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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 199 records · Page 11
All sourcesNASA NTRSDOE OSTI
NASA NTRS1993

High-Tc thermal bridges for space-borne cryogenic infrared detectors

The potential for using high-temperature superconductive elements, screen-printed onto ceramic substrates, as thermal bridges to replace the currently employed manganin wires is studied at NASA-LaRC. Substrate selection is considered to be the most critical parameter in device production. Due to the glass-like thermal behavior of yttria-stabilized-zirconia (YSZ) and fused silica substrates, these materials are found to reduce the heat load significantly. The estimated thermal savings for superconductive leads printed onto YSZ or fused silica substrates range from 6 to 14 percent.

Wise, S. A.↗
NASA NTRS1993

Superconductivity devices: Commercial use of space

The processing and screen printing of the superconducting BSCCO and 123 YBCO materials on substrates is described. The resulting superconducting properties and the use of these materials as possible electrode materials for ferroelectrics at 77 K are evaluated. Also, work performed in the development of solid-state electromechanical actuators is reported. Specific details include the fabrication and processing of high strain PBZT and PLZT electrostrictive materials, the development of PSZT and PMN-based ceramics, and the testing and evaluation of these electrostrictive materials. Finally, the results of studies on a new processing technology for preparing piezoelectric and electrostrictive ceramic materials are summarized. The process involves a high temperature chemical reduction which leads to an internal pre-stressing of the oxide wafer. These reduced and internally biased oxide wafers (RAINBOW) can produce bending-mode actuator devices which possess a factor of ten more displacement and load bearing capacity than present-day benders.

Haertling, Gene↗
NASA NTRS1995

Characterizing and testing a thermally isolating superconducting link for SAFIRE-like missions

The discovery of a new class of ceramic superconductors with transition temperatures above the boiling point of liquid nitrogen has opened the doors for several space applications. One important space application is the fabrication of an electrically conducting and thermally isolating link to replace manganin wires used in connecting IR detectors to data acquisition electronics on remote sensing platforms like SAFIRE and SIRTF. These NASA platforms designed to monitor the earth's atmosphere from space use infrared detectors which operate at liquid helium temperature (4.2K) for optimum performance. The SAFIRE mission employs hybrid dewars which combine both mechanical and cryogenic liquid cooling. The lifetime of such a mission is limited by the heat conducted through sensor array leads that connect the electronics (at approximately 80 K) to the sensors (at approximately 4 K). Currently these remoter sensing systems use manganin wires to connect the IR detectors to the data acquisition electronics. This link between a detector operating at 4 K and electronics operating at 80 K must be made of material that has high electrical conductivity and high thermal resistance. The YBCO superconductor with a transition temperature, Tc, of 93 K can achieve these conflicting requirements. A link with these characteristics will improve the thermal isolation of IR detectors and will increase the lifetime of the cryogen. The fabrication of an electrically conducting and thermally isolating link that replaces the manganin wires is an important application that will improve thermal isolation of IR detectors and will increase the lifetime of the cryogen. The link is made by screen printing superconducting lines on a low thermal conductivity ceramic substrate. Developing, modeling, and testing this high temperature superconducting link is a collaborative effort among NASA-Langley Research Center, Christopher Newport University (CNU), Clemson University and the industrial companies that have joined the Commercialization of Space Program for the purpose of developing and testing this link. CNU's effort in the development of this superconducting link included the following major efforts: (1) Development of a thermal conductivity measurement system for high temperature superconductors and ceramic materials which are potential candidates for use as substrates in this link. (2) Development of a mathematical model for the superconducting link that studies the effect of materials and geometry on the heat load and life time of missions. (3) Characterization of high Tc materials and assemblies made for space applications. Properties studied include humidity effects and aging effects on high Tc materials. This report summarizes the results of the research studies that were completed. Copies of publications detailing these findings are attached to this report.

Selim, Raouf R.↗
NASA NTRS2000

Thin Film Catalyst Layers for Direct Methanol Fuel Cells

One of the primary obstacles to the widespread use of the direct methanol fuel cell (DMFC) is the high cost of the catalyst. Therefore, reducing the catalyst loading well below the current level of 8-12 mg/cm 2 would be important to commercialization. The current methods for preparation of catalyst layers consisting of catalyst, ionomer and sometimes a hydrophobic additive are applied by either painting, spraying, decal transfer or screen printing processes. Sputter deposition is a coating technique widely used in manufacturing and therefore particularly attractive. In this study we have begun to explore sputtering as a method for catalyst deposition. Present experiments focus on Pt-Ru catalyst layers for the anode.

