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NASA NTRS1999

NASA's Space Environments and Effects (SEE) Program: Contamination Engineering Technology Development

ABSTRACT The return of the Long Duration Exposure Facility (LDEF) in 1990 brought a wealth of space exposure data on materials, paints, solar cells, etc. and data on the many space environments. The effects of the harsh space environments can provide damaging or even disabling effects on spacecraft, its materials, and its instruments. In partnership with industry, academia, and other government agencies, National Aeronautics & Space Administration's (NASA's) Space Environments & Effects (SEE) Program defines the space environments and provides technology development to accommodate or mitigate these harmful environments on the spacecraft. This program provides a very comprehensive and focused approach to understanding the space environment, to define the best techniques for both flight and ground-based experimentation, to update the models which predict both the environments and the environmental effects on spacecraft, and finally to ensure that this information is properly maintained and inserted into spacecraft design programs. This paper will describe the current SEE Program and will present SEE contamination engineering technology development and risk mitigation for future spacecraft design.

Pearson, Steven D.↗

NASA NTRS1981

Advanced Microbial Check Valve development

The Microbial Check Valve (MCV) is a flight qualified assembly that provides bacteriologically safe drinking water for the Space Shuttle. The 1-lb unit is basically a canister packed with an iodinated ion-exchange resin. The device is used to destroy organisms in a water stream as the water passes through it. It is equally effective for fluid flow in either direction and its primary method of disinfection is killing rather than filtering. The MCV was developed to disinfect the fuel cell water and to prevent back contamination of stored potable water on the Space Shuttle. This paper reports its potential for space applications beyond the basic Shuttle mission. Data are presented that indicate the MCV is suitable for use in advanced systems that NASA has under development for the reclamation of humidity condensate, wash water and human urine.

Colombo, G. V.↗

NASA NTRS1994

Outgassing considerations for composites in space applications

Composites have been increasingly used in the construction of spacecraft. However, unlike metals, composites must be used with particular discretion in space applications because of their outgassing properties. For example, the outgas materials may cause serious contamination problems and affect the performance of delicate instruments. This paper presents an overview of the testing procedure and acceptance criteria for outgassing selection of spacecraft materials. Since composites can contain and absorb moisture which will outgas in space as water vapor, the test results of moisture absorption and desorption of a composite material are discussed also.

Arsenovic, Petar↗

NASA NTRS1997

Nineteenth Space Simulation Conference Cost Effective Testing for the 21st Century

The Nineteenth Space Simulation Conference was hosted by the Institute of Environmental Sciences (IES) and was supported by the American Institute of Aeronautics and Astronautics (AIAA), the American Society for Testing and Materials (ASTM), the National Aeronautics and Space Administration (NASA), and the Canadian Space Agency (CSA). These proceedings attest to the scope of the conference; papers were presented on topics as diverse as shuttle payload contamination effects, simulating Martian environment for testing, to state-of-the-art 6-axis hydraulic shaker testing system. A good cross section of the international aerospace community took advantage of the opportunity to get together, to share their experiences, and to participate in the technical sessions. The two invited keynote speakers were Lieutenant General Malcolm O'Neill (USA, Ret.), past Director of BMDO, and Mr. Thomas Coughlin, Space Programs Manager at the Johns Hopkins University Applied Physics Laboratory. Their most informative and thought provoking talks were on cost effective testing approaches in Defense Department programs for the 21st Century and what part testing plays in the faster, better, cheaper approach for the NEAR and APL programs, respectively. The preceding tutorial and the tour of the Garber Facility of the Air and Space Museum rounded out a comprehensive conference contributing to the knowledge base vital to cost effective testing for successful missions into the 21st Century.

Stecher, Joseph L., III↗

NASA NTRS1997

Study of SRM Critical Surfaces Using Near Infrared Optical Fiber Spectrometry

The measurement and control of cleanliness for critical surfaces during manufacturing and in service operations provides a unique challenge in the current thrust for environmentally benign processes. Of particular interest has been work performed in maintaining quality in the production of bondline surfaces in propulsion systems and the identification of possible contaminants which are detrimental to the integrity of the bondline. This work requires an in-depth study of the possible sources of contamination, methodologies to identify contaminants, discrimination between contaminants and chemical species caused by environment, and the effect of particular contaminants on the bondline integrity of the critical surfaces. This paper will provide an introduction to the use of Near Infrared (NIR) optical fiber spectrometry in a nondestructive measurement system for process monitoring and how it can be used to help clarify issues concerning surface chemistry. In a previous conference, experimental results for quantitative measurement of silicone and Conoco HD2 greases, and tape residues on solid rocket motor surfaces were presented. This paper will present data for metal hydroxides and discuss the use of the integrating sphere to minimize the effects of physical properties of the surfaces (such as surface roughness) on the results obtained from the chemometric methods used for quantitative analysis.

