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DOE OSTI2023

A portable and monoenergetic 24 keV neutron source based on 124Sb-9Be photoneutrons and an iron filter

A portable monoenergetic 24 keV neutron source based on the 124Sb-9Be photoneutron reaction and an iron filter has been constructed and characterized. The coincidence of the neutron energy from SbBe and the low interaction cross-section with iron (mean free path up to 29 cm) makes pure iron specially suited to shield against gamma rays from 124Sb decays while letting through the neutrons. To increase the 124Sb activity and thus the neutron flux, a >1 GBq 124Sb source was produced by irradiating a natural Sb metal pellet with a high flux of thermal neutrons in a nuclear reactor. The design of the source shielding structure makes for easy transportation and deployment. A hydrogen gas proportional counter is used to characterize the neutrons emitted by the source and a NaI detector is used for gamma background characterization. At the exit opening of the neutron beam, the characterization determined the neutron flux in the energy range 20–25 keV to be 6.00±0.30 neutrons per cm2 per second and the total gamma flux to be 245±8 gammas per cm2 per second (numbers scaled to 1 GBq activity of the 124Sb source). A liquid scintillator detector is demonstrated to be sensitive to neutrons with incident kinetic energies from 8 to 17 keV, so it can be paired with the source as a backing detector for neutron scattering calibration experiments. This photoneutron source provides a good tool for in-situ low energy nuclear recoil calibration for dark matter experiments and coherent elastic neutrino-nucleus scattering experiments.

Dark Matter detectors (WIMPs, axions, etc.)↗

DOE OSTI2022

Evaluation of a positron-emission-tomography-based SiPM readout for compact segmented neutron imagers

Gamma-ray emission from special nuclear material (SNM) is relatively easy to shield from detection using modest amounts of high-Z material. In contrast, fast-neutrons are much more penetrating and can escape relatively thick high-Z shielding without losing significant energy. Furthermore, fast neutrons provide a clear and unambiguous signature of the presence of SNM with few competing natural background sources. The challenge of detecting fast neutrons is twofold. First, the neutron flux from SNM are only a fraction of the corresponding gamma-ray flux. Second, fast neutrons can be difficult to differentiate from gamma rays. The ability to discriminate gamma rays from neutrons, combined with a neutron imaging capability, can in some situations enable the localization of SNM neutron sources distinct from background. With the developments of pulse-shape-sensitive plastic scintillators that offer excellent gamma-ray/neutron discrimination, and arrays of silicon photomultipliers combined with highly scalable and fast positron-emission-tomography (PET) multi-channel readout systems, field-deployable neutron imagers suitable for SNM detection might now be within reach. In this paper, we present a characterization of the performance of a recently available commercial PET-scanner readout, including its sensitivity to pulse-shape differences between fast neutrons and gamma rays, energy and timing resolution. Here, we find that, while the pulse-shape discrimination is achievable with stilbene, further improvement of the readout is required to achieve it with the PSD-capable available plastic scintillators.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2019

Nuclear recoil scintillation linearity of a high pressure 4 He gas detector

We investigate scintillation linearity of a commercial high pressure 4 He gas detector using monoenergetic 2.8 MeV neutrons from a deuterium-deuterium fusion neutron generator. The scintillation response of the detector was measured for a range of recoil energies between 83 keV and 626 keV by tagging neutrons scattering into fixed angles with a far-side organic scintillator detector. Detailed Monte Carlo simulations were compared to experimental data to determine the linearity of the detector response by comparing the scaling of the energy deposits in the simulations to the detector output. In this analysis, a linear scintillation response corresponds to a consistent value for the scaling factor between simulated energy deposits and experimental data for several different scattering angles. Here we demonstrate that the detector can be used to detect fast neutron interactions down to 83 keV recoil energies and can be used to characterize low-energy neutron sources, one of its potential applications.

47 OTHER INSTRUMENTATION↗

DOE OSTI2023

Studies of event burst phenomenon with SiPMs in liquid nitrogen

Silicon photomultiplier (SiPM) are used to collect scintillation photons in many cryogenic noble liquid detectors deployed around the world, such as DarkSide, nEXO, MEGII, ProtoDUNE and DUNE. An event burst phenomenon was observed during routine characterization on many models of SiPMs operated in liquid nitrogen. These bursts of consecutive pulses are initiated by an intense dark photoelectron pulse with an event rate much lower than the time-uncorrelated thermal dark pulse. Although the rate of these burst events is very low, it can potentially compromise some dedicated rare physics event searches which are also anticipated to be of extremely low rate. Here, we systematically studied the behavior of the event burst phenomenon and identified the probable cause of the phenomenon. Here, this investigation is important for the selection of SiPMs for use in noble liquid detectors, high energy physics experiments, and industrial applications where SiPMs are used in cryogenic environment.

