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At least 199 records · Page 11

Ultrasonic Verification of Metal-Grain Size

Ultrasonic attenuation as function of frequency determined for metal sample having known mean grain diameter. Once function determined for one sample of material, scaled to determine mean grain size of other samples of materials. Results suggest ultrasonic approach viable for verifying effects of heat treatments that vary grain size. Uses of this technology include nondestructive ultrasonic verification size heat treatments and other online inspection systems.

Generazio, E. R.↗

Nondestructive ultrasonic characterization of engineering materials

The development of an ultrasonic method for the nondestructive characterization of mechanical properties of engineering material is described. The method utilizes the nonlinearity parameter measurement which describes the anharmonic behavior of the solid through measurements of amplitudes of the fundamental and of the generated second harmonic ultrasonic waves. The nonlinearity parameter is also directly related to the acoustoelastic constant of the solid which can be determined by measuring the linear dependence of ultrasonic velocity on stress. A major advantage of measurements of the nonlinearity parameter over that of the acoustoelastic constant is that it may be determined without the application of stress on the material, which makes it more applicable for in-service nondestructive characterization. The relationships between the nonlinearity parameter of second-harmonic generation and the percentage of solid solution phase in engineering materials such as heat treatable aluminum alloys was established. The acoustoelastic constants are measured on these alloys for comparison and confirmation. A linear relationship between the nonlinearity parameter and the volume fraction of second phase precipitates in the alloys is indicated.

Salama, K.↗

Ultrasonic nondestructive materials characterization

A brief review of ultrasonic wave propagation in solid materials is presented with consideration of the altered behavior in anisotropic and nonlinear elastic materials in comparison with isotropic and linear elastic materials. Some experimental results are described in which ultrasonic velocity and attenuation measurements give insight into materials microstructure and associated mechanical properties. Recent developments with laser beam non-contact generation and detection of ultrasound are presented. The results of several years of experimental measurements using high-power ultrasound are discussed, which provide substantial evidence of the inability of presently accepted theories to fully explain the interaction of ultrasound with solid materials. Finally, a special synchrotron X-ray topographic system is described which affords the possibility of observing direct interaction of ultrasonic waves with the microstructural features of real crystalline solid materials for the first time.

Green, R. E., Jr.↗

Ultrasonic characterization of microstructure in powder metal alloy

The ultrasonic wave propagation characteristics were measured for IN-100, a powder metallurgy alloy used for aircraft engine components. This material was as a model system for testing the feasibility of characterizing the microstructure of a variety of inhomogeneous media including powder metals, ceramics, castings and components. The data were obtained for a frequency range from about 2 to 20 MHz and were statistically averaged over numerous volume elements of the samples. Micrographical examination provided size and number distributions for grain and pore structure. The results showed that the predominant source for the ultrasonic attenuation and backscatter was a dense (approx. 100/cubic mm) distribution of small micropores (approx. 10 micron radius). Two samples with different micropore densities were studied in detail to test the feasibility of calculating from observed microstructural parameters the frequency dependence of the microstructural backscatter in the regime for which the wavelength is much larger than the size of the individual scattering centers. Excellent agreement was found between predicted and observed values so as to demonstrate the feasibility of solving the forward problem. The results suggest a way towards the nondestructive detection and characterization of anomalous distributions of micropores when conventional ultrasonic imaging is difficult. The findings are potentially significant toward the application of the early detection of porosity during the materials fabrication process and after manufacturing of potential sites for stress induced void coalescence leading to crack initiation and subsequent failure.

Tittmann, B. R.↗

Ultrasonic measurement of porosity in casts and welds

The development of a quantitative nondestructive method which involves ultrasonic attenuation measurements in frequency domain to determine volume fraction of porosity in aluminum cast is discussed. The aluminum alloy A357 casting samples were produced at the Ohio State University Foundry with controlled porosity contents ranging from 0% to 6%. A computer controlled system was used to direct ultrasonic beam to a test sample to different places to conduct ultrasonic attenuation measurements. The plot of attenuation coefficients as a function of frequency was then evaluated based on existing theories to determine volume fraction of porosity and pore size.

Adler, L.↗

Analytical ultrasonics for structural materials

The application of ultrasonic velocity and attenuation measurements to characterize the microstructure of structural materials is discussed. Velocity measurements in cast stainless steel are correlated with microstructural variations ranging from equiaxed (elastically isotropic) to columnar (elastically anisotropic) grain structure. The effect of the anisotropic grain structure on the deviation of ultrasonic waves in cast stainless steel is also reported. Field-implementable techniques for distinguishing equiaxed from columnar grain structures in cast strainless steel structural members are presented. The application of ultrasonic velocity measurements to characterize structural ceramics in the green state is also discussed.