Witham, C. K.↗
DOE OSTI2015

Glass strengthening and patterning methods

High intensity plasma-arc heat sources, such as a plasma-arc lamp, are used to irradiate glass, glass ceramics and/or ceramic materials to strengthen the glass. The same high intensity plasma-arc heat source may also be used to form a permanent pattern on the glass surface--the pattern being raised above the glass surface and integral with the glass (formed of the same material) by use of, for example, a screen-printed ink composition having been irradiated by the heat source.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Evaluation of Encapsulant Adhesion to Surface Metallization of Photovoltaic Cells: Preprint

Delamination of encapsulant materials from PV cell surfaces often appears to originate at regions with metallization. Using a fracture mechanics based metrology, the adhesion of EVA encapsulant to screen printed silver metallization was evaluated. At room temperature, the fracture energy, Gc [J/m2], of the EVA/silver interface (952 J/m2) was ~70% lower than that of the EVA/AR coating (>2900 J/m2) and ~60% lower than that of the EVA to the surface of cell (2265 J/m2). After only 300 hours of damp heat aging, the adhesion energy of the silver interface dropped to and plateaued at ~50-60 J/m2, while that of the EVA/AR coating and EVA/cell remained mostly unchanged. Elemental surface analysis showed that the EVA separates from the silver in a purely adhesive manner, indicating that bonds at the interface were likely displaced in the presence of humidity and elevated temperature, and may explain the propensity for delamination to occur at metallized surfaces in the field.

14 SOLAR ENERGY↗
DOE OSTI2019

Approaches to Metallization for Poly-Si/SiOx Passivated Contacts

Recent improvements in Si solar cell efficiency beyond 25% have used doped poly-Si/SiOx or a-Si:H passivated contacts, the former culminating in a 25.7% cell with a n-poly-Si/SiOx rear contact 1 that is fundamentally compatible with screen printing and firing. However, metallization of the <100 nm thick stack is challenging and can limit open-circuit voltage (Voc) 2, 3. The goal of the work presented here is to develop metallization routes for poly-Si/SiOx passivated contacts with acceptable contact resistivity and minimized Voc loss. This is approached through incremental as well as disruptive improvements to metal evaporation. We examine all aspects of the poly-Si/SiOx process chain that can contribute to contact performance, including poly-Si/SiOx properties, passivation routes, capping layers, and metal deposition methods and post-treatments. We also discuss how to best quantify the contact resistivity that exists while operating a solar cell at maximum power point. Finally, we present two novel approaches to contacting poly-Si/SiOx - a thermally evaporated ITO interlayer, and a transparent conducting adhesive.

14 SOLAR ENERGY↗
DOE OSTI2020

Light source and method for making a light source

A light source fabrication process to fabricate a customized light source includes attaching a plurality of light emitting diodes to a circuit board, where each light emitting diode is configured to emit light within a same wavelength range. Further, the light source fabrication process includes applying a first phosphor layer to a first set of light emitting diodes of the plurality of light emitting diodes and applying a second phosphor layer to a second set of light emitting diodes of the plurality of light emitting diodes. The phosphor layers are applied to the light emitting diodes using one of a screen printing process and an inkjet printing process. The first phosphor layer is different from and has different optical properties from the second phosphor layer.

42 ENGINEERING↗
DOE OSTI2022

Local nm-Scale Imaging of Electrical Contact for Series Resistance Degradation of Silicon Solar Cells

We report on an electrical conduction mechanism for series resistance (Rs) degradation observed in a utility scale solar farm by nm-scale imaging of the local resistance at the Ag/Si interface of c-Si cell front metallization. Our previous work showed that the I-V measurement of individual cells demonstrated exclusively the cell Rs degradation, and the "beads pattern" of electroluminescence indicated the degradation at the Ag grid of front metallization. Scanning spreading resistance microscopy (SSRM) imaging, which is based on the contact mode of atomic force microscopy and taken on the cross-sections of Ag/Si contact, revealed the electrical conduction pathway of Ag particles in point or small area contact with Si cell emitter. The SSRM results illustrated that the number of electrical contacts in the degraded cell decreased largely compared with the unaffected cell, demonstrating the direct cause of the Rs degradation. This reduction in electrical contact in the degraded cell could be caused by a structural change in the Ag grid during long-term field service: The Ag particles in contact with Si aggregate into the Ag bulk and a highly resistive ceramic oxide is formed in a "belt" shape at the Ag/Si interface. This resistive belt with a thickness of ~1 m blocks the current conduction from cell emitter to the Ag grid. The degraded cell shows both a morphological and chemical difference in the screen-printed finger contact compared to the unaffected cell, which likely caused the different degradation susceptibility during the long-term field service. Our results demonstrate an example of the multi-scale characterization approach for understanding photovoltaic degradation mechanisms.