47 OTHER INSTRUMENTATION↗

DOE OSTI2023

Performance and Commissioning of the BigBite Timing Hodoscope for Nucleon Form Factor Measurements at Jefferson Lab

The BigBite Timing Hodoscope detector is the primary subject of this thesis. The Super BigBite Spectrometer is a Jefferson Lab Hall A Collaboration project that has and will continue to measure nucleon electromagnetic form factors. This spectrometer includes the Timing Hodoscope which provides high resolution particle timing data for scattered electrons in the electron arm of BigBite. The Timing Hodoscope utilizes 90, 25 × 25 × 600 mm3 scintillator bars stacked on top of each other to form a single detector plane, and these bars are connected to 180 photo-multiplier tubes via light guides. Particles collide with the scintillating material creating a shower of optical photons and these particle events in the bars are collected to generate signals that are readout by the data acquisition (DAQ) electronics. NINO ASIC amplifier-discriminator cards output signals from the photo-multiplier tubes into analogue and logic signals, which are sent to analogue-to-digital (ADC) and time-to-digital (TDC) converter data acquisition readout modules. This data is then used for analysis of the detector. The focus of this thesis is the construction, commissioning, calibration, and performance of the BigBite Timing Hodoscope before and during the first of five nucleon electromagnetic form factor experiments at Jefferson Lab Hall A. Before the neutron magnetic form factor, G n M, experiment, cosmic ray data was collected during commissioning to confirm proper operation of the Timing Hodoscope electronics by observing the ADC and TDC data. Commissioning studies for charge normalization, gain matching, and other ADC and TDC detector data variables were performed before moving the detector into Hall A. Following installation in Hall A, several calibration studies were implemented to fine-tune the detector in preparation for use in the experiment. The calibration studies included analysis of timing cuts, TDC alignment, the time-walk effect, time difference offsets, and scintillator velocity corrections. Once the Timing Hodoscope was well-calibrated, data-taking during the experiment commenced and the beam-on-target data was used to characterize the Timing Hodoscope performance during the G n M experiment run-time. The performance analysis included studies observing energy deposit, cluster size, rates, accidentals, pile-up, tracking efficiency, position resolution, and time resolution. After application of physics cuts to ensure a data set comprised of particle tracks corresponding to elastic electrons, which is the main data of interest for measurement of G n M, the Timing Hodoscope is shown on average across all kinematic settings to have a >98% tracking efficiency, a position resolution of 4-6 cm in the non-dispersive plane and 1.5-2 cm in the dispersive plane, and a time resolution of 500-750 ps. These performance results are compared to a GEANT4 based performance simulation of the BigBite Timing Hodoscope for reference, showing to what degree the measured performance values match those taken from the simulation.

Marinaro, Ralph↗

NASA NTRS2013

Impacts of Atmospheric Ultrafast Kelvin Waves on Radio Scintillations in the Equatorial Ionosphere

We present a statistical analysis of the amplitudes of GPS scintillations (S4 index) observed throughout 2008–2010 using the satellite radio occultation measurements of the Constellation Observing System for Meteorology, Ionosphere, and Climate (COSMIC). Here, for the first time, periodic variability in the occurrence of S4 is investigated using these data. Significant variations of S4 with periods of 2.5-4 days (quasi-3 days) are identified from the observations during postsunset hours (1900-2400 local time) between 15°S-15°N magnetic latitude during this 3-year interval. Coherence analyses of these variations with the geomagnetic Ap index, solar EUV irradiance, and atmospheric wind measurements from an equatorial mesosphere meteor radar at Thumba, India (8.5°N, 77°E) are performed, providing a measure of the relationship between variations in the scintillations and potential drivers. The quasi-3-day variations in S4 are found to covary with the variations of the three drivers examined. In particular, the S4 signatures are found to be coherent with the atmospheric ultrafast Kelvin (UFK) planetary waves characterized by the zonal wind measurements of the radar. This study shows that these UFK waves are as important as the solar and geomagnetic drivers in forcing the day-to-day variations of the occurrence of equatorial spread F.

Ultra Fast Kelvin planetary wave↗

NASA NTRS1994

Hard X-rays from NGC 4151: A thermal origin?