Workman, G. L.↗

NASA NTRS2006

The Use of Liquid Isopropyl Alcohol and Hydrogen Peroxide Gas Plasma to Biologically Decontaminate Spacecraft Electronics

Legitimate concern exists regarding sending spacecraft and their associated hardware to solar system bodies where they could possibly contaminate the body's surface with terrestrial microorganisms. The NASA approved guidelines for sterilization as set forth in NPG 8020.12C, which is consistent with the biological contamination control objectives of the Committee on Space Research (COSPAR), recommends subjecting the spacecraft and its associated hardware to dry heat-a dry heat regimen that could potentially employ a temperature of 110(deg)C for up to 200 hours. Such a temperature exposure could prove detrimental to the spacecraft electronics. The stimulated growth of intermetallic compounds (IMCs) in metallic interconnects and/or thermal degradation of organic materials composing much of the hardware could take place over a prolonged temperature regimen. Such detrimental phenomena would almost certainly compromise the integrity and reliability of the electronics. Investigation of sterilization procedures in the medical field suggests that hydrogen peroxide (H202) gas plasma (HPGP) technology can effectively function as an alternative to heat sterilization, especially for heat-sensitive items. Treatment with isopropyl alcohol (IPA) in liquid form prior to exposure of the hardware to HPGP should also prove beneficial. Although IPA is not a sterilant, it is frequently used as a disinfectant because of its bactericidal properties. The use of IPA in electronics cleaning is widely recognized and has been utilized for many years with no adverse affects reported. In addition, IPA is the principal ingredient of the test fluid used in ionic contamination testers to assess the amount of ionic contamination found on the surfaces of printed wiring assemblies. This paper will set forth experimental data confirming the feasibility of the IPA/H202 approach to reach acceptable microbial reduction (MR) levels of spacecraft electronic hardware. In addition, a proposed process flow in which both IPA liquid and HPGP are utilized will be presented in Section 7.0.

microbial reduction↗

NASA NTRS2020

Atacama Cosmology Telescope: Component-separated maps of CMB temperature and the thermal Sunyaev-Zel'dovich effect

Optimal analyses of many signals in the cosmic microwave background (CMB) require map-level extraction of individual components in the microwave sky, rather than measurements at the power spectrum level alone. To date, nearly all map-level component separation in CMB analyses has been performed exclusively using satellite data. In this paper, we implement a component separation method based on the internal linear combination (ILC) approach which we have designed to optimally account for the anisotropic noise (in the 2D Fourier domain) often found in ground-based CMB experiments. Using this method, we combine multi-frequency data from the Planck satellite and the Atacama Cosmology Telescope Polarimeter (ACTPol) to construct the first wide area (≈2100 sq. deg.), arcminute-resolution component-separated maps of the CMB temperature anisotropy and the thermal Sunyaev-Zel'dovich (tSZ) effect sourced by the inverse-Compton scattering of CMB photons off hot, ionized gas. Our ILC pipeline allows for explicit deprojection of various contaminating signals, including a modified blackbody approximation of the cosmic infrared background (CIB) spectral energy distribution. The cleaned CMB maps will be a useful resource for CMB lensing reconstruction, kinematic SZ cross-correlations, and primordial non-Gaussianity studies. The tSZ maps will be used to study the pressure pro les of galaxies, groups, and clusters through cross-correlations with halo catalogs, with dust contamination controlled via CIB deprojection. The data products described in this paper are available on LAMBDA.