ENGINEERING,SOLAR ENERGY↗
DOE OSTI2015

Acoustic sensors for fission gas characterization: R and D skills devoted to innovative instrumentation in MTR, non-destructive devices in hot lab facilities and specific transducers for measurements of LWR rods in nuclear plants

First of all, we will present the main principle of the method. A piezoelectric transducer, driven by a pulse generator, generates the acoustic waves in a cavity that may be the fuel rod or a chamber connected to an instrumented rod. The composition determination consists in measuring the time of flight of the acoustic signal emitted. The pressure can be estimated by a calibration process, above the measurement of the amplitude of the signal. Two projects will then be detailed. The first project consists in the development of advanced instrumentation for in-pile experiments in Material Testing Reactor. It constitutes a main goal for the improvement of the nuclear fuel behavior knowledge. This acoustic method was tested with success during a first experiment called REMORA 3, and the results were used to differentiate helium and fission gas release kinetics under transient operating conditions. This experiment was lead at OSIRIS reactor (CEA Saclay, France). As a first step of the development program, we performed in-pile tests on the most sensitive component, i.e., the piezoelectric transducer. For this purpose, the active part of this sensor has been qualified on gamma and neutron radiations and at high temperature. Various industrial piezo-ceramics were exposed to a high activity Cobalt source for few days. The cumulated dose was ranged from 50 kGy up to 2 MGy. Next, these devices were placed inside a Material Test Reactor to investigate their reliability towards neutron fluence. The final fluence after 150 days of irradiation was up to 1.6.10{sup 21}n/cm{sup 2} (for thermal neutron). Irreversible variations have been measured. Next, a specific sensor has been implemented on an instrumented fuel rod and tested in the frame of a REMORA 3 Irradiation test. It was the first experiment under high mixed, temperature neutron and gamma flux. A first irradiation phase took place in March 2010 in the OSIRIS reactor and in November 2010 for the second step of the irradiation. The instrumented fuel rod incorporating the ultrasonic gas composition sensor was finally irradiated during 2 weeks in nominal conditions. Neutronics calculation will be performed in order to calculate the thermal and fast neutron fluence and the gamma dose absorbed by acoustic sensor. A first evaluation gives a thermal fluence about 4,5.10{sup 19} n/cm{sup 2}, a fast neutrons fluence about 4,5.1018 n/cm{sup 2} and a total gamma dose up to 0,25 MGy The maximal temperature during the irradiation test was about 150 C. Although the ultrasonic sensor appears to be damaged, the optimization of the electrical attack parameters and the development of a new signal processing maintain the measurement feasibility up the end of the irradiation campaign. It was the first time that the composition of fission gas has been monitored all along an irradiation experiment in a MTR, giving access to the gas release kinetics. New researches involve thick film transducers produced by screen-printing process in order to propose piezoelectric structures for harsh temperature and irradiation measurements. The second project consists in the development of a non-destructive device that can be directly applied on a LWR fuel rod. The problem to be solved relates to the measurement of the fission gas pressure and composition in a fuel rod using a non-destructive method. Fuel rod internal pressure is one of the safety criteria applied in nuclear power analyses. This criterion must be verified in order to avoid any fuel-cladding gap reopening risk and therefore any local clad ballooning. Apart from the safety implications, this parameter is also a fuel behaviour indicator and reflects the overall fuel performance in operation, but also during shipping and long-term storage. Rod internal pressure is one criterion amongst others, like cladding corrosion, against which the acceptable fuel burn-up limit is set. A sensor has been achieved in 2007. A full-scale hot cell test of the internal gas pressure and composition measurement by an acoustic sensor was conducted successfully between 2008 and 2010 on 5 high burn-up MOX fuel rods and 2 very high burn-up UO{sub 2} fuel rods in LECA Facility at Cadarache Centre. An improvement of this sensor has been proposed, allowing us to divide by two the uncertainty on the pressure measurement. In the case of hot-cell measurements, viscous liquid can be used to couple the sensor with the rod. For gas content with a pressure exceeding 15 bars and a 10% Xe/Kr ratio, such coupling may reduce relative acoustic method accuracy by ±7% for pressure measurement result and ±0.25 % for the assessment of gas composition. These results make it possible to demonstrate the feasibility of the technique on LWR fuel rods. The transducer and the associated methodology are now operational for non-destructive measurements in hot lab facilities and allow characterising the fission gas without puncturing the fuel rods. Up to now, any other non-destructive method can be proposed. A next step will be the development of an industrial application in a fuel storage pool in order to perform a large number of measurements on a fuel assembly in nuclear plants.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
DOE OSTI2016

Electromagnetic and thermal properties of three-dimensional printed multilayered nano-carbon/poly(lactic) acid structures