We present a model for explaining the recent combined X-ray and low-energy gamma-ray observations of the Seyfert galaxy NGC 4151. According to this model, soft photons become Comptonized in a hot spot producing simultaneously the low-energy power law as observed by Ginga and the high-energy cutoff observed by the Oriented Scintillation Spectrometer Experiment (OSSE). Implementing recently developed theoretical calculations toward a generalized theory of Comptonization, we were able to find fits to the observations using only two parameters which characterize the physical quantities of the emission region: the plasma cloud optical depth and its temperature. We find that there is no need for additional nonthermal, reflection, or higher temperature thermal components to fit the aforementioned OSSE and Ginga observations. We derive in addition the size of the photon region and the temperature of the upscattered soft photons. We should emphasize, also, that any attempt at fitting only the high-energy parts of the spectrum (photon energies greater than 60 keV) by the Sunyaev & Titarchuk (1980) nonrelativistic Comptonization model leads to an underestimate of the Comptonization parameter y (or, equivalently, to an overestimation of the X-ray power-law spectral slope) and leads, as a result, to incorrect proportions between the low-energy and high-energy parts of the spectrum.

Titarchuk, Lev↗

DOE OSTI2024

Nucleon Structure Studies at Jefferson Lab and the Electron Ion Collider

The research programs of Thomas Jefferson Laboratory (JLab) and the future Electron- Ion Collider (EIC) focus on one of the main goals of strong interaction studies : understanding the structure of nucleons in terms of the quarks and gluons composing them. Their structure is encoded in functions such as Generalized Parton Distributions (GPDs), which describe how quarks and gluons’ transverse position and longitudinal momentum are distributed inside nucleons. GPDs allow to obtain three-dimensional pictures of nucleons and to understand some of their fundamental properties, such as their internal pressure or the emergence of their spin from the dynamics of the partons composing them. At JLab and the EIC, electron beams are used to probe nucleons. Measurement of reactions such as Deeply Virtual Compton Scattering (DVCS) allows access to GPDs. The first longitudinally polarized-target experiment of the CLAS12 program at Jlab took place in 2022-2023. Combining polarized electron beams and nucleon targets, this experiment offers unique access to observables that allow the measurement of different types of GPDs. In particular, the DVCS beam- and target-spin asymmetries for protons and neutrons in deuterium will be measured for the first time. They give access to kinds of GPDs that are still poorly known, and the comparison between proton and neutron data will allow the extraction of the flavor dependence of the structure of nucleons. Specific analysis methods have been implemented to work with a polarized nuclear target and are presented in this thesis. These methods allow to obtain preliminary results for the asymmetries, waiting for the complete statistics to be available. In the long term, the experimental program for the EIC has been established with a strong emphasis on the measurement of the structure of nucleons at high energy. Measurements of reactions such as DVCS impose strict requirements on the electromagnetic calorimeter that will allow to measure the energy of the scattered electrons and photons. This calorimeter, which is under development, will be based on scintillating crystals read by Silicon Photomultipliers (SiPMs). A new type of glass-based scintillating material was tested, evaluating the possibilities to meet the technical requirements concerning their light yield and resistance to radiation damage in particular. Several models of SiPMs have been characterized, demonstrating they can operate over the vast energy range necessary to address the physics case at the EIC and providing guidelines for developing their readout electronics.

Pilleux, Noemie↗

DOE OSTI2020

Temporal Characterization of Tritium Smear Activities

Tritium collection efficiency varies as a function of smear media. The use of porous smear materials leads to an increase in the measured tritium activity as a function of time when the measurement is performed with liquid scintillation counters. Operational inclusion of the efficiency differences and the time dependence of the tritium smear activity is necessary to preclude inadvertently releasing materials or areas. Thomas Jefferson National Laboratory Radiological Control Department identified a contaminated stainless steel containment vessel that previously housed a target containing more than 37 TBq of tritium. The item was systematically sectioned and surveyed to compare three smear types: water-wetted cotton swabs, water-wetted paper smears, and ethanol-wetted Styrofoam wipes (NUC-Wipes™). The total activity of each section was determined using repeated decontamination. The time dependence of the measured activity was also studied. The measured activity of both paper smears and cotton swabs showed significant time dependence. The cotton swabs also showed significantly reduced collection efficiency. Given the widespread use of both of these media in routine contamination surveys, site operational limits were derived using fitted curves for time dependence and average efficiency results. In conclusion, the use of these more restrictive limits allows for rapid measurement of tritium smears while ensuring regulatory compliance.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

DOE OSTI2021

Development of a 83 mKr source for the calibration of the CENNS-10 liquid argon detector

We report on the preparation of and calibration measurements with a 83 mKr source for the CENNS-10 liquid argon detector. 83 mKr atoms generated in the decay of a 83 Rb source were introduced into the detector via injection into the Ar circulation loop. Scintillation light arising from the 9.4 keV and 32.1 keV conversion electrons in the decay of 83 mKr in the detector volume were then observed. This calibration source allows the characterization of the low-energy response of the CENNS-10 detector and is applicable to other low-energy-threshold detectors. The energy resolution of the detector was measured to be 9% at the total 83 mKr decay energy of 41.5 keV. Lastly, we performed an analysis to separately calibrate the detector using the two conversion electrons at 9.4 keV and 32.1 keV.