Mathew S. Madhavacheril↗

NASA NTRS2017

Development and Testing of a Friction-Based Post-Installable Sensor for Subsea Fiber-Optic Monitoring Systems

This paper presents the design and development of a friction-based coupling device for a fiber-optic monitoring system that can be deployed on existing subsea structures. This paper provides a summary of the design concept, prototype development, prototype performance testing, and design refinements of the device. The results of the laboratory testing of the first prototype performed at the National Aeronautics and Space Administration (NASA) Johnson Space Center (JSC) are included in this paper. Limitations of the initial design were identified and future design improvements were proposed. These new features will enhance the coupling of the device and improve the monitoring system measurement capabilities. A major challenge of a post-installed instrumentation monitoring system is to ensure adequate coupling between the instruments and the structure of interest for reliable measurements. Friction-based coupling devices have the potential to overcome coupling limitations caused by marine growth and soil contamination on subsea structures, flowlines or risers. The work described in this paper investigates the design of a friction-based coupling device (friction clamp), which is applicable for pipelines and structures that are suspended in the water column and those that are resting on the seabed. The monitoring elements consist of fiber-optic sensors that are bonded to a metal clamshell with a high-friction coating. The friction clamp has a single hinge design to facilitate the operation of the clamp and dual rows of opposing fasteners to distribute the clamping force on the structure. The friction clamp can be installed by divers in shallow depths or by remotely operated vehicles in deep-water applications. NASA-JSC was involved in the selection and testing of the friction coating, and in the design and testing of the prototype clamp device. Four-inch diameter and eight-inch diameter sub-scale friction clamp prototypes were built and tested to evaluate the strain measuring capabilities of the design under different loading scenarios. The testing revealed some limitations of the initial design concept, and subsequent refinements were explored to improve the measurement performance of the system. This study was part of a collaboration between NASA-JSC and Astro Technology, Inc. within a study called Clear Gulf. The primary objective of the Clear Gulf study is to develop advanced instrumentation technologies that will improve operational safety and reduce the risk of hydrocarbon spillage. NASA provided unique insights, expansive test facilities, and technical expertise to advance these technologies that would benefit the environment, the public, and commercial industries.

Bentley, Nicole↗

NASA NTRS2017

Development and Testing of a Friction-Based Post-Installable Sensor for Subsea Fiber-Optic Monitoring System

Bentley, Nicole L.↗

NASA NTRS2010

Integration and Testing of the Lunar Reconnaissance Orbiter Attitude Control System

Throughout the Lunar Reconnaissance Orbiter (LRO) Integration and Testing (I&T) phase of the project, the Attitude Control System (ACS) team completed numerous tests on each hardware component in ever more flight like environments. The ACS utilizes a select group of attitude sensors and actuators. This paper chronicles the evolutionary steps taken to verify each component was constantly ready for flight as well as providing invaluable trending experience with the actual hardware. The paper includes a discussion of each ACS hardware component, lessons learned of the various stages of I&T, a discussion of the challenges that are unique to the LRO project, as well as a discussion of work for future missions to consider as part of their I&T plan. LRO ACS sensors were carefully installed, tested, and maintained over the 18 month I&T and prelaunch timeline. Care was taken with the optics of the Adcole Coarse Sun Sensors (CSS) to ensure their critical role in the Safe Hold mode was fulfilled. The use of new CSS stimulators provided the means of testing each CSS sensor independently, in ambient and vacuum conditions as well as over a wide range of thermal temperatures. Extreme bright light sources were also used to test the CSS in ambient conditions. The integration of the two SELEX Galileo Star Trackers was carefully planned and executed. Optical ground support equipment was designed and used often to check the performance of the star trackers throughout I&T in ambient and thermal/vacuum conditions. A late discovery of potential contamination of the star tracker light shades is discussed in this paper. This paper reviews how each time the spacecraft was at a new location and orientation, the Honeywell Miniature Inertial Measurement Unit (MIMU) was checked for data output validity. This gyro compassing test was performed at several key testing points in the timeline as well as several times while LRO was on the launch pad. Sensor alignment tests were completed several times to ensure that hardware remained on a rigid platform.

Simpson, Jim↗

NASA NTRS1983

Environmental Measurements Session summaries

Emphasis was placed on data from payloads flown on the subject flights including results from the Induced Environment Contamination monitor (IECM). Brief summaries of the vibroacoustics, loads, electromagnetic and thermal aspects of the environment, as derived from Shuttle system measurements, were presented primarily to indicate where the environment was different than observed and, therefore, where specification changes may be forthcoming. In addition, brief summaries of two somewhat unexpected effects, the vehicle glow and interaction between the low Earth environment and Shuttle payload by materials were presented as an aid in interpreting other environmental data. Papers for each payload/experiment involved in Shuttle flights were presented essentially in flight related chronological order. A significant portion of time was allocated for presentation of IECM data since this payload was flown on STS-2, STS-3, and STS-4 and, therefore, represents the largest data base relative to the contamination environment. Summaries of papers are presented.