A new type of light-weight material produced by 3D printing consisting of nano-carbon doped polymer layer followed by a dielectric polymer layer is proposed. We performed temperature dependent characterization and measured the electromagnetic (EM) response of the samples in the GHz and THz range. The temperature dependent structural characteristics, crystallization, and melting were observed to be strongly affected by the presence and the number of nano-carbon doped layers in the sandwich structure. The electromagnetic measurements show a great potential of such a type of periodic material for electromagnetic compatibility applications in microwave frequency range. Sandwich structures containing only two nano-carbon layers already become not transparent to the microwaves, giving an electromagnetic interference shielding efficiency at the level of 8–15 dB. A sandwich consisting of one nano-carbon doped and one polymer layer is opaque for THz radiation, because of 80% of absorption. These studies serve as a basis for design and realization of specific optimal geometries of meta-surface type with the 3D printing technique, in order to reach a high level of electromagnetic interference shielding performance for real world EM cloaking and EM ecology applications.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2021

Investigating the Impact of Thickness, Calendering and Channel Structures of Printed Electrodes on the Energy Density of LIBs - 3D Simulation and Validation

Current lithium ion batteries (LIBs) are expensive and bulky, limited by relatively low charging rates. To increase the rate of charging and reduce weight, thin electrodes with high energy density are required. The increase in energy density can be achieved by several techniques including boosting electrolyte transport, high loading/utilization of active material, employing high conductive electrolytes and electrodes with advanced architectures, and increasing cell temperature. In this paper, a 3D physics-based electrochemical model of LIBs is developed in COMSOL simulation software for different thickness, calendering steps as well as channel structures (conical, cylindrical) to optimize the electrode design and in turn maximize volumetric energy density. The simulation results demonstrated that calendering the electrodes with high initial porosity increases the volumetric energy density of the cell. In addition, cylindrical channel structures with relatively lower edge-to-edge distance also results in increased volumetric energy density. The simulation results of the 3D model was validated by comparing it with experimental results.

improving volumetric energy density↗
DOE OSTI2026

Nickel Interlayer for Improved Silver Complex Inks Metallization in GaAs Photovoltaic Devices

Large areas of III-V photovoltaic panels are essential to supplying operational energy for a growing demand of satellites of strategic importance to the United States military, covering a range of applications. High fabrication costs and low manufacturing throughput are key barriers to meeting the necessary supply, which can in turn jeopardize mission success. At the device level, metallization based on printing of complex metal inks has attracted significant research interest due to its potential to substantially reduce processing costs and increase throughput while achieving electrical performance comparable to those of conventional metallization schemes. For GaAs photovoltaic devices, however, reliable electrical contacting remains challenging due to the formation of an interfacial oxide layer at the metal-semiconductor interface. This oxide barrier severely limits current extraction from the PV absorber, resulting in unacceptably high contact resistance. In this study, we report the introduction of a reactive nickel (Ni) interfacial layer between the silver metal fingers and the GaAs substrate to suppress oxide formation while maintaining a low-resistance electrical interface, and show performance data from fully fabricated GaAs devices incorporating the Ni interlayer. These results demonstrate the potential of reactive Ni ink as an effective interfacial layer for improved electrical contacting in low-cost PV metallization schemes.

14 SOLAR ENERGY↗
DOE OSTI2018

Mechanisms of adhesion degradation at the photovoltiac module's cell metallization-encapsulant interface

Adhesion measurements and chemical characterization of the encapsulant/silver metallization interface of a photovoltaic (PV) module through temperature, humidity, and voltage bias exposures were conducted. Results demonstrate two independent degradation mechanisms: (a) with voltage bias, the ionic conduction of Na + ions through the encapsulant results in the formation of sodium silicate at the silver metallization surface, thereby weakening that interface and (b) with moisture ingress, dissociation of the silane bonding to silver in the silver oxide similarly weakens this interface resulting in significantly lower debond energies.

14 SOLAR ENERGY↗
DOE OSTI2017

Adhesion Degradation of the Metallization-Encapsulant Interface

Adhesion of the silver metallization/ encapsulant interface was measured through temperature, humidity and voltage bias stress. Results indicate that adhesion at this interface is severely compromised by even short exposures to humidity and quickly plateaus with further, prolonged, exposure. The magnitude of degradation is also identical to that measured through a three-month outdoor, on-sun, exposure. While the addition of a voltage bias also appears capable of further degrading adhesion below this plateau level, in the absence of humidity, adhesion may be similarly degraded.

14 SOLAR ENERGY↗
NASA NTRS1996

(abstract) Ion-Molecule Reactions at Your Finger Tips

A standalone search engine is described along with a database of ion-molecule kinetics. The engine is available for either Macintosh or IBM/PC computers. The engine will search a supplied database of ion-molecule kinetics data for two body reactions and positive ions. The database includes data found in various publications and reference works written by the author. Currently that database has over 10 600 reaction entries and uses over 1 000 referenced citations. Searches of the database can be by either reactants or products and either ions or neutrals. Narrowing searches can be made on up to three specifications. Reports of the searches are either viewed on the screen or printed. The reports also include the short list of references cited.

ion-molecule reactions search engine database ion-↗