosol mass concentrations are used in conjunction with those obtained for CO2 in order to calculate ratios of aerosol and CO2. The ratios are noted to be higher for the smoldering phase of the fire than for its flaming phase.

Woods, David C.↗
DOE OSTI2024

Nanobubble Formation and Coverage during High Current Density Alkaline Water Electrolysis

Gas bubbles are a necessary byproduct of water electrolysis whereby hydrogen and oxygen are produced from water. These attached gases reduce the electrode’s active area, which necessitates a deep understanding of the bubble life cycle starting from nanobubbles. Synchronized with the electrochemistry, the time evolution of the surface nanobubble size and coverage is resolved using grazing incidence small-angle X-ray scattering (GISAXS) and correlated with optical microscopy and theoretical calculations to show that a significant portion of the surface is covered in nanobubbles after larger micron-sized bubbles are observed. Further, these nanobubbles increase in number and decrease in size, toward 2 nm diameter, with the charge passed. The trend in size and number is consistent with an increase in supersaturation, which reduces the nascent bubble size. Altogether, this study suggests a significant portion of the surface contains nanobubbles and that strategies to reduce the dissolved hydrogen would be effective at reducing the nanobubble surface coverage.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS2017

NIAC Phase II Orbiting Rainbows: Future Space Imaging with Granular Systems

Inspired by the light scattering and focusing properties of distributed optical assemblies in Nature, such as rainbows and aerosols, and by recent laboratory successes in optical trapping and manipulation, we propose a unique combination of space optics and autonomous robotic system technology, to enable a new vision of space system architecture with applications to ultra-lightweight space optics and, ultimately, in-situ space system fabrication. Typically, the cost of an optical system is driven by the size and mass of the primary aperture. The ideal system is a cloud of spatially disordered dust-like objects that can be optically manipulated: it is highly reconfigurable, fault-tolerant, and allows very large aperture sizes at low cost. This new concept is based on recent understandings in the physics of optical manipulation of small particles in the laboratory and the engineering of distributed ensembles of spacecraft swarms to shape an orbiting cloud of micron-sized objects. In the same way that optical tweezers have revolutionized micro- and nano-manipulation of objects, our breakthrough concept will enable new large scale NASA mission applications and develop new technology in the areas of Astrophysical Imaging Systems and Remote Sensing because the cloud can operate as an adaptive optical imaging sensor. While achieving the feasibility of constructing one single aperture out of the cloud is the main topic of this work, it is clear that multiple orbiting aerosol lenses could also combine their power to synthesize a much larger aperture in space to enable challenging goals such as exo-planet detection. Furthermore, this effort could establish feasibility of key issues related to material properties, remote manipulation, and autonomy characteristics of cloud in orbit. There are several types of endeavors (science missions) that could be enabled by this type of approach, i.e. it can enable new astrophysical imaging systems, exo-planet search, large apertures allow for unprecedented high resolution to discern continents and important features of other planets, hyperspectral imaging, adaptive systems, spectroscopy imaging through limb, and stable optical systems from Lagrange-points. Furthermore, future micro-miniaturization might hold promise of a further extension of our dust aperture concept to other more exciting smart dust concepts with other associated capabilities. Our objective in Phase II was to experimentally and numerically investigate how to optically manipulate and maintain the shape of an orbiting cloud of dust-like matter so that it can function as an adaptable ultra-lightweight surface. Our solution is based on the aperture being an engineered granular medium, instead of a conventional monolithic aperture. This allows building of apertures at a reduced cost, enables extremely fault-tolerant apertures that cannot otherwise be made, and directly enables classes of missions for exoplanet detection based on Fourier spectroscopy with tight angular resolution and innovative radar systems for remote sensing. In this task, we have examined the advanced feasibility of a crosscutting concept that contributes new technological approaches for space imaging systems, autonomous systems, and space applications of optical manipulation. The proposed investigation has matured the concept that we started in Phase I to TRL 3, identifying technology gaps and candidate system architectures for the space-borne cloud as an aperture.

Quadrelli, Marco B.↗
NASA NTRS1974

Particle flow in blade passages of turbomachinery with application to laser-Doppler velocimetry

A theoretical analysis was conducted of the dynamic behavior of micron size particles entrained in gas flow on the two-dimensional blade-to-blade surface of a circular stationary cascade of turbine stator blades. The particle velocity lag and angular deviation relative to the gas was determined as a function of particle diameter and mass density. Particles size and density were varied over ranges selected to correspond to typical laser-Doppler velocimeter (LDV) flow field mapping applications. It was found that velocity lag and angular deviation increased whenever particle size or mass density increased, and that particle tracking was more sensitive to a change in particle diameter than to a change in mass density. Results indicated that LDV applications employing 1 gm/cc tracer particles with diameters greater than approximately 1 micron, or 0.5 micron diameter particles with mass densities greater than 4 gm/cc would experience velocity and angular deviations generally greater than 2 percent and 1 degree, respectively.