Kupperman, D. S.↗

Ultrasonic characterization of structural ceramics

Ultrasonic velocity and attenuation measurements were used to characterize density and microstructure in monolithic silicon nitride and silicon carbide. Research samples of these structural ceramics exhibited a wide range of density and microstructural variations. It was shown that bulk density variations correlate with and can be estimated by velocity measurements. Variations in microstructural features such as grain size or shape and pore morphology had a minor effect on velocity. However, these features had a pronounced effect on ultrasonic attenuation. The ultrasonic results are supplemented by low-energy radiography and scanning laser acoustic microscopy.

Klima, S. J.↗

Analytical ultrasonics for evaluation of composite materials response. Part 1: Physical interpretation

The phenomena associated with the propagation of elastic waves in anisotropic materials are discussed. Wave modes propagating in general directions relative to the material coordinate system are not purely longitudinal nor transverse. Hence the generation of ultrasonic waves by common piezoelectric transducers will generate multiple modes to some extent. The received signals will likely be a combination of different modes. When using two transducers to send and receive ultrasonic waves, deviation of the energy flux vector may reduce the apparent value of the received signal unless the proper orientation of the two transducers with respect to one another is taken into account. And application of reflection from plane boundaries for the purposes of making certain measurements may lead to misinterpretation of results unless one is aware of the differences in multiple mode generation and critical angle phenomena between isotropic and anisotropic materials. When studies or characterizations of composite materials by ultrasonics are to be performed, these phenomena must be taken into consideration so that proper and correct application and interpretation of the measurements can be made. Finally, attention must be drawn again to the fact that composite materials are heterogeneous by definition. The results discussed here have been determined for homogeneous materials only. While the assumption of homogeneity appears to be valid for certain wavelength ranges in composites, future work must continue to study the phenomena of wave propagation in anisotropic, nonhomogeneous materials.

Henneke, E. G., II↗

Gain-Compensating Circuit For NDE and Ultrasonics

High-frequency gain-compensating circuit designed for general use in nondestructive evaluation and ultrasonic measurements. Controls gain of ultrasonic receiver as function of time to aid in measuring attenuation of samples with high losses; for example, human skin and graphite/epoxy composites. Features high signal-to-noise ratio, large signal bandwidth and large dynamic range. Control bandwidth of 5 MHz ensures accuracy of control signal. Currently being used for retrieval of more information from ultrasonic signals sent through composite materials that have high losses, and to measure skin-burn depth in humans.

Kushnick, Peter W.↗

Ultrasonic determination of recrystallization

Ultrasonic attenuation was measured for cold worked Nickel 200 samples annealed at increasing temperatures. Localized dislocation density variations, crystalline order and colume percent of recrystallized phase were determined over the anneal temperature range using transmission electron microscopy, X-ray diffraction, and metallurgy. The exponent of the frequency dependence of the attenuation was found to be a key variable relating ultrasonic attenuation to the thermal kinetics of the recrystallization process. Identification of this key variable allows for the ultrasonic determination of onset, degree, and completion of recrystallization.

Generazio, E. R.↗

Correlation of the deply technique with the ultrasonic imaging of impact damage in graphite/epoxy composites

A quantitative ultrasonic technique for the nondestructive assessment of impact damage is described. The method, which involves digitizing the entire backscattered ultrasonic wave from a sample, was applied to two test panels removed from a 16-ply graphite/epoxy laminate and impacted with an aluminum ball fired at a velocity of 150 ft/sec. The results of the ultrasonic NDE were compared with the results obtained using the destructive deply technique of Freeman (1984). The NDE method provides through-the-thickness information on damage and only requires access to a single side of the material, while the deply technique gives exact information on the actual damage. Good quantitative agreement between the two techniques was obtained.

Smith, B. T.↗

In-flight measurement of ice growth on an airfoil using an array of ultrasonic transducers

Results from three research flights to obtain in-flight ultrasonic pulse-echo measurements of airfoil ice thickness as a function of time using an array of eight ultrasonic transducers mounted flush with the leading edge of the airfoil are presented. The accuracy of the thickness measurements is found to be within 0.5 mm of mechanical and stereophotograph measurements of the ice accretion. The ultrasonic measurements demonstrate that the ice growth rate typically varies during the flight, with variations in the ice growth rate for dry ice growth being primarily due to fluctuations in the cloud liquid water content. Discrepancies between experimental results and results predicted by an analytic icing code underline the need for a better understanding of the physics of wet ice growth.