Lehmann, J.↗

NASA NTRS2015

Process Development for Removal of Siloxanes from ISS Atmosphere

Dimethylsilanediol (DMSD) has been identified as a problematic organic contaminant aboard the ISS. This contaminant was initially identified in humidity condensate and in the Water Processor Assembly (WPA) product water in 2010 when routine water quality monitoring an increasing total organic carbon (TOC) trend in the WPA product water. Although DMSD is not a crew health hazard at the levels observed in the product water, it can degrade the WPA catalytic reactor's effectiveness and cause early replacement of Multifiltration Beds. DMSD may also degrade the performance of the Oxygen Generation System (OGS) which uses the WPA product water for electrolysis. An investigation into the source of DMSD has determined that polydimethylsiloxane (PDMS) compounds are likely hydrolyzing in the Condensing Heat Exchangers (CHX) to form DMSD. PDMS compounds are prevalent aboard ISS from a variety of sources, including crew hygiene products, adhesives, caulks, lubricants, and various nonmetallic materials. PDMS compounds are also known to contribute to CHX hydrophilic coating degradation by rendering it hydrophobic and therefore adversely affecting its ability to effectively transmit water to the condensate bus. Eventually this loss in performance results in water droplets in the air flow exiting the CHX, which may lead to microbial growth in the air ducts and may impact the performance of downstream systems. Several options have been evaluated to address these concerns. Modifications to the Water Processor Multifiltration Beds and Catalytic Reactor for removal of DMSD were not considered viable, and did not address the issue with PDMS compound degradation of the CHX coating. Design concepts are now in development for removing PDMS compounds from the air stream before they can reach the CHX coating, thus preventing coating degradation and hydrolysis of the PDMS compounds to DMSD. This paper summarizes the current status of the effort to treat these contaminants on ISS.

Carter, Layne↗

NASA NTRS2018

Preliminary Testing of NASA's Molecular Adsorber Coating Technology for Future Missions to Mars

The Molecular Adsorber Coating (MAC) is a sprayable coatings technology that was developed at NASA Goddard Space Flight Center (GSFC). The coating is comprised of highly porous, zeolite materials that help capture outgassed molecular contaminants on spaceflight applications. The adsorptive capabilities of the coating can alleviate molecular contamination concerns on or near sensitive surfaces and instruments within a spacecraft. This paper will discuss the preliminary testing of NASA’s MAC technology for use on future missions to Mars. The study involves evaluating the coating’s molecular adsorption properties in simulated test conditions, which include the vacuum environment of space and the Martian atmosphere. MAC adsorption testing was performed using a commonly used plasticizer called dioctyl phthalate (DOP) as the test contaminant.

CO2↗

NASA NTRS2018

Preliminary Testing of NASA's Molecular Adsorber Coating Technology for Future Missions to Mars

The Molecular Adsorber Coating (MAC) is a sprayable coatings technology that was developed at NASA Goddard Space Flight Center (GSFC). The coating is comprised of highly porous, zeolite materials that help capture outgassed molecular contaminants on spaceflight applications. The adsorptive capabilities of the coating can alleviate molecular contamination concerns on or near sensitive surfaces and instruments within a spacecraft. This paper will discuss the preliminary testing of NASA's MAC technology for use on future missions to Mars. The study involves evaluating the coating's molecular adsorption properties in simulated test conditions, which include the vacuum environment of space and the Martian atmosphere. MAC adsorption testing was performed using a commonly used plasticizer called dioctyl phthalate (DOP) as the test contaminant.