47 OTHER INSTRUMENTATION↗

DOE OSTI2022

Characterization of PIPS detectors for measurement of radioxenon

The International Monitoring System arm of the Comprehensive Nuclear-Test-Ban Treaty Organization utilizes sampling of atmospheric radioxenon to scan the world for nuclear testing events. Current designs utilized in the field involve plastic scintillator cells run in coincidence with Sodium Iodide (NaI) or High Purity Germanium (HPGe) detectors. The use of plastic scintillators as electron detectors exhibit some issues in comparison to other materials. Silicon detectors are analyzed as an alternative to plastic scintillators for beta detection based on their higher energy resolution and lowered memory effect. A radioxenon detection setup was created with the intent of measuring radioxenon samples using coincidence counting between silicon and NaI detectors as well as silicon and HPGe. Finally, the absolute efficiency of both setups is calculated and compared.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

DOE OSTI2024

Source shape estimation for neutron imaging systems using convolutional neural networks

Neutron imaging systems are important diagnostic tools for characterizing the physics of inertial confinement fusion reactions at the National Ignition Facility (NIF). In particular, neutron images give diagnostic information on the size, symmetry, and shape of the fusion hot spot and surrounding cold fuel. Images are formed via collection of neutron flux from the source using a system of aperture arrays and scintillator-based detectors. Currently, reconstruction of fusion source geometry from the collected neutron images is accomplished by solving a computationally intensive maximum likelihood estimation problem via expectation maximization. In contrast, it is often useful to have simple representations of the overall source geometry that can be computed quickly. In this work, we develop convolutional neural networks (CNNs) to reconstruct the outer contours of simple source geometries. We compare the performance of the CNN for penumbral and pinhole data and provide experimental demonstrations of our methods on both non-noisy and noisy data.

Machine learning, neutron imaging, source reconstr↗

NASA NTRSDate not supplied

Performance of A Real-Time Photon Counting Optical Receiver in the Presence of Emulated Channel Fading

Free-space optical communication links with terrestrial ground stations experience fading due to atmospheric scintillation and beam pointing. Fiber-coupled receiver systems experience additional fading at the interface between the fiber and free-space optics of the telescope. The National Aeronautics and Space Administration (NASA) Glenn Research Center (GRC) has characterized a real-time photon-counting optical ground receiver system with an atmospheric fade emulation system. The receiver system is comprised of a fiber interconnect, an array of superconducting nanowire single photon detectors (SNSPDs), and a field programmable gate array (FPGA) based receive modem. Two fiber interconnect/detector architectures have been studied. One architecture uses a 70-mode photonic lantern coupled to seven single pixel SNSPDs. The other architecture uses a 10-mode few-mode fiber (FMF) coupled to a 15-pixel SNSPD array. The receiver system complies with the Consultative Committee for Space Data Systems (CCSDS) Optical Communications High Photon Efficiency Coding and Synchronization Standard, which uses serially concatenated convolutionally coded pulse-position modulation (SCPPM). The CCSDS standard is designed for use in low photon flux missions, including the Orion Artemis-II Optical (O2O) communications demonstration. The standard utilizes a convolutional symbol interleaver which can be resized to mitigate different fades. The fade emulation system employed in this work emulates scintillation-induced, pointing-induced, and coupling-induced fading. This paper gives an overview of the real-time optical receiver system and the fade emulation system. It presents tests results which show the impact of fading on the performance on the receiver. The test results show that in the presence of channel fading, the 70-mode photonic lantern outperforms the 10-mode FMF under higher (D/r_0=9) turbulence conditions due to high fiber-coupling-induced fading and fiber coupling loss on the 10-mode FMF. When operating in lower turbulence (D/r_0=4), the 10-mode FMF outperforms the 70-mode photonic lantern. The paper also shows a larger convolutional interleaver improves the system performance as long as the receiver does not lose acquisition.