Hansman, R. John, Jr.↗

Ultrasonic Determination Of Recrystallization

State of recrystallization identified. Measurement of ultrasonic attenuation shows promise as means of detecting recrystallization in metal. Technique applicable to real-time acoustic monitoring of thermomechanical treatments. Starting with work-hardened material, one ultrasonically determines effect of annealing, using correlation between ultrasonic attenuation and temperature.

Generazio, Edward R.↗

Quantitative non-destructive evaluation of porous composite materials based on ultrasonic wave propagation

Two complementary ultrasonic techniques for characterizing porosity in fiber-reinforced composite laminates are evaluated. Five uniaxial graphite-fiber/epoxy-matrix composites having a range of 1 to 8 percent volume fraction of solid glass inclusions to model porosity were investigated. In one technique, signal loss was measured in transmission mode and slope of attenuation, obtained from the first order coefficient of a two-parameter polynomial fit about the center frequency of the useful bandwidth, was used as the ultrasonic parameter to characterize the porosity. The results of these transmission mode measurements displayed a good correlation between the volume fraction of porosity and the slope of attenuation. Integrated polar backscatter was used as a second ultrasonic parameter for the characterization of the porosity in these samples. A single transducer insonified the samples and measured the resulting backscatter at a polar angle of 30 deg with respect to the normal of the sample surface with the azimuthal angles centered at 0 deg with respect to the fiber orientation (i.e., along the fibers). Integrated polar backscatter also displayed good correlation with the volume fraction of porosity.

Miller, James G.↗

In-flight measurement of ice growth on an airfoil using an array of ultrasonic transducers

Results of preliminary tests to measure ice growth on an airfoil during flight icing conditions are presented. Ultrasonic pulse echo measurements of ice thickness are obtained from an array of eight ultrasonic transducers mounted flush with the leading edge of the airfoil. These thickness measurements are used to document the evolution of the ice shape during the encounter in the form of successive ice profiles. Results from 3 research flights are presented and discussed. The accuracy of the ultrasonic measurements is found to be within 0.5 mm of mechanical and stereo photograph measurements of the ice accretion.

Hansman, R. John, Jr.↗

Ultrasonic techniques for aircraft ice accretion measurement

Ultrasonic pulse-echo measurements of ice growth on cylinders and airfoils exposed to both artificial (icing wind tunnel) and natural (flight) icing conditions are presented. An accuracy of + or - 0.5 mm is achieved with the present method. The ultrasonic signal characteristics associated with each of the two types of icing regimes identified, wet and dry ice growth, are discussed. Heat transfer coefficients are found to be higher in the wind tunnel environment than in flight. Results for ice growth on airfoils have also been obtained using an array of ultrasonic transducers. Icing profiles obtained during flight are compared with mechanical and stereo image measurements.

Hansman, R. John, Jr.↗

Quality Evaluation By Acousto-Ultrasonic Testing Of Composites

Promising nondestructive-testing method based on ultrasonic simulation of stress waves. Report reviews acousto-ultrasonic technology for nondestructive testing. Discusses principles, suggests advanced signal-analysis schemes for development, and presents potential applications. Acousto-ultrasonics applied principally to assess defects in laminated and filament-wound fiber-reinforced composite materials. Technique used to determine variations in such properties as tensile, shear, and flexural strengths and reductions in strength and toughness caused by defects. Also used to evaluate states of cure, porosities, orientation of fibers, volume fractions of fibers, bonding between fibers and matrices, and qualities of interlaminar bonds.

Vary, Alex↗

Ultrasonic attenuation measurements determine onset, degree, and completion of recrystallization

Ultrasonic attenuation was measured for cold worked Nickel 200 samples annealed at increasing temperatures. Localized dislocation density variations, crystalline order and volume percent of recrystallized phase were determined over the anneal temperature range using transmission electron microscopy, X-ray diffraction, and metallurgy. The exponent of the frequency dependence of the attenuation was found to be a key variable relating ultrasonic attenuation to the thermal kinetics of the recrystallization process. Identification of this key variable allows for the ultrasonic determination of onset, degree, and completion of recrystallization.

Generazio, E. R.↗