outgassing↗

NASA NTRS2005

Amateur Cleanrooms: Costs May Not Offset Benefits

Contamination and Coatings Branch During my career at NASA, I have encountered a variety of cleanroom systems. With many projects, cost pressures and lack of adequate facilities have forced the managers to resort to amateur cleanrooms to manufacture spacecraft and instruments. These rooms are usually spaces that have been used for other purposes that are converted to cleanroom, usually without the assistance of a contamination control specialist. Often, scientists and engineers are successful in converting an area for experimental use. However, when the area is used for production, countless difficulties are encountered. This paper will document some of the disasters that I have personally witnessed and offer some guidelines for contamination professionals to follow if you are called upon to assist in the development of new cleanrooms. Cleanroom come in all shapes and sizes from special purpose mini-environments (such as flow benches) to large, expansive production facilities. These areas may require a variety of unit operations to be carried out within a short range of each other. The design of the cleanroom should account for compatibilities of these operations to protect the product and personnel. The level of cleanliness has traditionally been associated with the method of ventilation. However, just because and =ea has HEPA filters and greater that 20 air changes per hour does not mean that it is a cleanroom. Airflow is extremely complex; the only way to properly design a cleanroom is through the use of a computer based model. In the aerospace industry, few engineered cleanrooms are modeled. Modeling has been perceived as expensive; however, modern programs and fast computers are changing perception. It is the lack of appreciation for how air flow and location within a cleanroom affects the product that causes most of the problems I have experienced. Currently, the rules defining the best air flow design practices are based on simplistic historical data that are often wrong. The performance of a cleanroom is defined by a set of complex interactions between the airflow, sources of contamination and heat, position of the air terminals and exhausts as well as the objects occupying the space in question. These subtleties are almost never appreciated in the setup of amateur cleanrooms (and sadly, in some engineered cleanroom as well). Experience with the room, measurement of air flows in the room, and black light inspections can be used to

Ramsey, W. Lawrence↗

NASA NTRS2017

Electronic Crosstalk Impact Assessment in the Terra MODIS Mid-Wave Infrared Bands

The Moderate Resolution Imaging Spectroradiometer (MODIS) on board the Terra spacecraft is one of thekey instruments in NASA's Earth Observing System. Since 2000, MODIS has collected continuous data in 36spectral bands ranging in wavelength between 0.4 Âµm and 14.2 Âµm. Since before launch, signal contamination inthe form of electronic crosstalk has been observed in many of the MODIS thermal emissive bands, particularlyfor bands 27 30, a correction for which has been applied to the current Collection 6 algorithm. The mid-waveinfrared bands in Terra MODIS, 20 25, also show signs of electronic crosstalk contamination, which can beseen clearly during observations of the Moon. In this paper, we'll present an impact assessment of electroniccrosstalk on the mid-wave infrared bands in Terra MODIS. We will also derive correction coefficients from thelunar observations, which can be applied to correct the calibrated radiance in the MODIS Level-1B product. Wewill provide an analysis of these results and potential improvements to the MODIS Level-1B product.

calibration↗

NASA NTRS1995

Planetary Protection and Mars Exploration

Planetary spacecraft to explore Mars are subject to international and NASA policy regarding biological cleanliness. This policy is referred to as planetary protection and it establishes guidelines to prevent biological cross-contamination of planets during solar system exploration missions. Mars mission designs and exploration strategies are incomplete without consideration of planetary protection. In this paper, the foundation for planetary protection policy will be reviewed and key issues identified. Existing guidelines governing both forward and back contamination will be summarized. Various Mars exploration scenarios will be examined and the impact of planetary protection requirements will be assessed. Technical issues that need resolution will also be identified. Finally, there will be a discussion of anticipated public attitudes concerning the risk of back contamination from Mars sample return missions.

DeVincenzi, D. L.↗

NASA NTRS1975

Migratory gold resistive shorts - Chemical aspects of a failure mechanism

Integrated-circuit devices using the Ti/W/Au metal system are subject to failure mechanisms based on electrolytic corrosion. The migratory gold resistive short (MGRS) failure mode is one example of this mechanism and results in the formation of filamentary or dendritic deposits of gold between adjacent stripes on the IC chip. This reaction requires the presence of a sufficient amount of water, a bias voltage between adjacent stripes, and the activation of the cathodic (-) stripe. Gold ions are transported from anode to cathode through a film of moisture adsorbed on the surface of the chip; halide ions are probably involved in the transfer. Their presence is verified experimentally by X-ray photoelectron spectroscopy. Some of the chemical and electrostatic factors involved in the MGRS mechanism are discussed in this paper, including the questions of a threshold level of moisture and contamination.

Grunthaner, F. J.↗