optical communications↗

NASA NTRSDate not supplied

Performance of a real-time photon counting optical receiver in the presence of emulated channel fading

optical communications↗

DOE OSTI2020

Onset of Fogging and Degradation in Polyvinyl Toluene-Based Scintillators

Plastic-based gamma-ray detector materials such as polyvinyl toluene (PVT) occasionally suffer from loss of optical light transmission due to internal defects or “fogging” when exposed to some environmental conditions over time. Fogging results in reduced scintillation light propagated to the photomultiplier tube for collection. Investigations of the physical cause of these defects and their associated environmental conditions are ongoing. The goal of this work was to characterize the signs and effects of fogging over a simulated 22-year lifespan of the PVT in outdoor environments. Here, two potential mitigation methods were also evaluated, and one successfully mitigated the phenomena.

36 MATERIALS SCIENCE↗

NASA NTRS1979

Prospects for experimental research on black holes in binary systems

Cygnus X-1, the single widely accepted example of a black hole in a binary system, is characterized by unusual X-ray properties. The X-ray spectrum of Cygnus X-1 is not cut off above 20 keV, as in most strong X-ray sources. Recent scintillation counter measurements reveal a power law spectrum extending from 40 to 200 keV with a photon spectral index of approximately 2.2. However, it is not clear that these and other X-ray properties of the system are related to the black-hole nature of Cygnus X-1. It is suggested that without a direct test to show that the mass of the compact object in other systems similar to Cygnus X-1 (Circinus X-1 and GX339-4) exceeds the limit of the neutron star mass, a better understanding of the accretion disk phenomenon must be achieved to demonstrate how the properties peculiar to these systems are related to the black hole nature of the compact object. Current accretion disk models are examined, including the alpha-accretion disk and two-temperature accretion disk models.

Long, K. S.↗

DOE OSTI2022

Standard Analytical Methods for Pyrolysis Bio-Oils

There has been significant recent interest in the production of renewable fuels and chemicals from biomass and waste feedstocks. Pyrolysis pathways produce a liquid bio-oil product, which must be processed further, or upgraded, to yield fuel or chemical products. Bio-oils are very complex and often unstable samples, and research and development on upgrading processes needs reliable analytical information. In particular, chemical characterization techniques are needed to quantify both functional groups and individual compounds present in bio-oils. Reliable analytics are also needed to enable the bioenergy industry, as industrial facilities often have different analytical needs and capabilities than research facilities. In this presentation, we will discuss the development of a suite of standard analytical methods for pyrolysis bio-oils. Analytical methods to be discussed include: Determination of Carbon, Hydrogen, Nitrogen, and Oxygen in bio-oils; Accelerated Aging of Fast Pyrolysis Bio-oil using Carbonyl Titration; Determination of Water Content in Bio-oils by Volumetric Karl Fischer Titration; Determination of Carbon Functional Groups; Elemental Analysis of Bio-oils by Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES) - Na, K, Mg, Ca, S, P, and Fe; Determination of Phenolic Groups in Bio-oils using Revised Folin-Ciocalteu Methods: Single Cuvette and Plate Reader; Corrosivity of Bio-oils: Screening Test using Metal Leaching; Determination of Biogenic Content by 14C Measurement using Liquid Scintillation Counter. These new analytical methods are publicly available as Laboratory Analytical Procedures (https://www.nrel.gov/bioenergy/bio-oil-analysis.html), along with previously developed standard methods: GC-MS, Acid Titration, Carbonyl Titration, and 31P NMR. Additionally, the development of diffusion ordered NMR for characterization of bio-oil molecular weight will be discussed. Collectively, this suite of analytical methods represents the most comprehensive set of standard methods available for pyrolysis bio-oils. These standard methods are commonly used by the bioenergy community, and provide reliable information that enables research, scaleup, and industrial processing of biomass to produce renewable fuels and chemicals.

analytical↗

DOE OSTI2019

The radioactive source calibration system of the PROSPECT reactor antineutrino detector

The Precision Reactor Oscillation and Spectrum (PROSPECT) Experiment is a reactor neutrino experiment created to search for sterile neutrinos with a mass on the order of 1 eV/c 2 and to measure the spectrum of electron antineutrinos from a highly-enriched 235 U nuclear reactor. The PROSPECT detector consists of an 11 by 14 array of optical segments in 6 Li-loaded liquid scintillator at the High Flux Isotope Reactor in Oak Ridge National Laboratory. Antineutrino events are identified via inverse beta decay and read out by photomultiplier tubes located at the ends of each segment. The detector response is characterized using a radioactive source calibration system. Here, we describe the design, operation, and performance of the PROSPECT source calibration system.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