Maxwell, B. R.↗
DOE OSTI2024

Dust and Ions: Self Organization and Stability (Final Report)

This project explores the stability and structure of systems with non-reciprocal interactions, challenging the traditional understanding based on Newton's third law, which states that every action has an equal and opposite reaction. Reciprocal forces are fundamental to the stability of systems ranging in size from atomic nuclei to galactic clusters. Our research investigates what happens when the forces between two objects are not equal and opposite. We used dusty plasmas as a model system to study non-reciprocal interactions. In a plasma chamber, micron-sized dust particles acquire a negative charge and form 2D planar "dust crystals" when levitated by the electric field present in the plasma sheath at the interface between the plasma and the lower surface of the chamber. This electric field also drives a vertical ion flow, creating a positively charged "plasma wake" downstream of the dust grains. While horizontally aligned dust grains interact reciprocally, a slight vertical displacement causes non-reciprocal interactions due to the attraction of the lower dust grain to the upper dust grain’s ion wake. Our experiments investigated the range of plasma conditions (gas pressure and system power) where stable dusty plasma structures are able to self-organize, aided by the ion wake. We studied systems ranging from pairs of dust particles to large 2D crystals, providing insights into the conditions that lead to stable or unstable structures. We used numerical simulations to investigate how ion wakes changed in response to changes in the operating conditions as well as how the wakes of separate grains interact when dust grains are in close proximity.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1993

Spectroscopic constraints on the properties of dust in active galactic nuclei

The optical properties of graphite, silicate, and SiC grains over the wavelength range 1000 microns - 1 A are calculated for grains in the 0.005-10-micron size range. Both graphite + silicate (MRN) and graphite + SiC grain mixtures are considered, with various grain size distributions. A detailed radiative transfer calculation is performed to obtain constraints on the emission properties of dust in AGN in either 'optically thin' or optically thick configurations. Warm graphite + silicate or graphite + SiC dust (T is greater than 200 K) with the MRN size distribution and a column density less than about 10 exp 23/sq cm produces a strong silicate or SiC emission feature. Such dust cannot be responsible for the observed IR emission from AGN. MRN dust with a high optical depth at 10 microns produces an emission feature with an amplitude of about 57 percent, in excess of the typical observational limit for most objects. Reddening of the broad emission lines and continuum is unlikely to be common.

Laor, Ari↗
NASA NTRS2004

A MEMS Micro-Translation Stage with Long Linear Translation

A MEMS Micro-Translation Stage (MTS) actuator concept has been developed that is capable of traveling long distances, while maintaining low power, low voltage, and accuracy as required by many applications, including optical coupling. The Micro-Translation Stage (MTS) uses capacitive electrostatic forces in a linear motor application, with stationary stators arranged linearly on both sides of a channel, and matching rotors on a moveable shuttle. This creates a force that allows the shuttle to be pulled along the channel. It is designed to carry 100 micron-sized elements on the top surface, and can travel back and forth in the channel, either in a stepping fashion allowing many interim stops, or it can maintain constant adjustable speeds for a controlled scanning motion. The MTS travel range is limited only by the size of the fabrication wafer. Analytical modeling and simulations were performed based on the fabrication process, to assure the stresses, friction and electrostatic forces were acceptable to allow successful operation of this device. The translation forces were analyzed to be near 0.5 micron N, with a 300 micron N stop-to-stop time of 11.8 ms.

Ferguson, Cynthia K.↗
NASA NTRS2008

Making High-Tensile-Strength Amalgam Components

Structural components made of amalgams can be made to have tensile strengths much greater than previously known to be possible. Amalgams, perhaps best known for their use in dental fillings, have several useful attributes, including room-temperature fabrication, corrosion resistance, dimensional stability, and high compressive strength. However, the range of applications of amalgams has been limited by their very small tensile strengths. Now, it has been discovered that the tensile strength of an amalgam depends critically on the sizes and shapes of the particles from which it is made and, consequently, the tensile strength can be greatly increased through suitable choice of the particles. Heretofore, the powder particles used to make amalgams have been, variously, in the form of micron-sized spheroids or flakes. The tensile reinforcement contributed by the spheroids and flakes is minimal because fracture paths simply go around these particles. However, if spheroids or flakes are replaced by strands having greater lengths, then tensile reinforcement can be increased significantly. The feasibility of this concept was shown in an experiment in which electrical copper wires, serving as demonstration substitutes for copper powder particles, were triturated with gallium by use of a mortar and pestle and the resulting amalgam was compressed into a mold. The tensile strength of the amalgam specimen was then measured and found to be greater than 10(exp 4) psi (greater than about 69 MPa). Much remains to be done to optimize the properties of amalgams for various applications through suitable choice of starting constituents and modification of the trituration and molding processes. The choice of wire size and composition are expected to be especially important. Perusal of phase diagrams of metal mixtures could give insight that would enable choices of solid and liquid metal constituents. Finally, whereas heretofore, only binary alloys have been considered for amalgams, ternary additions to liquid or solid components should be considered as means to impart desired properties to amalgams.

Grugel, Richard↗
NASA NTRS1993

Determination of parameters for hypervelocity dust grains encountered in near-Earth space

Primarily interest was in the determination of the population of micrometeoroids and space debris and interpretation of the hole size in a thin film or in a micropore foam returned from space with theoretical calculations describing the event. In order to augment the significance of the theoretical calculations of the impact event, an experiment designed to analyze the charge production due to hypervelocity impacts on thin films also produced data which described the penetration properties of micron and sub-micron sized projectiles. The thin film penetration sites in the 500 A and 1000 A aluminum films were counted and a size distribution function was derived. In the case of the very smallest dust grains, there were no independent measurements of velocities like that which existed for the larger dust grains (d(sub p) is less than or equal to 1 micron). The primary task then became to assess the relationship between the penetration hole and the particle diameter of the projectile which made the hole. The most promising means to assess the measure of the diameters of impacting grains came in the form of comparing cratering mechanics to penetration mechanics. Future experimentation will produce measurements of the cratering as opposed to the penetrating event. Particles encountered by surfaces while being flown in space will degrade that surface in a systematic manner even when the impact is with small hypervelocity particles, d(sub p) is less than or equal to 10 microns. Though not to a degree which would precipitate a catastrophic failure of a system, the degradation of the materials comprising the interconnected system will occur. It is the degradation of the optical system and the subsequent embrittlement of other materials that can lead to degradation if not to failure. It is to this end that research was conducted to compare the primary consequences for experiments which will be flown to those which have been returned.

Tanner, William G.↗